川芎在中药复方制剂中的使用及质量控制.pdf

S=zL1bcSEb2.2.7null重现性实验|1.8mg/ml0vA10null,l5Q,RSD=2.395%b2.2.8null测定法sY|vA,kA10null,lsYAMN,bm2bm2null00crAMm0=HW19.948min,752081bSE90c57.5626mg/gb3null)Raaa660F,rAa!*rbZ0,0#5L,01rsbyNLZ0kYcbLTV,bR_ZEe,v0kY0c0,4|ZEV04|,R9_0bac0,cM8_,_90cb0rAME,TeL,)Z0s0,T,z,VTR4ePbID:1nullSE0.S0,nullS.:,2005:cVIB,31.2nulll+,B,.YBR!#eJ.SD0,2006,26(3):336.3nullA,.bRSJ.0,2006,28(5):664.4nullf,wr.ARSJ.D0ea癥瘕腹痛a胸胁刺痛a跌打肿痛a头痛a风湿痹痛等症b在615LISHIZHENMEDICINEANDMATERIAMEDICARESEARCH2008VOL.19NO.3HSDS02008M1935W,+ara9aa$bM+#+Z3her,VV*eaU*ea*a7hbN+VaaT9hbd9,S0!(2005M)1l529Z4,87c+,S0!0916.4%b+1c?a3aas,Ms1FsGQ=(ligustilide)a+(chuanxiongzine)a(ferulicacid),Nc5=a5=a4ea8aavpa=?sbS0!2005Mnull(/e0),30S0Z4(/eS)120a20022007MD(/eD)#s0Sl678c+04+0ZTd9,cse,)+#0Z4ef217b1nullc+44d9|S4HWd9,0aDa0d9,l,y0ZTeZE,sY1B0aSD(+0aSD(l)bTnV1bV1VA,4K,4QbQ0.d450B；54a4aR44,B9Qg0f,98C64#+ZrTbBt4Aa4aa4,4419F,Q04?ZZ_b2null+0ZTd9d9087,S535,D32,024bSaDa0sE,Ed90ZT,#L=d9085,S512,D6,04bTnV2bV1null+44sf402005M1561011151620D20022007M09s1(%)444935831267326238.641220201321329113.443191071300527.7R481091342375.554775812105548.002628400223.241252121142.142534600202.946068736365.34054000091.34022320091.3X0646600223.24000020020.34001410391.34020010030.44022201071.041000000107001110030.4w4001100020.3400010001034000110240.64001000010.1%1(?)03(4aab0)3(Zaa4)3(a3aBre4)00101.59871701281121253224678nullnullV44V2null+gZTd9TS0S0D99s1(%)S0S0D99s1(%)30x512413329849.1010010.2Y?4|%91161012620.8010010.2X1284029816.1x?020020.34|?52600315.14020020.33601101.64|040040.7sux,sX260081.34|110020.3sux,s4|?010010.2%020020.3sux,sY?4|010010.204010010.24|%21200142.30X010010.24|040040.798551246607nullnull%Y?4|Y?A4|a4|；4|cBZI(2P,S)；cnullnullV2d9+190ZT,130x0,QY?4|XbVn,.dux0ZT+1616HSDS02008M193LISHIZHENMEDICINEANDMATERIAMEDICARESEARCH2008VOL.19NO.3null0ZTb+$,Y?T44|V；V+AaY?A3aavAT,43aVf3a2,yNY?4|X0ZTb3null+e4f04+ef,d9678c+4S1+ef,HqcZEZd9sb/1d9c+4+ckY#cSfbTnV34bV3null4+efS9kYc0(2005)87432S(120)535501024121D(20022007)32263996781317nullnullV3V,c+4+e:0l2(+aS,rAME)；Sl1(ZBA,E)；0l1(75,rAME),-c+Z4e,Z4,+re,c+4NB4b,y1+eZEAbV4null4+cZE#SfZESsQrAME6E1V4V,4+cHSs(,ZErAMEb4null+EM1d94.1null川芎薄层鉴别数量统计|0aSaD0lc+4+0ZTvMd9kYfbTnV5bV5null0aSaDa0+kYd9T0ZT+00SD00SD0vp0SD0+0SD0+0a0SD09()30x2215221110100100000030494|?130004000000000000008X5410220001000000000015Y?4|4600110001000000000013431000000000000000008000001000000000000001281460062000100100000409383918849721202001000309910322513134nullnullVV5VA,+kYH,Kv+v0,Qb7+kY4,i+v0S,30x0fK,QXY?4|b4.2null川芎薄层鉴别展开系统条件统计4.2.1null川芎药材的薄层色谱法相关数据统计4dFsd9,45Z7d,-ZYdK(37),Fs1,-nullZY(9&1)K(34)bZ74:FnullZY(9&2),&null-(4&1),o_null&(8&2),F(3060)null-nullZYnullbZ(6&12&5&0.5)b4.2.2null阿魏酸的薄层色谱法相关数据统计4dFsd9,13Z7d,&-bZ-J?d(4),Fs1,&nullbZnullJ?(30&1&3)K(4)bZ74:&null=BnullZ(90&25&4),YnulloJnullJ(10&50&1),J&nullZYnullJ(20&10&1),o_nullZY-J(25&12&1)b4.2.3null大黄酚的薄层色谱法相关数据统计4dFs1d9,3Z7d,sYF(3060)nullJYnullJ(15&5&1),F(3060)nullJYnullJ(14&7&1)F(6090)nullo_nullJ?(10&3&2)b4.2.4null川芎嗪的薄层色谱法相关数据统计+Z7d1,Fnullo_(1&1)b4.2.5null川芎药材和阿魏酸的薄层色谱法相关数据统计4dFs1d9,3Z7d,sY&nullZYnullbZ(18&9&9),Fnullo_nullbZ(6&3&1),&nullbZnullJ?(30&1&3)b4.3null川芎薄层色谱检视条件的情况_jHq,v,；365nm/_j,s,；254nm/_j,_jHq4+1s1bVEM1d9TVA,+kYKS+v0,Z7d-ZY(9&1),_jHq,；365nmb5nulllc+Z444,Q0.d450B；4a54aR44,B9Qg0f；Aa4aa449F,Q04?ZZ_bNVn,+0gW,c+Z44v_?ZZ_b+410ZT30x0,QXY?4|b+1s?s,YV4rs,7?4rsc,9+r,4Aa?4Az0,+1sb30x0=KSaK,9P+!svK,4a434?4,?.d$?7,?3arq0ZTA1b-c+Z4ve?,#Z4,+re,BCc+4NB4b,y1+eZEAb4+cHSs(617LISHIZHENMEDICINEANDMATERIAMEDICARESEARCH2008VOL.19NO.3HSDS02008M193,ZErAMEb+rs,VSscb+c?a3aaapa=s,1=a5=a5=a+aavp2bd9TAU+kYH+0v,+,TbZ7d,-ZYd,Fs1,-nullZY(9&1)KbZ74:FnullZY(9&2),&null-(4&1),o_null&(8&2)bVLlA,-nullZY(9&1)rTzbID:1nullSE0.S0,nullS.:.+s#0ZJ.HSDS0,2006,17(7):1298.3nullRnull,C,null,.+s?sJ.S0,1993,18(9):551.4null),9,S.+?sGC-MSsJ.nD0,2005:49.5null,N,.+?sJ.0,2004,27(8):580.6nullnullb,y,.0+rs0TZJ.S0Y,2006,22(9):1043.7nullnullT,null1.!BSJ.2D0v,2007,23(1):61.8nullnull,BSS,.aRSJ.S0,2006,17(16):1257.9nullnull,.5SJ.0050,2006,17(4):268.10nullnull,P.BRSJ.=D0v,2006,22(2):52.11null,V,；,.mSJ.0,2006,29(3):286.12null7null,:),y.4SJ.SLZ4,2006,12(1):15.13nulldSp,Z,null,.B5SZEJ.null,.,4!#SJ.CD0,2005,34(1):51.16nullnull,null,vc,.RSJ.0,2004,26(1):23.17nullya,3b,E.B4SJ.0,2003,25(7):543.nullS0kYnulll:2007null04null26；null:2007null09null20:广西科学基金资助项目(No.桂科目自0640011)；nullnullnullnull广西大学科研基金资助项目(No.X061106)Te:胡null彦(1966null),男(汉族),云南西畴人,现为云南文山师范高等专科学校副教授,硕士学位,主要从事植物学a植物生理学教学和中草药的研究工作.*YTe:黄荣韶(1964-),男(汉族),广西平南人,现为广西大学副研究员,博士学位,主要从事药用植物资源利用研究及教学工作.s胡null彦1,2,罗永明3,刘大强2,林null兴2,黄荣韶2*(1.=SSn,2null663000；null2.vj,2anull530005；3.j/,2anull530007)K1:用图片的方式介绍中草药鸡骨草和毛鸡骨草在根a茎a叶a种子a荚果等方面的形态学区别,为正确地鉴定这两种植物提供最简单方法,为鸡骨草和毛鸡骨草的开发利用提供依据b1oM:鸡骨草；null毛鸡骨草；null形态学差异ms|:R282.5nullnullDSM:AnullnullcI|:1008null0805(2008)03null0618null02StudyontheMorphologicalDifferencebetweenAburscantoniensisandAbrusrnollisHUYan1,2,LUOYongnullming3,LIUDanullqiang2,LINXing2,HUANGRongnullshao2*(1.DepartmentofBiochemistry,WenshanNormalCollege,Wenshan663000,China；2.AgriculturalCollegeofGuangxiUniversity,Nanning,Guangxi530005,China；3.GuangxiAgriculturalVocationalTechnologicalColnulllege,Nanning,Guangxi,530007,China)Abstract:Usingphotographs,thisarticlemainlyintroducesthemorphologicaldifferencebetweenAburscantoniensisHanceandAbrusrnollisHanceinroots,stems,leaves,seedsandbeanpodetc.Toprovideasimplewaytoidentifythetwoplants,andtoprovideabasisfortheutilizationofthetwotypesofChineseherbalmedicine.Keywords:Aburscantoniensis；nullAbrusrnollis；n