对牛的抽样计划范文.doc

对牛的抽样计划范文 Table1表1Sampling Programmefor Cattle对牛的抽样计划Compound分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limit MRL Methods(g/kg)(g/kg)二苯乙烯类Stibenes ELISA己烯雌酚Diethylstilbestrol RIA己二烯雌酚Dienoestrol LC/MS-MS己烷雌酚Hexoestrol牛肝1不得检出ND类固醇类Steroids19-去甲睾酮19-Nortestosterone氢化泼尼松（强地松龙）Prednisolone Estradiol雌二醇1不得检出ND甲基氢化泼尼松prednisolone牛肝ELISA GC/MS1不得检出ND二羟基苯甲酸内酯类Resorcylic acidlactones玉米赤酶醇Zeranol牛肝ELISA LC/MS/MS0.5不得检出ND呋喃唑酮Furazolidone呋喃西林Nitrofurazone呋喃它酮Furaltadone牛肝LC/MS/MS0.5不得检出ND呋喃妥因Nitrofurantoin ELISA RIA GC/MS LC/MS/MS氯霉素Chloramphenicol牛肉0.3不得检出ND-受体激动剂Beta-agonists ELISA不得检出克伦特罗Clenbuterol GC/MS0.5ND LC/MS/MS沙丁胺醇Salbutamol牛肝0.5化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limit MRL Methods(g/kg)(g/kg)邻氯青霉素Cloxacillin CHARMII100300双氯青霉素Dicloxacillin LC/MS/MS100300苄青霉素Benzyl penicillin5050萘Nafcillin夫西林牛肝55(JAP)抗生素类Antibiotics1.四环素Tetracycline503002.土霉素Oxytetracycline503003.金霉素Chlortetracycline503004.强力霉素Doxycycline牛肝HPLC50300链霉素Streptomycin牛肝HPLC10500甲砜霉素Thiamphenicol0.520(JAP)氟苯尼考florfenicol牛肝GC/MS5200(JAP)恩诺沙星Enrofloxacin HPLC300环丙沙星Ciprofloxacin LC/MS/MS300丹诺沙星Danofloxacin400氟甲喹Flumequine500麻Marbofloxacin保沙星牛肝xx0(EU)驱虫剂Anthelmintics牛肝1.苯亚砜咪唑Oxfendazole HPLC105002.苯硫达唑Fenbendazole LC/MS/MS105003.丙硫达唑Albendazole1010004氧化丙硫咪唑Albendazole Oxide101000(EU)5氟苯哒唑Flubendazole1010(JAP)6甲苯咪唑Mebendazole1020(JAP)化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limit MRL Methods(g/kg)(g/kg)磺胺类Sulphonamides1.磺胺嘧啶Sulfadiazine501002.磺胺-5-甲氧嘧啶Sulfamethoxydiazine501003.磺胺二甲嘧啶Sulfadimidine501004.磺胺喹恶啉Sulfaquinoxaline501005磺胺二甲氧嘧啶Sulfadimoxinum501006磺胺间甲氧嘧啶Sulfamonomethoxine501007磺胺甲氧嗪Sulfamethoxypyridazine501008磺胺甲Sulfamethoxazole恶唑501009磺胺氯哒嗪Sulfachlorpyridazine50100(JAP)10磺胺胍Sulfaguanidine50100(JAP)11磺胺甲氧哒嗪Sulfamethoxypyridazine牛肝HPLC50未制定不得检出卡巴氧Carbadox牛肝GC/MS1ND有机氯OCS牛脂GC1.六六六BHC GC/MS53002.滴滴涕DDT1010003.六氯苯Hexachlorobenzene肪5200拟除虫菊酯类Pyrethoids牛肝GC溴氰菊酯Deltamethrin HPLC1010氯氰菊酯Cypermethrin50200化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)有机磷OPS1皮蝇磷Fenchlorphosxx0002毒死蜱Chlorpyrofos1020003敌百虫Trichlorfon10504蝇毒磷Coumaphosxx005马拉硫磷Malathion牛肝GC108000化学元素Chemical elements铅Lead5500镉Cadmiam AAS51000砷牛肾ICP-MS101000Arsenic汞Mercury51000HPLC左旋咪唑Levamisole牛肝GC-NPD10100HPLC阿维菌素Avermectin牛肝LC/MS/MS220伊维菌素Ivermectin牛肝HPLC10100Table2表2Sampling Programmefor Sheep对羊的抽样计划化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)己烯雌酚Diethylstilbestrol ELISA己二烯雌酚Dienoestrol RIA己烷雌酚Hexoestrol羊肝LC/MS/MS1不得检出ND呋喃唑酮Furazolidone呋喃西林Nitrofurazone呋喃它酮Furaltadone呋喃妥因Nitrofurantoin羊肝LC/MS/MS0.5不得检出ND ELISAGC/MS氯霉素Chloramphenicol羊肉LC/MS/MS0.3不得检出ND邻氯青霉素Cloxacillin CHARMII100300双氯青霉素Dicloxacillin HPLC100300萘夫西林Nafcillin羊肝LC/MS/MS100300(JAP)抗生素类药Antibacterial四环素Tetracycline50300土霉素Oxytetracycline50300金霉素Chlortetracycline羊肝HPLC50300驱虫剂Anthelmintics羊肝1.苯亚砜咪唑Oxfendazole105002.苯硫达唑Fenbendazole HPLC105003.丙硫达唑Albendazole LC/MS/MS1010004氧化丙硫咪唑Albendazole Oxide101000(EU)5氟Flubendazole苯哒唑1010(JAP)6甲Mebendazole苯咪唑10200(JAP)磺胺类Sulphonamides1.磺胺嘧啶Sulfadiazine羊肝HPLC501002.磺胺二甲嘧啶Sulfadimidine501003.磺胺喹恶啉Sulfaquinoxaline501004.磺胺二甲氧嘧啶Sulfadimoxinum501005磺胺间甲氧嘧啶Sulfamonomethoxine501006磺胺甲氧嗪Sulfamethoxypyridazine501007磺胺甲Sulfamethoxazole恶唑501008磺胺氯哒嗪Sulfachlorpyridazine50未制定9磺胺胍Sulfaguanidine5010010磺胺甲氧哒嗪Sulfamethoxypyridazine50未制定HPLC GC-NPD左Levamisole旋咪唑羊肝10100Table3表3Sampling Programmefor Pig对猪的抽样计划化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)己烯雌酚Diethylstilbestrol ELISA不得检出己二烯雌酚Dienoestrol RIA1ND己烷雌酚Hexoestrol猪肝LC/MS/MS抗生素类药Antibacterial四环素Tetracycline50300土霉素Oxytetracycline50300金霉素Chlortetracycline50300强力霉素Doxycyclines猪肝HPLC5050ELISA不得检出GC/MS0.3ND氯霉素Chloramphenicol猪肉LC/MS/MS化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)邻氯青霉素Cloxacillin100300双氯青霉素Dicloxacillin CHARMII100300苄青霉素Benzyl penicillinHPLC5050萘夫西林Nafcillin猪肝LC/MS/MS55(JAP)不得检出卡巴氧Carbadox猪肝GC/MS1ND伊维菌素Ivermectin猪肝HPLC10100化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratory Detection limitMRL Methods(g/kg)(g/kg)甲砜霉素Thiamphenicol猪肝GC/MS0.520-受体受激动剂-agonists猪肝0.5不得检出ND1.克伦特罗Clenbuterol ELISA2.沙丁胺醇Salbutamol GC/MS莱克多巴胺Ractopamine LC/MS/MS0.5不得检出ND HPLC GC-NPD10左旋咪唑Levamisole猪肝100化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)磺胺类Sulphonamides1磺胺嘧啶Sulfadiazine501002磺胺二甲嘧啶Sulfadimidine501003磺胺喹恶啉Sulfaquinoxaline501004磺胺二甲氧嘧啶Sulfadimoxinum501005磺胺间甲氧嘧啶Sulfamonomethoxine猪肝HPLC50100磺胺甲氧嗪Sulfamethoxypyridazine501007磺胺甲恶唑Sulfamethoxazole501008磺Sulfachlorpyridazine胺氯哒嗪5050(JAP)9磺胺胍Sulfaguanidine50100(JAP)10磺胺甲氧哒嗪Sulfamethoxypyridazine5050(JAP)硝基呋喃类呋喃唑酮Furazolidone呋喃西林Nitrofurazone呋喃它酮Furaltadone呋喃妥因Nitrofurantoin猪肝LC/MS/MS0.5不得检出ND驱虫剂Anthelmintics1.苯亚砜咪唑Oxfendazole LC/MS/MS105002.苯硫达唑Fenbendazole HPLC105003.丙硫达唑Albendazole1010004氧化Albendazole Oxide丙硫咪唑101000(EU)5氟苯哒唑Flubendazole1010(JAP)6甲苯咪唑Mebendazole猪肝1020(JAP)化学元素Chemical elements铅Lead5500镉Cadmiam AAS51000砷Arsenic ICP-MS101000汞Mercury猪肾51000Table4表4Sampling Programmefor Poultry对禽的抽样计划化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)ELISA己烯雌酚Diethylstilbestrol RIA己二烯雌酚Dienoestrol LC/MS/MS己烷雌酚Hexoestrol鸡肝1不得检出ND甲巯咪唑Tapazole硫脲嘧啶Thiouracil鸡肝HPLC100不得检出ND19-去甲睾酮19-Nortestosteron鸡肝ELISA1不得检出ND氢化泼尼松（强地松龙）Prednisolone GC-MS雌二醇Estradiol甲基氢化泼尼松prednisolone1不得检出ND玉米赤霉醇Zeranol鸡肝ELISA LC/MS/MS0.5不得检出ND硝基咪唑类GC-NPD GC/MS二甲硝咪唑Dimetridazole LC/MS/MS甲硝哒唑Metronidazole洛硝哒唑Ronidazole鸡肾5不得检出ND化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)硝基呋喃类呋喃唑酮Furazolidone呋喃西林Nitrofurazone呋喃它酮Furaltadone呋喃妥因Nitrofurantoin鸡肝LC/MS/MS0.5不得检出ND甲砜霉素Thiamphenicol0.550氟苯尼考florfenicol鸡肝GC/MS52500(EU)卡巴氧Carbadox鸡肝GC/MS1不得检出ND邻氯青霉素Cloxacillin CHARMII100300双氯青霉素Dicloxacillin HPLC100300苄青霉素Benzyl penicillinLC/MS/MS5050萘夫西林Nafcillin鸡肝55(JAP)新霉素Neomyin鸡肝HPLC CHARMII100500螺旋霉素Spiramycin鸡肝HPLC CHARMIIxx00化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)四环素Tetracycline50300土霉素Oxytetracycline50300金霉素Chlortetracycline50300强力霉素Doxycyclines鸡肝HPLC5050链霉素Streptomycin鸡肝HPLC1010驱虫剂Anthelmintics1氟Flubendazole苯哒唑LC/MS/MS10400(EU)2甲Mebendazole苯咪唑鸡肝HPLC1020(JAP)磺胺类鸡肝HPLC1磺胺嘧啶Sulfadiazine501002磺胺间甲氧嘧啶Sulfameter501003磺胺二甲嘧啶Sulfadimidine501004磺胺喹恶啉Sulfaquinoxaline501005磺胺二甲氧嘧啶Sulfadimoxinum501006磺胺甲氧嗪Sulfamethoxypyridazine501007磺胺甲恶唑Sulfamethoxazole501008磺Sulfachlorpyridazine胺氯哒嗪50未制定9磺胺胍Sulfaguanidine50未制定10磺胺甲氧哒嗪Sulfamethoxypyridazine50未制定化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)HPLC GC5氯羟吡啶Clopidol鸡肝GC/MS10HPLC盐霉素Salinomycin鸡肝LC/MS/MS20500莫能菌素Monensin鸡肝HPLC50500恩诺沙星Enrofloxacin10环丙沙星Ciprofloxacin10丹诺沙星Danofloxacin10400沙拉沙星Sarafloxacin80氟甲喹Flumequine鸡肝HPLC800马杜霉素Maduramicin鸡肝800左旋咪唑Levamisole鸡肝HPLC GC-NPD10100HPLC阿维菌素Avermectin鸡肝LC/MS/MS220化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratory Detection limitMRL Methods(g/kg)(g/kg)尼卡巴嗪Nicarbazin鸡肾50200HPLC505005050氨基甲酸酯类(Carbamates)50500甲萘威Carbaryl杀线威Oxamyl异丙威Isoprocarb克百威Carbofuran鸡肾GC HPLC5050拟除虫菊酯类Pyrethriods溴氰菊酯Deltamethrin5050氯氰菊酯Cypermethrin鸡肾GC HPLC5050HPLC对乙酰氨基酚Paracetamol阿司匹林Aspirin鸡肝LC/MS/MS50未制定多氯联苯PCBs鸡脂肪GC-HRMS0.1ppt2pg WHO-PCDD/F-TEQ/g有机氯农药OCS1.六六六BHC53002.滴滴涕DDT1010003.六氯苯HCB鸡脂肪GC GC/MS5200化学元素Chemical elements铅Lead5500镉Cadmium鸡肝AAS ICP/MS5500汞Mercury51000砷Arsenic101000化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratory Detection limit MRLMethods(g/kg)(g/kg)己烯雌酚Diethylstilbestrol ELISA己二烯雌酚Dienoestrol RIA己烷雌酚Hexoestrol鸭肝LC-MS-MS1不得检出NDELISA、GC-MS氯霉素Chloramphenicol鸭肉HPLC-MS0.3ND硝基呋喃类呋喃唑酮Furazolidone呋喃西林Nitrofurazone呋喃它酮Furaltadone呋喃妥因Nitrofurantoin鸭肝HPLC/MS/MS0.5不得检出ND化学元素Chemical elementsAAS铅Lead ICP/MS5500镉Cadmium5500汞Mercury鸭肾51000砷Arsenic101000Table5表5Sampling Programmefor Egg对蛋类的抽样计划化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetectionlimitMRLMethods(g/kg)(g/kg)氯霉素Chloramphenicol蛋ELISARIAGC-MS HPLC-MS0.3不得检出ND呋喃唑酮Furazolidone呋喃西林Nitrofurazone呋喃它酮Furaltadone呋喃妥因Nitrofurantoin蛋HPLC/MS/MS0.5不得检出ND抗生素类药Antibiotics四环素Tetracycline50200土霉素Oxytetracycline50200金霉素Chlortetracycline蛋HPLC50200化学元素Chemical elements铅Lead蛋AAS ICP/MS5500镉Cadmium5500汞Mercury51000砷Arsenic101000Table6表6Sampling Programmefor Rabbit对兔的抽样计划化合物Substance实验方法检测限最高残留限量LaboratoryDetection limitMRL分析材料Matrix Methods(g/kg)(g/kg)己烯雌酚Diethylstilbestrol ELISA己二烯雌酚Dienoestrol RIA己烷雌酚Hexoestrol兔肝LC/MS-MS1不得检出ND甲状腺拮抗剂Thyrostats甲巯咪唑Tapazole硫脲嘧啶Thiouracil兔肝HPLC100不得检出类固醇类Steroids19-去甲睾酮19-Nortestosterone氢化泼尼松（强地松龙）Prednisolone雌二醇Estradiol兔肝ELISA LC/MS-MS1不得检出ND甲基氢化泼尼松prednisolone1不得检出ND二羟基苯甲酸内酯类Resorcylic acidlactones玉米赤酶醇Zeranol兔肝ELISA LC/MS-MS0.5不得检出ND硝基呋喃类Nitrofurans呋喃唑酮Furazolidone呋喃西林Nitrofurazone呋喃它酮Furaltadone呋喃妥因Nitrofurantoin兔肝HPLC/MS0.5不得检出ND GC/MS LC/MS/MS不得检出氯霉素Chloramphenicol兔肉ELISA0.3ND甲砜霉素Thiamphenicol0.5未制定氟苯尼考florfenicol兔肉HPLC0.52000(EU)恩诺沙星Enrofloxacin200环丙沙星Ciprofloxacin200丹诺沙星Danofloxacin200氟甲喹Flumequine兔肝HPLC10500硝基咪唑类兔GC-NPD5不得检出二甲硝咪唑Dimetridazole GC-MS ND甲硝哒唑Metronidazole LC/MS/MS洛硝哒唑Ronidazole肾四环素Tetracycline50300土霉素Oxytetracycline50300金霉素Chlortetracycline兔肝HPLC50300磺胺类磺胺嘧啶Sulfadiazine磺胺甲氧嘧啶Sulfameter磺胺二甲嘧啶Sulfadimidine磺胺喹恶啉Sulfaquinoxaline兔肝HPLC50100拟除虫菊酯类Pyrethriods GC溴氰菊酯Deltamethrin HPLC10未制定氯氰菊酯Cypermethrin兔肝2020HPLC对乙酰氨基酚Paracetamol阿司匹林Aspirin兔肝LC/MS/MS50未制定有机氯农药OCPS GC六六六BHC GC-MS5300滴滴涕DDT101000六氯苯HCB脂肪5200化学元素Chemical elements铅Lead5500镉Cadmium AAS51000汞Mercury ICP/MS51000砷Arsenic兔肾101000Table7表7Sampling Programmefor Fish对鱼类的抽样计划化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)己Diethylstilbestrol烯雌酚ELISA己二烯雌酚Dienoestrol RIA1不得检出己Hexoestrol烷雌酚鳗鱼LC/MS-MS ND19-去甲睾酮19-Nortestosteron ELISA雌二醇鱼GC-MS1不得检出Estradiol鱼GC/MS LC/MS/MS不得检出氯Chloramphenicol霉素鳗鱼RIA0.3ND呋喃唑酮Furazolidone不得检出呋Nitrofurazone喃西林ND呋喃它酮Furaltadone呋Nitrofurantoin喃妥因鱼、鳗鱼LC/MS/MS0.5四环素Tetracycline土霉素Oxytetracycline50100金霉素Chlortetracycline鱼HPLC恩诺沙星Enrofloxacin100环丙沙星Ciprofloxacin100诺氟沙星Norfloxacin10氧氟沙星Ofloxacin鳗鱼HPLC10100磺胺类Sulphonamides1磺胺嘧啶Sulfadiazine10102磺胺二甲嘧啶Sulfadimidine10103磺胺喹恶啉Sulfaquinoxaline10104磺胺二甲氧嘧啶Sulfadimoxinum鳗鱼HPLC101005磺胺间甲氧嘧啶Sulfamonomethoxine10106磺胺甲氧嗪Sulfamethoxypyridazine10107磺胺甲恶唑Sulfamethoxazole10108磺Sulfachlorpyridazine胺氯哒嗪10未制定9磺胺胍Sulfaguanidine10未制定10磺胺甲氧哒嗪Sulfamethoxypyridazine10未制定HPLC左旋咪唑Levamisole鱼GC-NPD10未制定伊维菌素Ivermectin鱼HPLC2未制定HPLC恶喹酸Oxolinic acid鳗鱼LC/MS/MS1050GC-HRMS多氯联苯PCBs鱼0.1ppt4pg WHO-PCDD/F-TEQ/g化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)化学元素Chemical elements铅Lead5200镉Cadmium AAS550汞Mercury鱼、鳗鱼ICP/MS5500砷Arsenic101000多氯联苯PCBs鳗鱼GC-HRMS0.1ppt4pg WHO-PCDD/F-TEQ/g ELISA不得检出B3d.真菌毒素Mycotoxins HPLC0.5ND黄B1B2G1G2曲霉毒素AflaToxin B1B2G1G2鱼B3e.染料类Dyes孔雀石绿Malachite green2（孔雀石绿和隐性孔雀石绿之和）结晶紫Crystal Violet鳗鱼LC/MS/MS2（结晶紫和隐性结晶紫之和）不得检出ND化学法未制定甲醛Formaldehyde鱼1,000化学法未制定二氧化硫Sulfurdioxide鱼1,000Table8表8Sampling Programmefor Crustacea对甲壳类的抽样计划化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)硝基呋喃类养殖虾呋Furazolidone喃唑酮Cultured Shrimp0.5不得检出呋Nitrofurazone喃西林ND呋Furaltadone喃它酮呋Nitrofurantoin喃妥因LC/MS/MSELISA不得检出GC/MS ND LC/MS/MS氯Chloramphenicol霉素养殖虾Cultured Shrimp0.1己Diethylstilbestrol养殖虾烯雌酚ELISA己二烯雌酚Dienoestrol Cultured Shrimp RIA1不得检出己Hexoestrol烷雌酚LC/MS/MS ND四Tetracycline环素养殖虾50100土Oxytetracycline霉素Cultured Shrimp50100金Chlortetracycline霉素HPLC50100恩Enrofloxacin诺沙星养殖虾不得检出ND环Ciprofloxacin丙沙星Cultured Shrimp不得检出ND诺Norfloxacin氟沙星未制定氧Ofloxacin氟沙星HPLC20未制定19-去甲睾酮19-Nortestosteron养殖虾ELISA不得检出Estradiol雌二醇Cultured Shrimp GC/MS1NDLC/MS/MS磺胺类Sulphonamides1磺Sulfadiazine胺嘧啶养殖虾202磺胺二甲嘧啶Sulfadimidine Cultured Shrimp203磺Sulfaquinoxaline胺喹恶啉204磺胺二甲氧嘧啶Sulfadimoxinum205磺胺间甲氧嘧啶HPLC100Sulfamonomethoxine206Sulfamethoxypyridazine磺胺甲氧嗪207磺胺甲恶唑Sulfamethoxazole208磺Sulfachlorpyridazine胺氯哒嗪20未制定9磺胺胍Sulfaguanidine20未制定10磺胺甲氧哒嗪Sulfamethoxypyridazine20未制定苯Benzimidazoles并咪唑类养殖虾苯Oxfendazole亚砜咪唑Cultured ShrimpHPLC苯硫达唑Fenbedazole LC/MS/MS20未制定丙硫达唑Albendazole噻Cambendazole苯咪唑酯养殖虾HPLC Cultured Shrimp GC-NPD左旋咪唑Levamisole10未制定养殖虾Cultured Shrimp伊维菌素Ivermectin HPLC2未制定养殖虾HPLC,Cultured ShrimpLC/MS/MS恶喹酸Oxolinic acid10100化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)B3e.染料类Dyes养殖虾不得检出孔Malachite green雀石绿Cultured Shrimp2（孔雀石绿与隐性孔雀石绿之和）ND结晶紫Crystal VioletLC/MS/MS2（结晶紫和隐性结晶紫之和）养殖虾Cultured Shrimp化学法未制定甲Formaldehyde醛1000养殖虾CulturedShrimp化学法未制定二Sulfurdioxide氧化硫1000B3d.真菌毒素Mycotoxins养殖虾ELISA不得检出黄曲B1B2G1G2霉毒素CulturedShrimpHPLC0.5ND AflaToxinB1B2G1G2化Chemical elements养殖虾AAS学元素铅Lead CulturedShrimp ICP-MS5500镉Cadmium5500砷Arsenic101000汞Mercury5500有机氯OCS养殖虾GC1.六六六BHC CulturedShrimpGC/MS53002.滴滴涕DDT1010003.六氯苯Hexachlorobenzene5200养殖虾CulturedShrimp多氯联苯PCBs GC-HRMS0.1ppt4pg WHO-PCDD/F-TEQ/g化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)非养殖虾不得检出硝基呋喃类Other ShrimpLC/MS/MS0.5ND呋Furazolidone喃唑酮呋Nitrofurazone喃西林呋喃它酮Furaltadone呋Nitrofurantoin喃妥因非养殖虾GC/MS不得检出Other ShrimpLC/MS/MSND ELISA氯Chloramphenicol霉素0.3化学元素Chemical elements非养殖虾AAS铅Lead Other Shrimp ICP-MS5500镉Cadmium5500砷Arsenic101000汞Mercury5500非养殖虾有机氯OCS OtherShrimp1.六六六BHC53002.滴滴涕DDT1010003.六氯苯Hexachlorobenzene GCGC-MS5200非养殖虾OtherShrimp多氯联苯PCBs GC-HRMS0.1ppt4pg WHO-PCDD/F-TEQ/g化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)甲壳类GC/MS不得检出(小龙虾等)LC/MS/MSND氯Chloramphenicol霉素ELISA0.3化学元素Chemical elements甲壳类铅Lead(小龙虾等)5500镉Cadmium5500砷Arsenic101000汞Mercury AASICP-MS5500有机氯OCS甲壳类GC 1、六六六BHC(小龙虾等)GC-MS 53002、滴滴涕DDT1010003.六氯苯Hexachlorobenzene5200甲壳类(小龙虾等)多氯联苯PCBs GC-HRMS0.1ppt4pg WHO-PCDD/F-TEQ/g硝基呋喃类甲壳类呋Furazolidone喃唑酮(小龙虾等)呋Nitrofurazone喃西林呋喃它酮Furaltadone呋Nitrofurantoin喃妥因LC/MS/MS0.5不ND得检出Table9表9Sampling Programmefor Casing对肠衣的抽样计划化合物分析材料Substance Matrix有机氯OCS猪肠衣 1、六六六BHC 2、滴滴涕DDT3.六氯苯Hexachlorobenzene化学元素Chemical elements猪肠衣铅Lead镉Cadmiam砷Arsenic汞Mercury氯Chloramphenicol1霉素猪肠衣硝基呋喃类猪肠衣呋Furazolidone喃唑酮呋Nitrofurazone喃西林呋喃它酮Furaltadone呋Nitrofurantoin喃妥因硝基呋喃类羊肠衣呋Furazolidone喃唑酮呋Nitrofurazone喃西林呋喃它酮Furaltadone呋Nitrofurantoin喃妥因化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)化学元素Chemical elementsAAS铅Lead ICP-MS5500镉Cadmiam5500砷Arsenic101000汞Mercury羊肠衣51000GC-MS不得检出氯Chloramphenicol霉素羊肠衣ELISA0.3ND Table10表10Sampling Programmefor Royaljelly蜂王浆的抽样计划化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRL Methods(g/kg)(g/kg)氯霉素Chloramphenicol蜂王浆LC/MS/MS0.3不得检出ND硝基咪唑类甲硝哒唑Metronidazole蜂王浆HPLCGC/MS10不得检出ND硝基呋喃类不得检出呋喃唑酮Furazolidone0.5ND呋喃西林Nitrofurazone呋喃它酮Furaltadone呋喃妥因Nitrofurantoin蜂王浆LC/MS/MS化合物分析材料实验方法检测限最高残留限量Substance MatrixLaboratoryDetection limitMRLMethods(g/kg)(g/kg)磺胺类Sulphonamides HPLC磺胺嘧啶Sulfadiazine蜂王浆LC/MS/MS10未制定磺胺噻唑sulfath