环己烷一步氧化法制己二酸年产5万吨设备规范表

1、环己烷绿色催化氧化法生产己二酸反应器设计说明书项目名称环己烷一步氧化法制己二酸设备规范表.第一张流程图各主要设备第一张流程图各主要设备设备位号设备名称技术规格标准号材料数量备注R101a第一氧化反应釜1700X 5400X20GB9845-19881Cr18Ni9Ti1R101b第二氧化反应釜1700X 5400X20GB9845-19881Cr18Ni9Ti1R101c第三氧化反应釜1700X 5400X20GB9845-19881Cr18Ni9Ti1R101d第四氧化反应釜1700X 5400X20GB9845-19881Cr18Ni9Ti1R101e第五氧化反应釜1700X 5400X2

2、0GB9845-19881Cr18Ni9Ti1R102皂化釜1300X 4320GB9845-1988A3F1P101a环己烷原料泵IH80-50-315GB/T 5656-941附表1P101b环己烷原料泵IH80-50-315GB/T 5656-941P102a环己烷进料泵IH65-40-250GB/T 5656-941P102b环己烷进料泵IH65-40-250GB/T 5656-941P103a三酸输送泵IH200-150-250GB/T 5656-941P103b三酸输送泵IH200-150-250GB/T 5656-941P104a去皂化输送泵IH65-40-250GB/T 565

3、6-941P104b去皂化输送泵IH65-40-250GB/T 5656-941P105aT101回流泵IH200-150-250GB/T 5656-944P105bT101回流泵IH200-150-250GB/T 5656-944P106aT102回流泵MPH3-30GB/T 5656-941P106bT102回流泵MPH3-30GB/T 5656-941P107a环己醇输送泵MPH1.5-50CGB/T 5656-941P107b环己醇输送泵MPH1.5-50CGB/T 5656-941P108a环己酮输送泵MPH1.5-50CGB/T 5656-941P108b环己酮输送泵MPH1.5-

4、50CGB/T 5656-941E101进料预热换热器AES900-2.5-186.9-4.5/19-6JB1168-731Cr18Ni9Ti1E102闪蒸罐冷凝器1E103加热器1E104T101全凝器AES800-2.5-189.8-4.5/19-4JB1168-731Cr18Ni9Ti1E105T101再沸器BVS1100-1.6-211-3/25-1JB1168-731Cr18Ni9Ti1E106T102冷凝器AES700-2.5-77-4.5/19-6JB1168-73碳钢1E107T102再沸器BVS800-1.6-106-3/25-1JB1168-73碳钢1T101脱环己烷精馏塔

5、3200X198720R1T102精馏塔1400X102920R1C101鼓风机15-400-1600GB/T17774-19992C102空气压缩机QW-150 型GB/T13279-200221010冷却水分配器500X 3050碳钢11011汽液分离罐600X 126011012闪蒸罐11013蒸汽汽提灌1真空泵101真空泵101S5(PMK-3)2配电机28千瓦真空泵102真空泵102S4(PMK-2)2配电机10千瓦附表1设备设备产品型号进口法兰尺寸出口法兰尺寸位号名称DN DDud1b1f 1 m-do1DND2D2d2b2f 2 n2-d 02P101a环己 烷原 料泵IH80-

6、50-315802001601322038-17.550165125992034-17.5P101b环己 烷原 料泵IH80-50-315802001601322038-17.550165125992034-17.5P102a环己 烷进 料泵IH65-40-250651851451182034-17.540150110841834-17.5P102b环己 烷进 料泵IH65-40-250651851451182034-17.540150110841834-17.5P103a三酸 输送 泵IH200-150-25020034029526624312-22.01502852402112438-12

7、.0P103b三酸 输送 泵IH200-150-25020034029526624312-22.01502852402112438-12.0P104a去皂化输送泵IH65-40-250651851451182034-17.540150110841834-17.5P104b去皂化输送泵IH65-40-250651851451182034-17.540150110841834-17.5P105aT101回流 泵IH200-150-25020034029526624312-22.01502852402112438-12.0P105bT101回流 泵IH200-150-2502003402952662

8、4312-22.01502852402112438-12.0.第二张流程图各主要设备第二张流程图各主要设备设备位号设备名称技术规格标准号材料数量备注P201乙醇泵ZA40-250AGB/T 5656-942P202T206冷凝回流泵IH65-50-160GB/T 5656-942P203压送泵IH50-32-250GB/T 5656-942P204T205塔顶回流泵IH50-32-200GB/T 5656-942P206工艺水泵6SH-6GB/T 5656-942P208戊二酸二乙酯泵IS50-32-200GB/T 5656-942P205丁二酸二乙酯泵IS50-32-200GB/T 5656

9、-942P207己二酸二乙酯泵6SH-9AGB/T 5656-942P210戊二酸晶体输送泵GB/T 5656-942P211丁二酸晶体输送泵GB/T 5656-942P209己二酸晶体输送泵GB/T 5656-942V201三酸贮罐A3F衬铝1V204己二酸二乙酯贮罐A3F1V202丁二酸二乙酯贮罐A3F1V203戊二酸二乙酯贮罐A3F1V205T205冷凝贮罐 1400 X 6127 X 9.3A3F1V206T206冷凝贮罐 1400 X 6127 X 9.3A3F1V207乙醇贮罐2400X 4500 X24A3F1V208工艺水贮罐2200X 3462A3F1V210戊二酸贮罐240

10、0X 7000X35L11V211丁二酸贮罐2400X 7000X35L11V209己二酸贮罐2400X 7000X35L11T201脱水塔1T202脱乙醇塔1T203脱乙醇塔1T204脱乙醇塔1T205酯化精馏塔22000X 1465 X681附表2T206酯化精馏塔13600X 2227X401R201酯化釜 800 X 10770 X 4A3F1R202酯水解釜1R203酯水解釜1R204酯水解釜1E201酯化预沸器1E204己二酸冷凝结晶器1E202丁二酸冷凝结晶器1E203戊二酸冷凝结晶器1E205T205冷凝器1E206T206冷凝器1E207T205再沸器 38 X 2.5JB1

11、146-73不锈耐酸钢1立式热虹吸再沸器E208T202再沸器 25 X 2JB1146-7310号碳钢1立式热虹吸再沸器2005己二酸离心过滤机2002酸液分离器2001丁二酸离心分离机2004酸液分离器2003戊二酸离心过滤机2006酸液分离器2007工艺水分配器2008酯化分相器2009蒸汽分配器附表2设备位设备名称产品型号转速流量Q扬程效率功率必须汽蚀叶轮号n(r/mi n)H (m)n (%Kw余量直径m/h i/s轴功(NPSH rmm率Pa(m)P101a环己烷原 料泵IH80-50-3151450256.9432434.191.4P101b环己烷原 料泵IH80-50-3151

12、450256.9432434.191.4P102a环己烷进 料泵IH65-40-2502900308.3378.45012.8P102b环己烷进 料泵IH65-40-2502900308.3378.45012.8P103a三酸输送 泵IH200-150-250145040011120814.5P103b三酸输送泵IH200-150-250145040011120814.5P104a去皂化输 送泵IH65-40-2502900308.3378.45012.8P104b去皂化输 送泵IH65-40-2502900308.3378.45012.8P105aT101回流泵IH200-150-25014

13、5040011120814.5P105bT101回流泵IH200-150-250145040011120814.5P106aT102回流泵MPH3-30290041.11280.84158P106bT102回流泵MPH3-30290041.11280.84158P107a环己醇输 送泵MPH1.5-50C47701.230.34180.34480P107b环己醇输 送泵MPH1.5-50C47701.230.34180.34480P108a环己酮输 送泵MPH1.5-50C47701.230.34180.34480P108b环己酮输 送泵MPH1.5-50C47701.230.34180.34480P201乙醇泵ZA40-250A325318.5P202T206冷凝回流泵IH65-50-1602900308.3330594.15P203压送泵IH50-32-25014506.31.7420271.27P204T205塔顶回流泵IH50-32-20014503.751.0412.9230.57P206工艺水泵6SH-6290016245787446.55251P208戊二酸二 乙酯泵IS50-32-20014507.52.0812440.562.5P205丁二酸二 乙酯泵IS50-32-20014507.52.0812440.562.5P207己二酸二 乙酯泵6SH-9A290