高分子实验报告.doc

1. 1. 1. 2. 250ml 250ml 250ml am am am nps nps 1. 10g80ml 80ml0.10.2g 0.10.2g 2. 10g 10g 80ml 0.10.2g 20ml 20ml 20ml 35 3. 35 35 4. 70, 6. 70 ,23 70 2 3 7. 8 2. - 1 2- 3 250ml 250ml 250ml am aa am aa am aa nps nps 1. 8g2ml 2ml80ml 80ml 2. 8g 8g 2ml 80ml 1.1gnaoh 1.1gnaoh 1.1gnaoh3550 50 3. 35 35 50 0.5g 0.3g 50ml10ml 4. 0.5g 0.3g 50ml 0.5g 0.3g 50ml 10ml 5. 5. 12 12 12 ph45 45ph ph89 89 6. ph ph 45 ph 89 7 3. 1. 1. 2. 2. 3. 3. am ampam pam am pam () ( ) pam pam pam 123% 3% 1. 12 12 3% 250ml 2. 1g pam 1g pam250ml 250ml 100ml 100ml 100ml 3. 3. 4.3% 23 4. 3% 2 3 5.100ml 100ml 5. 100ml 34 3 4 6. 6. 24 24 24 p ps s sw1 sw1 w24. 4.: : 1. 1. 2. 2. : : 250ml 250ml 250ml pam pam pam 8%100ml( 100ml( 1. 1258% 1 2 5 8% 100ml( ) ) 2. 1mol/l 1mol/lph ph3 1mol/l ph 3 15ml60 602 3. 15ml 15ml 60 2 4 5. 5. 1. 1. 2. 2. pam pam pam hpam hpam hpam hd degreeofhydrolysis ofhydrolysis pam 5%naoh pam 5%naoh pam 0.1mol/l hcl 0.1mol/l hcl 0.81g 100ml 100ml 1. 0.81g 100ml 0.81g ) ) 20ml 2. 20ml 20ml 5% 5%10ml 10ml 5% 10ml 3.80 802 3. 80 2 4.250ml 250ml 4. 250ml 5.250ml 250ml250ml 250ml 5. 250ml 250ml 0.1mol/l 0.1mol/l 0.1mol/l 0.1mol/l 0.1mol/l 0.1mol/l 6. 6. 7. 7.6. 6. 1. 1.2. 2. 3. 3. 25ml mma bpo mma bpo mma bpo 25ml15ml 15ml 1. 25ml 25ml 15ml 0.2g 20.2g 0.2g 3.80 80 3. 80 4.50 50 4. 50 1002-3 100 2 5. 5.7. 7.: : 1. 1. 2. 2. 3. 3. m m 0.57mm 0.57mm 0.10.4%25ml () 25ml( 1. 0.10.4% 0.10.4% 25ml ) 2. 3.30 0.1 300.1 20cm 3. 30 0.1bc20cm b c 20cm d d 4.a10ml 10ml10min 10minc 4. a 10ml 10min c bbd b b d cba c b a b b 0.2 0.2c1 0.2 c t1 5.5ml 5mlaac 5. 5ml a a cbd10min 4c2 2/3 c1 b d 10min 4 c t2 t 6.5ml 10ml 10ml 5ml10ml 10ml 6. 5ml 10ml10ml 1/2 1/3 1/4 1/21/3 1/4t3t4t5 1/2 1/31/4 t t t 7. 7. 1020ml 20ml 10min 10 20ml 10min t0 sp/c lnr /cc sp/ ln c =0 =0a a = a / c0 a pam pam30 30k