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BRITISH STANDARD BS EN 1096-2:2001 Glass in building Coated glass Part 2: Requirements and test methods for class A, B and S coatings The European Standard EN 1096-2:2001 has the status of a British Standard ICS 81.040.20 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW BS EN 1096-2:2001 This British Standard, having been prepared under the direction of the Sector Committee for Building and Civil Engineering, was published under the authority of the Standards Committee and comes into effect on 15 March 2001 BSI 03-2001 ISBN 0 580 37062 3 National foreword This British Standard is the official English language version of EN 1096-2:2001. The UK participation in its preparation was entrusted by Technical Committee B/520, Glass and glazing in building, to Subcommittee B/520/1, Basic and transformed glass products, which has the responsibility to: A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 26, an inside back cover and a back cover. The BSI copyright date displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 1096-2 January 2001 ICS 81.040.20 English version Glass in building Coated glass Part 2: Requirements and test methods for class A, B and S coatings Verre dans la construction Verre couche Partie 2: Exigences et mthodes dessai pour les couches de classes A, B et S Glas im Bauwesen Beschichtetes Glas Teil 2: Anforderungen an und Prfverfahren fr Beschichtungen der Klassen A, B und S This European Standard was approved by CEN on 24 December 2000. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2001 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 1096-2:2001 E Page 2 EN 1096-2:2001 BSI 03-2001 Contents Page Foreword. 3 1 Scope 3 2 Normative references . 4 3 Terms and definitions. 4 4 Requirements 4 5 Samples and test pieces 6 6 Initial evaluation of test pieces7 7 Duration of the tests. 8 8 Test methods. 8 9 Final evaluation of test pieces.10 10 Test report . 11 Annex A (normative) Special procedures for toughened or heat strengthened coated glass. 13 Annex B (normative) Condensation resistance test. 14 Annex C (normative) Acid resistance test.16 Annex D (normative) Neutral salt spray test .18 Annex E (normative) Abrasion resistance test .20 Annex F (normative) Criteria to demonstrate equivalence of coatings 23 Annex G (informative) Summary of test report .25 Page 3 EN 1096-2:2001 BSI 03-2001 Foreword This European Standard has been prepared by Technical Committee CEN/TC 129, Glass in building, the Secretariat of which is held by IBN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by July 2001, and conflicting national standards shall be withdrawn at the latest by July 2001. This European Standard includes the following parts: Part 1: Definitions and classification Part 2: Requirements and test methods for class A, B and S coatings Part 3: Requirements and test methods for class C and D coatings Part 4: Evaluation of conformity According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. 1 Scope This European Standard specifies requirements and test methods related to artificial weathering and abrasion of coatings on glass for use in buildings. These tests are aimed at evaluating the resistance of the coating to attack by simulated natural weathering conditions as well as to abrasion. This European Standard applies to Class A, B and S coatings, as defined in EN 1096-1. Page 4 EN 1096-2:2001 BSI 03-2001 2 Normative references This European Standard incorporates by dated or undated reference, provisions from other publications. The normative references are cited at the appropriate places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to applies (including amendments). EN 1096-1, Glass in building Coated glass Part 1: Definitions and classification. 3 Terms and definitions For the purposes of this European Standard the following terms and definitions apply: 3.1 coated annealed glass coated glass which has an annealed glass substrate 3.2 toughened or heat strengthened coated glass coated glass which has to be toughened or heat strengthened to meet its final spectrophotometric properties 3.3 coated toughened or heat strengthened glass coated glass which has a toughened or heat strengthened glass substrate 4 Requirements The coated glass complying to this European Standard shall respect the requirements related to the different characteristics given in Table 1. Page 5 EN 1096-2:2001 BSI 03-2001 Table 1 Requirements Requirements CharacteristicsTest Method Visual InspectionSpectrophotometric measurements Condensation resistance Annex B No defect, as defined in EN 1096-1, greater than 3 mm length Maximum one defect between 2 mm and 3 mm length Maximum five defects between 1 mm and 2 mm length In addition, no scratches, staining of the coating or clusters of pinholes greater than 1 mm shall be allowed (see EN 1096-1). When compared with the reference test piece, in both reflection and transmission, there shall be no significant colour change. This observation shall be made within 20 sa. Acid resistanceAnnex CNo requirements Neutral salt spray resistance Annex D No defect, as defined in EN 1096-1, greater than 3 mm length Maximum one defect between 2 mm and 3 mm length Maximum five defects between 1 mm and 2 mm length In addition, no scratches, staining of the coating or clusters of pinholes greater than 1 mm shall be allowed (see EN 1096-1). When compared with the reference test piece, in both reflection and transmission, there shall be no significant colour change. This observation shall be made within 20 sa. The transmittance measured at 550 nm and 900 nm shall differ by no more than 0,03 from the corresponding measured value on the reference test piece. For a glass claimed to have a low emissivity coating the reflectance at 8 ?m shall decrease by no more than 0,02. Abrasion resistance Annex ENo requirement other than to ensure that the abraded area is uniform Total (diffuse plus direct) transmittance measured at 550 nm and 900 nm shall differ by no more than 0,05 from the corresponding value measured for the reference test piece. a The time for observation is fixed to 20 s in order to have a reference period which can influence the visual inspection. Page 6 EN 1096-2:2001 BSI 03-2001 5 Samples and test pieces 5.1 Preparation 5.1.1 Coated annealed glass A sample of 300 mm x 300 mm is needed for each test. For the three chemical durability tests, the test pieces are obtained by cutting the sample as shown in Figure 1. The abrasion test is undertaken on a 300 mm x 300 mm test piece. It is recommended that a spare sample be supplied in the event of one sample not being defect free. Dimensions in millimetres Key 1Test pieces 2Reference test piece for visual inspection 3Reference test piece for spectrophotometric measurement Figure 1 Plan for cutting a sample into test pieces 5.1.2 Toughened or heat strengthened coated glass As the test pieces cannot be cut from test samples, a special procedure has to be employed to obtain the test pieces (see annex A). 5.1.3 Coated toughened or heat strengthened glass Use coated annealed glass samples for testing this type of coated glass. Page 7 EN 1096-2:2001 BSI 03-2001 5.2 Storage The test pieces shall be stored inside a room at a temperature of (23 5)C with a relative humidity less than 80 %. Storage shall prevent dust, chemicals or condensation reacting with the test pieces. The test pieces shall not be stored for more than three months before performing the test. 5.3 Marking The test pieces shall be marked on the uncoated glass surface. The following information shall be marked: manufacturers coating reference test pieces number 1 to 4 code for test Glasses with coating on both surfaces shall be marked without damaging the coating. The two reference test pieces shall be marked as the test pieces plus “ref”. 6 Initial evaluation of test pieces 6.1 Preparation All test pieces shall be cleaned with demineralized water and with a soft tissue. Drying shall also be done with a soft tissue. If necessary this cleaning procedure can be repeated. 6.2 Visual inspection The test pieces shall be subjected to a visual inspection under an artificial sky in accordance with EN 1096-1. The inspection shall take place in both transmission and reflection. The test pieces shall be observed at a distance of 600 mm. All test pieces shall be defect free. No scratches or pinholes shall be observed. If a test piece contains defects it shall be replaced. NOTE The replacement of test pieces is to avoid any misinterpretation of the testing results. 6.3 Spectrophotometric measurements 6.3.1 Coated annealed glass A measurement sample shall be cut from the centre of the reference test piece. The actual size shall be dependent on the type of equipment being used for the measurements. The transmittance of the measurement sample shall be measured with radiation of normal incidence at the following wavelengths: 550 nm (representative wavelength for light and solar transmittance); 900 nm (representative wavelength for solar transmittance). For glass claiming to have a low emissivity coating a measurement of the reflectance shall be made at 8 ?m using radiation of nearly normal incidence. 6.3.2 Toughened or heat strengthened coated glass As the measurement sample cannot be cut from the reference test piece, a special procedure has to be employed to make the measurement (see annex A). Page 8 EN 1096-2:2001 BSI 03-2001 7 Duration of the tests The durations of the tests are set out in Table 2. Table 2 Duration of the tests Test duration for classTest ABS Condensation resistance Acid resistance Neutral salt spraya Abrasion resistance 21 days 5 cycles 21 days 500 strokes 4 days 1 cycle 10 days 50 strokes 14 days 5 cycles a 500 strokes a The neutral salt spray test is excluded for Class S coatings as they are subject to frequent cleaning in the applications for which they are used in accordance with EN 1096-1. 8 Test methods 8.1 General The coated glass complying to this part of the European Standard shall pass the tests given in annexes B, C, D and E which are designed to verify the chemical and mechanical characteristics of the coating. The tests are as follows: condensation resistance test (see annex B) acid resistance test (see annex C) neutral salt spray test (see annex D) abrasion resistance test (see annex E) Annex F gives criteria to demonstrate equivalence of coatings, i.e. an indications of whether or not the coated glass needs to be tested. These tests are evaluated by their effect on the visual quality of the product and its spectrophotometric properties. Whilst it would be feasible to evaluate the spectrophotometric properties across the entire spectrum a number of representative wavelengths have been picked. These wavelengths represent transmission of light and energy, together with reflectance relating to emissivity. Page 9 EN 1096-2:2001 BSI 03-2001 Each test shall be carried out without interruption. The only exception is the acid resistance test which can be interrupted after each cycle. However, any interruption shall not exceed three days. Testing shall start as soon as possible after the test pieces have been cleaned. The exception is the abrasion resistance test where testing shall commence within 30 min of the test piece being cleaned. Care shall be taken to ensure the test pieces are clean and uncontaminated. 8.2 Positioning of test pieces in the test cabinets The test pieces shall have their coated side oriented upwards, the pieces presenting an angle of (15 5) with the vertical, and the coated side shall face away from the door. For consistent results, a certain quantity of glass shall be present. For 300 l cabinet the total weight of the glasses shall be (7,5 0,5) kg. An insufficient quantity of coated glass shall be compensated with uncoated clear glasses. In the centre of the test pieces a piece of 6 mm clear glass is placed, with the reference thermocouple attached (see Figure 2). The following spacing shall be maintained: distance from the wallsnot less than 100 mm distance between bottom of the test pieces and waternot less than 200 mm spacing between adjoining test piecesnot less than 20 mm not more than 40 mm Where there is an insufficient quantity of coated glass for testing, it is required to use uncoated clear glasses to fill up a cabinet. Page 10 EN 1096-2:2001 BSI 03-2001 Dimensions in millimetres Key 1Position of the thermocouple 2Substrate holder 36 mm clear glass used for temperature control inside cabinet Figure 2 Description of the reference thermocouple position 9 Final evaluation of test pieces 9.1 General Test pieces having completed the specified length of time under the test conditions, for the appropriate class, shall be cleaned and if necessary have their surfaces polished before undergoing final evaluation. Dependent on the class, evaluation shall consist of visual inspection and measurement of spectrophotometric properties. 9.2 Cleaning All test pieces shall be cleaned with demineralized water and with a soft tissue. Drying shall also be done with a soft tissue. If necessary this cleaning procedure can be repeated. The non-coated surface of the glass might have been damaged during the tests. If this deterioration would affect the evaluation of the degradation of the coated surface it is permissible to polish the non coated surface. The polishing can be undertaken using fine abrasive powder e.g. cerium oxide and/or alumina. Care shall be taken to ensure that the polishing compound does not contaminate the coated surface. Coated glasses with coatings on both surfaces, shall not be polished. Page 11 EN 1096-2:2001 BSI 03-2001 9.3 Visual Inspection The test pieces to be examined shall be subjected to a visual inspection under an artificial sky according to EN 1096-1. The examination shall be in both transmission and reflection. Inspection of the test samples shall be from a distance of 600 mm. A band 15 mm wide around the edge of the pieces shall be excluded from the inspection. All defects shall be noted. The requirements for the acceptance of the coated glass related to the different classes are given in Table 1. 9.4 Spectrophotometric measurements 9.4.1 Coated annealed glass The four test pieces which have been subjected to each chemical durability test (condensation resistance test, acid resistance test, neutral salt spray test) shall be cut so that measurement samples are obtained for the spectrophotometric measurements. The actual size of the measurement sample shall be dependent on the equipment being used for the measurement. The measurement samples shall be cut from the centre of the test piece. The test piece which has been subjected to the abrasion resistance test shall be cut so that measurement samples can be obtained for spectrophotometric measurement. The actual size of the measurement samples shall be dependent on the equipment being used for the measurement. The pattern of the cutting of measurement samples is shown in Figure E.2. The transmittanc
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