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川芎在中药复方制剂中的使用及质量控制.pdf

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川芎在中药复方制剂中的使用及质量控制.pdf

SZLŸ1BC“SEB227NULL重现性实验|18MG/ML0VA10NULL,L5Q,‚RSD2395B228NULL测定法SY|VA,KA10NULL,LSYAMN,,BM2BM2NULL00CRAMM0HW19948MIN,‚752081B“SE90C575626MG/GB3NULL‚RAAA660F,RAARB„Z0,05‹L,„01RSBYNLZ0›KY„CBLTV,BRŸ_ZEE†,V0‹KY0‹C0,4|ZEV„04|Ÿ,R9_0BAC0,CM8_,_Ÿ90CB0RAME›,TEL,Z0‹S0,T’,‹Ÿ,ŸZ,VTR4EPB•ID1NULLSE0S0,NULL†S,2005CVIB,312NULLL,BŠ,ˆ,YŽBREJSD0,2006,2633363NULLA,ˆBRSJ0,2006,2856644NULLF,WRARSJD0,2005,235914L2007NULL06NULL13;NULL2007NULL11NULL20四川省科技厅重大科技招标项目2006E08091T€E蒋桂华1970NULL,女汉族,四川成都人,现任成都中医药大学药学院副教授,硕士学位,主要从事中药品种质量与资源开发的教学A科研工作0Z4PE蒋桂华,陈素兰,吴媛媛,马逾英D0V0,NULL610075K1通过对中药复方制剂中川芎的入药方式A制剂剂型和质量控制等方面进行统计,分析川芎在中成药中的应用和研究状况BZE分别以中国药典2005年版A部颁标准A文献资料以及部分新药标准为基础,进行含川芎制剂的剂型A入药方式A薄层色谱和含量测定方法及条件的统计BT含川芎的中药成方制剂多为丸剂,其中川芎多以生药粉入药;有部分药品标准建立了专属性较强的川芎质量控制方法,但还有很多未建立川芎薄层鉴别和质量控制方法,在建立了控制方法的标准中,有的还不能反应工艺与质量的关系,甚至还有入药方式与检验结果不相匹配的情况B‚应加强川芎在中药复方制剂中质量控制的研究B1OM川芎;NULL制剂;NULL质量控制MS|R283NULLNULLDSM’ANULLNULLCI|1008NULL0805200803NULL0615NULL03THEAPPLICATIONANDQUALITYCONTROLONTHECOMPOUNDPRESCRIPTIONOFRHIZOMACHUANXNULLIONGJIANGGUINULLHUA,CHENSUNULLLAN,WUYUANNULLYUAN,MAYUNULLYINGCOLLEGEOFPHARMACOLOGY,CHENGDUUNIVERSITYOFTRADITIONALCHINESEMEDICINE,CHENGDU610075,CHINAABSTRACTOBJECTIVETOANALYZETHEACTUALITYOFTHEAPPLICATIONSANDRESEARCHESOFRHIZOMACHUANXIONGINTRADITIONALCHINESEMEDICINECOMPOUNDPRESCRIPTIONSBYSUMMINGUPTHENUMBEROFTHEUSEFORM,PREPARATIONANDTHEQUALITYCONTROLINTHECOMPOUNDPRESCRIPTIONOFRHIZOMACHUANXIONGMETHODSSUMUPTHENUMBEROFTHEMETHODSANDCONDITIONSOFTHEPREPARATION,THEUSEFORM,TLCANDCONTENTDETERMINATIONBASEDONCHINESEPHARMACOPOEIA2005,DEPARTMENTISSUESTANDARD,THELITERATUREMATERINULLALSANDTHEINFORMATIONSONTHENEWMEDICINESRESULTSTHESTATISTICSSHOWSTHATCHINESEPATENTMEDICINECONTAININGRHIZOMACHUANXIONGISTHEMOSTBOLUSANDTHEPOWDEROFRHIZOMACHUANXIONGISWIDELYUSEDINTHEMEDICINESSOMEEFFECTIVEMETHODSUSEDTOCONTROLTHEQUALITYOFRHIZOMACHUANXIONGHAVEBEENESTABLISHED,BUTTHERESTILLEXISTESALOTOFCOMPOUNDPRESCRIPTIONSCONTAINEDRHIZOMACHUANXIONGFORWHICHEFFECTIVEMETHODSHAVENOTBEENESTABLISHEDTOCONTROLTHEQUALITYOFRHIZOMACHUANXNULLIONGALTHOUGHSEVERALCOMPOUNDPRESCRIPTIONSHAVEBEENESTABLISHEDEFFECTIVEMETHODSTOCONTROLTHEQUALITYOFRHIZOMACHUANXNULLIONG,SOMECANNOTREFLECTTHERELATIONSHIPBETWEENTHEPROCESSOFPREPAVATIONANDQUALITY,SOMEUSEFORMSEVENCANNOTMATCHTOTHERESULTOFTHETESTCONCLUSIONITISNECESSARYTOSTRENGTHENTHEQUALITYCONTROLOFRHIZOMACHUANXIONGINCHINESEHERBALMEDINULLCINECOMPOUNDPRESCRIPTIONKEYWORDSRHIZOMACHUANXIONG;NULLPREPARATION;NULLQUALITYCONTROLNULLNULL™SLIGUSTICUMCHUANXIONGHORT2,0,SJ,B›A„ER,∀0B‚AEA癥瘕腹痛A胸胁刺痛A跌打肿痛A头痛A风湿痹痛等症B在∃615∃LISHIZHENMEDICINEANDMATERIAMEDICARESEARCH2008VOL19NO3HSDS02008M1935‹W,AR™A9™A™A{™BMŸZ3H›ER,VVEAUEAAŒŸ7HBN“VA}‚AT9ŽHBD9,S02005M1L529Z4,87C,S009”164B1CA3AAS,M‹S1F†SGQLIGUSTILIDEACHUANXIONGZINEAFERULICACID,N“C5A5A4EA8AAVPA‡SBS02005MNULL†/E0,3†0S0Z4/E†S120A20022007MD/ED†S0SL678C04˜„0ZT›”D9,†CSŸ„E,‚‹0Z4EFƒ217B1NULLC44˜D9|†S4HW›D9,0ADA0†D9,L,Y0ZTEZE‚,SY1B0A†S„D0A†S„DLBTNV1BV1VA,™4”K,4QBƒQ‹0D4˜50B;”‹54A4AR4„†4,ƒB9Q˜G0Fƒ,98C∀64›ZRTBBT4˜AA4A™A4,44˜1‚9F,Q˜04ZZ_B2NULL0ZTD9D9”087,†S535,D32,024BŒ†SADA0†SƒE,ED90ZT,LD9”085,†S512,D6,04BTNV2BV1NULL44˜SƒFƒ4˜02005M†15†610†1115†1620D20022007M0†9S1™4449358312673262386412202013213291134431910713005277R4810913423755‹547758121055480026284002232412521211421‹425346002029†46068736365340540000913}40223200913X064660022324000020020340014103913‹40200100304402220107104100000010140000320507™0011100304W4001100020340001000101400002002034000110240640010000101103}4AAB03ZAA}43A‹3AB{RE4001015†9871701281121253224678NULLNULLV4˜4V2NULLGZTD9TS0†S0D99S1S0†S0D99S130X5124133298491‡ž0100102Y4|911610126208ž0100102X12840298161Xž02002034|52600315140200203••36011016‚4|0400407†SUX,†SX26008134|1100203†SUX,†S4|0100102•0200203†SUX,†SY4|01001020401001024|2120014230X01001024|0400407†98551246607NULLNULLY4|“YA4|A4|;4|CBZI2P,†S;•C•„•NULLNULLV2D9190ZT,130X0,QY4|„XBVN,DUX0ZT1∃616∃HSDS02008M193LISHIZHENMEDICINEANDMATERIAMEDICARESEARCH2008VOL19NO3NULL0ZTB›,YT44|V;VAAYA„3A‰AVŠA†T,4„3AV”F3AŒ2,YNY4|„X0ZT†B3NULL‹ŸE4Fƒ04EFƒ,D9678C4S1EFƒ,HQ„CZEZ›D9„SB/1D9C4C„KY”CSFƒBTNV34BV3NULL4EFƒSŸ9”KYC0200587432†S120535501024121D2002200732263996781317NULLNULLV3V,C4E0L2™AS,RAME;†SL1Z’BA,E;0L17‹5,RAME,CZ4E“,“Z4,‚žRE,C4N{ŸB’4B,Y›1EZEA›BV4NULL4CZESFƒZESSQ”RAME6E1V4V,4›CHSŸS,ZERAMEB4NULLEM1D941NULL川芎薄层鉴别数量统计|0A†SAD„0LC40ZT„VM†ŸD9KYFƒBTNV5BV5NULL0A†SADA0KYD9T0ZT0‹0†SD00†SD0VP0†SD00†SD00‹A0†SD0†930X2215221110100100000030494|130004000000000000008X5410220001000000000015Y4|4600110001000000000013••431000000000000000008000001000000000000001ƒ28146006200010010000040†9383918849721202001000309910322513134NULLNULLVV5VA,›KYH,KVV0‹,QB7KY4,IV0‹S,30X0FƒK,QX„Y4|B42NULL川芎薄层鉴别展开系统条件统计421NULL川芎药材的薄层色谱法相关数据统计4DFSD9,45‚Z7D,žšZYDK37,FS1,žšNULLZY91K34BZ74FNULLZY92,NULLžš41,O_NULL82,F3060∋NULLšNULLZYNULLBZ612505B422NULL阿魏酸的薄层色谱法相关数据统计4DFSD9,13‚Z7D,BZJD4,FS1,NULLBZNULLJ3013K4BZ74NULLBNULLZ90254,YNULLOJšNULLJ10501,JNULLZYNULLJ20101,O_NULLZYJ25121B423NULL大黄酚的薄层色谱法相关数据统计4DFS„1D9,3‚Z7D,SYF3060∋NULLJYNULLJ1551,F3060∋NULLJYNULLJ1471„F6090∋NULLO_NULLJ1032B424NULL川芎嗪的薄层色谱法相关数据统计Z7D1,FNULLO_11B425NULL川芎药材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