202110测样茶树色谱图F 刘正芳 测

1、色谱图 F:刘正芳20150402测样茶树.qgdTIC36,272,6663.010.020.022.0min峰表 TIC峰高23804296717601948118197619121058621170413238612467674632500020791095702791437672593293963893561032648272697055118167828895397346736332847777258133446296525322050110026123479710551090851297231480682830527693181622949949100542316277317016

2、52841941363547216281133468586010549617535226869128654519331029150139417925017580618199080428853497618497028310244859912422023594760021165220908峰号123456789101112131415161718192021222324252627282930313233343536373839404142434445464748495051525354555657585960保留时间3.5793.6754.2344.2824.4824.6804.8624.976

3、5.0455.0785.4885.5255.6675.9356.0936.4326.7006.7676.8327.1097.2627.3007.4607.5257.6998.3548.5768.8289.2749.6769.99210.03910.23710.48910.55010.61810.72510.81710.86911.00311.05311.14811.29011.50311.57911.70511.79611.89812.01212.36212.45912.57312.65312.75812.86613.10013.15313.26713.31814.135I.Time 3.53

4、33.6334.1924.2584.3334.5424.8084.9255.0085.0585.4425.5085.6505.8836.0086.3926.6586.7426.8007.0757.1427.2837.4257.5007.6008.3178.5428.8009.2429.6429.95810.01710.20010.44210.53310.57510.68310.75810.83310.95811.03311.08311.20811.39211.53311.65811.75811.83311.96712.31712.41712.50812.60812.70012.81713.05

5、813.12513.20813.29214.100F.Time 3.6253.7254.2584.3334.5424.7424.9255.0085.0585.5.5085.6505.6836.0086.1426.4676.7426.8006.8837.1427.2837.4257.5007.6007.7428.3838.6258.8679.3179.72510.01710.12510.27510.53310.57510.68310.75810.83310.95811.03311.08311.20011.39211.53311.65811.75811.83311.96712.05812.4171

6、2.50812.60812.70012.81712.92513.12513.20813.29213.39214.175峰面积395326110506448161503131590613576602209243842209405127967479437260峰面积%峰高% 1.444.070.571.201.270.7114.444.653.035.5116.900.040.185.410.200.440.330.040.050.0421.990.054.920.180.190.070.070.040.070.080.090.170.050.490.030.610.100.101.720.220

7、.130.810.520.302.130.060.032.000.300.110.110.110.490.320.110.170.270.080.140.04100.00积/高度1.661.561.701.601.701.791.771.671.891.681.404.841.011.752.141.731.751.802.012.351.596.631.362.912.291.921.911.811.891.912.363.012.132.081.702.011.912.412.412.162.112.112.433.642.893.292.142.332.082.502.321.932.1

8、02.532.712.052.002.212.672.标记名称1.403.720.571.121.270.74V V V14.944.533.345.4213.810.120.105.520.250.450.340.040.060.0620.450.183.910.300.260.070.080.050.070.090.120.300.060.600.030.720.110.152.420.280.161.000.740.643.600.110.042.720.370.160.140.120.600.480.180.210.320.100.220.05100.00V V V3902173535

9、100829562015595516697581125805496334612183517978017294357804733515503110487508615027382692113692358801283352056692478433493338527091640731697642851612025785310973410110684965978631945699228191822088405180756810167508300315116512769686310448954488194085143512721686545135480950074558043589635527432563

10、0103127979VV VVV V VVV VV V V V VV V VV VV V V V VV V V谱库3 5793.675442.324824.4824.6805.04559.706784.8625.4885.5255.6676.0936.4325.9356.776070.8327.109.3007.4605257.262.6998.3548 5768 8289.2749 6769109.9023910.23710545809100.7621581801.786911.050311.14811.29011 51013.5791.705.01212.3465291122.567533

11、1122.8765681133.11050313.23617814.135<< 目标组分 >>行号#:1保留时间:3.575(扫描数#:130) 质量峰:197原始模式:平均 3.567-3.583(129-131)基峰:93.05(603280)背景模式:峰校准 组 1 -110093771366510512140154180 196218 232 244262 276 286305 318 332 3471030507090110130150170190210230250270290310330350 命中#:1 输入:9579 谱库:NIST05.LIBSI:96

12、式:C10H16 CAS:2867-05-2 摩尔质量:136 保留指数:902组分名称:Bicyclo3.1.0hex-2-ene, 2-methyl-5-(1-methylethyl)- $ 3-Thujene $ .alpha.-Thujene $ Origanene1009377412713665105 1211030507090110130150170190210230250270290310330350命中#:2 输入:6309 谱库:NIST05s.LIBSI:96式:C10H16 CAS:2867-05-2 摩尔质量:136 保留指数:902组分名称:Bicyclo3.1.0h

13、ex-2-ene, 2-methyl-5-(1-methylethyl)- $ 3-Thujene $ .alpha.-Thujene $ Origanene1009377412713665105 1211030507090110130150170190210230250270290310330350命中#:3 输入:6312 谱库:NIST05s.LIBSI:95式:C10H16 CAS:99-83-2 摩尔质量:136 保留指数:969组分名称:.alpha.-Phellandrene $ 1,3-Cyclohexadiene, 2-methyl-5-(1-methylethyl)- $

14、p-Menthadiene (-)-) $1009377391362765511191051030507090110130150170190210230250270290310330350命中#:4 输入:9594 谱库:NIST05.LIBSI:94式:C10H16 CAS:99-83-2 摩尔质量:136 保留指数:969组分名称:.alpha.-Phellandrene $ 1,3-Cyclohexadiene, 2-methyl-5-(1-methylethyl)- $ p-Menthadiene (-)-) $100937713641276551105 119103050709011

15、0130150170190210230250270290310330350 命中#:5 输入:9580 谱库:NIST05.LIBSI:94式:C10H16 CAS:58037-87-9 摩尔质量:136 保留指数:873组分名称:Bicyclo3.1.0hexane, 4-methyl-1-(1-methylethyl)-, didehydro deriv. $ 1-Isopropyl-4-methylbicycl10093772741136651051211030507090110130150170190210230250270290310330350<< 目标组分 >&

16、gt;行号#:2保留时间:3.675(扫描数#:142) 质量峰:203原始模式:平均 3.667-3.683(141-143)基峰:93.05(1460686)背景模式:峰校准 组 1 -11009377414012110513667167175194 207 216 230 239266292 3033203361030507090110130150170190210230250270290310330命中#:1 输入:9602 谱库:NIST05.LIBSI:97式:C10H16 CAS:80-56-8 摩尔质量:136 保留指数:948组分名称:.alpha.-Pinene $ Bic

17、yclo3.1.1hept-2-ene, 2,6,6-trimethyl- $ 2-Pinene $ Pinene $ 2,6,6-Trime100937741271211055367136103050命中#:2 输入:96037090110130150170190210230250270290310330谱库:NIST05.LIBSI:96式:C10H16 CAS:7785-70-8 摩尔质量:136 保留指数:948组分名称:1R-.alpha.-Pinene $ 1R-.alpha.-Pinene $ Bicyclo3.1.1hept-2-ene, 2,6,6-trimethyl-, (

18、1R)- $ 2,10093771214110567271361030507090110130150170190210230250270290310330命中#:3 输入:6319 谱库:NIST05s.LIBSI:96式:C10H16 CAS:488-97-1 摩尔质量:136 保留指数:729组分名称:Tricyclo2.2.1.0(2,6)heptane, 1,3,3-trimethyl- $ Cyclofenchene $1009379391212710513653651030507090110130150170190210230250270290310330命中#:4 输入:9601

19、谱库:NIST05.LIBSI:96式:C10H16 CAS:7785-26-4 摩尔质量:136 保留指数:948组分名称:1S-.alpha.-Pinene $ 1S-.alpha.-Pinene $ (-)-.alpha.-Pinene $ L-.alpha.-Pinene $ Bicyclo3.1.110093774112127105671361030507090110130150170190210230250270290310330命中#:5 输入:6320 谱库:NIST05s.LIBSI:95式:C10H16 CAS:80-56-8 摩尔质量:136 保留指数:948组分名称:.

20、alpha.-Pinene $ Bicyclo3.1.1hept-2-ene, 2,6,6-trimethyl- $ 2-Pinene $ Pinene $ 2,6,6-Trime1009339772712153105671361030507090110130150170190210230250270290310330<< 目标组分 >>行号#:3保留时间:4.233(扫描数#:209) 质量峰:188原始模式:平均 4.225-4.242(208-210)背景模式:峰校准 组 1 -1基峰:93.05(180021)10093774113640436912110714

21、4 155174191208 220 233249 257273 282305 317 32720406080100120140160180200220240260280300320340命中#:1 输入:6299 谱库:NIST05s.LIBSI:95式:C10H16 CAS:555-10-2 摩尔质量:136 保留指数:964组分名称:.beta.-Phellandrene $ Cyclohexene, 3-methylene-6-(1-methylethyl)- $ p-Mentha-1(7),2-diene $ Ph10093774113627651211052040608010012

22、0140160180200220240260280300320340命中#:2 输入:9578 谱库:NIST05.LIBSI:94式:C10H16 CAS:555-10-2 摩尔质量:136 保留指数:964组分名称:.beta.-Phellandrene $ Cyclohexene, 3-methylene-6-(1-methylethyl)- $ p-Mentha-1(7),2-diene $ Ph100937713641276512110720406080100120140160180200220240260280300320340命中#:3 输入:6300 谱库:NIST05s.LI

23、BSI:94式:C10H16 CAS:555-10-2 摩尔质量:136 保留指数:964组分名称:.beta.-Phellandrene $ Cyclohexene, 3-methylene-6-(1-methylethyl)- $ p-Mentha-1(7),2-diene $ Ph100937713641652712110520406080100120140160180200220240260280300320340命中#:4 输入:9568 谱库:NIST05.LIBSI:93式:C10H16 CAS:3387-41-5 摩尔质量:136 保留指数:897组分名称:Bicyclo3.1

24、.0hexane, 4-methylene-1-(1-methylethyl)- $ 4(10)-Thujene $ Sabinen $ Sabinene $ (10093417727694313612110520命中#:5 SI:93406080100120140160180200220240260280300320340输入:6292 谱库:NIST05s.LIB式:C10H16 CAS:3387-41-5 摩尔质量:136 保留指数:897组分名称:Bicyclo3.1.0hexane, 4-methylene-1-(1-methylethyl)- $ 4(10)-Thujene $ S

25、abinen $ Sabinene $ (10093417727536913612110520406080100120140160180200220240260280300320340<< 目标组分 >>行号#:4保留时间:4.283(扫描数#:215) 质量峰:185原始模式:平均 4.275-4.292(214-216)基峰:93.05(389450)背景模式:峰校准 组 1 -1100934169791211365310740146 155177208 221 233 242 253272 287306324 339103050709011013015017019

26、0210230250270290310330命中#:1 输入:9564谱库:NIST05.LIBSI:97式:C10H16 CAS:18172-67-3 摩尔质量:136 保留指数:943组分名称:Bicyclo3.1.1heptane, 6,6-dimethyl-2-methylene-, (1S)- $ 2(10)-Pinene, (1S,5S)-(-)- $ (-)-.bet100934169791212713653107103050命中#:2 输入:62897090110130150170190210230250270290310330谱库:NIST05s.LIBSI:97式:C10H

27、16 CAS:127-91-3 摩尔质量:136 保留指数:943组分名称:.beta.-Pinene $ Bicyclo3.1.1heptane, 6,6-dimethyl-2-methylene- $ 2(10)-Pinene $ Nopinen $ N100934169792753121 136107103050命中#:3 输入:62887090110130150170190210230250270290310330谱库:NIST05s.LIBSI:96式:C10H16 CAS:127-91-3 摩尔质量:136 保留指数:943组分名称:.beta.-Pinene $ Bicyclo3

28、.1.1heptane, 6,6-dimethyl-2-methylene- $ 2(10)-Pinene $ Nopinen $ N1009341697727531211361071030507090110130150170190210230250270290310330命中#:4 输入:6297谱库:NIST05s.LIBSI:96式:C10H16 CAS:18172-67-3 摩尔质量:136 保留指数:943组分名称:Bicyclo3.1.1heptane, 6,6-dimethyl-2-methylene-, (1S)- $ 2(10)-Pinene, (1S,5S)-(-)- $

29、(-)-.bet100934169791212753136107103050命中#:5 输入:95657090110130150170190210230250270290310330 谱库:NIST05.LIBSI:95式:C10H16 CAS:127-91-3 摩尔质量:136 保留指数:943组分名称:.beta.-Pinene $ Bicyclo3.1.1heptane, 6,6-dimethyl-2-methylene- $ 2(10)-Pinene $ Nopinen $ N1009341697727531211361071030507090110130150170190210230

30、250270290310330<< 目标组分 >>行号#:5保留时间:4.483(扫描数#:239) 质量峰:191原始模式:平均 4.475-4.492(238-240)基峰:41.00(385407)背景模式:峰校准 组 1 -1100419369795340107121 136152 166 180207 223243 259 275 288307315334 3501030507090110130150170190210230250 命中#:1 输入:6263 谱库:NIST05s.LIBSI:96式:C10H16 CAS:123-35-3 摩尔质量:136 保

31、留指数:958组分名称:.beta.-Myrcene $ 1,6-Octadiene, 7-methyl-3-methylene- $ Myrcene $2702903103303507-Methyl-3-methylene-1,6-oct100419369792753121107136103050命中#:2 输入:95057090110130150170190210230250270290310330350谱库:NIST05.LIBSI:96式:C10H16 CAS:123-35-3 摩尔质量:136 保留指数:958组分名称:.beta.-Myrcene $ 1,6-Octadiene,

32、7-methyl-3-methylene- $ Myrcene $7-Methyl-3-methylene-1,6-oct100419369275379121107136103050命中#:3 输入:62907090110130150170190210230250270290310330350谱库:NIST05s.LIBSI:95式:C10H16 CAS:123-35-3 摩尔质量:136 保留指数:958组分名称:.beta.-Myrcene $ 1,6-Octadiene, 7-methyl-3-methylene- $ Myrcene $7-Methyl-3-methylene-1,6-

33、oct100419369277953121 1361071030507090110130150170190210230250270290310330350命中#:4 输入:6287谱库:NIST05s.LIBSI:92式:C10H16 CAS:127-91-3 摩尔质量:136 保留指数:943组分名称:.beta.-Pinene $ Bicyclo3.1.1heptane, 6,6-dimethyl-2-methylene- $2(10)-Pinene $ Nopinen $ N100934169277953121136107103050命中#:5 输入:628970901101301501

34、70190210230250270290310330350谱库:NIST05s.LIBSI:91式:C10H16 CAS:127-91-3 摩尔质量:136 保留指数:943组分名称:.beta.-Pinene $ Bicyclo3.1.1heptane, 6,6-dimethyl-2-methylene- $2(10)-Pinene $ Nopinen $ N100934169792753121 1361071030507090110130150170190210230250270290310330350<< 目标组分 >>行号#:6保留时间:4.683(扫描数#:2

35、63) 质量峰:204原始模式:平均 4.675-4.692(262-264)背景模式:峰校准 组 1 -1基峰:93.05(318439)1009377136655111910540148166195 207 220 231 243262288 302320 3331030507090110130150170190210230250270290310330命中#:1 输入:6311 谱库:NIST05s.LIBSI:96式:C10H16 CAS:99-83-2 摩尔质量:136保留指数:969组分名称:.alpha.-Phellandrene $ 1,3-Cyclohexadiene, 2-

36、methyl-5-(1-methylethyl)- $ p-Menthadiene (-)-) $1009377136412751651191051030507090110130150170190210230250270290310330命中#:2 输入:9594谱库:NIST05.LIBSI:95式:C10H16 CAS:99-83-2 摩尔质量:136 保留指数:969组分名称:.alpha.-Phellandrene $ 1,3-Cyclohexadiene, 2-methyl-5-(1-methylethyl)- $ p-Menthadiene (-)-) $1009377136412

37、75165105 1191030507090110130150170190210230250270290310330命中#:3 输入:6312谱库:NIST05s.LIBSI:94式:C10H16 CAS:99-83-2 摩尔质量:136 保留指数:969组分名称:.alpha.-Phellandrene $ 1,3-Cyclohexadiene, 2-methyl-5-(1-methylethyl)- $ p-Menthadiene (-)-) $1009377391362751651191051030507090110130150170190210230250270290310330命中#

38、:4 输入:6309谱库:NIST05s.LIBSI:94式:C10H16 CAS:2867-05-2 摩尔质量:136 保留指数:902组分名称:Bicyclo3.1.0hex-2-ene, 2-methyl-5-(1-methylethyl)- $ 3-Thujene $ .alpha.-Thujene $ Origanene10093774127136651051211030507090110130150170190210230250270290310330命中#:5 输入:9579 谱库:NIST05.LIBSI:93式:C10H16 CAS:2867-05-2 摩尔质量:136 保留

39、指数:902组分名称:Bicyclo3.1.0hex-2-ene, 2-methyl-5-(1-methylethyl)- $ 3-Thujene $ .alpha.-Thujene $ Origanene10093774127136651051211030507090110130150170190210230250270290310330<< 目标组分 >>行号#:7保留时间:4.858(扫描数#:284) 质量峰:207原始模式:平均 4.850-4.867(283-285)背景模式:峰校准 组 1 -1基峰:121.10(3568063)1009312113677

40、105416540146154173191207223249 263290 30231920406080100120140160180200220240260280300320340命中#:1 输入:9616 谱库:NIST05.LIB SI:96式:C10H16 CAS:29050-33-7摩尔质量:136 保留指数:919组分名称:(+)-4-Carene $ 4,7,7-Trimethylbicyclo4.1.0hept-2-ene # $100931211367941105673620406080100120140160180200220240260280300320340命中#:2

41、输入:6331 谱库:NIST05s.LIBSI:95式:C10H16 CAS:99-86-5 摩尔质量:136 保留指数:998组分名称:1,3-Cyclohexadiene, 1-methyl-4-(1-methylethyl)- $ .alpha.-Terpinen $ .alpha.-Terpinene $ p-Men100931211367710541276520406080100120140160180200220240260280300320340命中#:3 输入:6335 谱库:NIST05s.LIBSI:95式:C10H16 CAS:586-62-9 摩尔质量:136 保留指

42、数:1052组分名称:Cyclohexene, 1-methyl-4-(1-methylethylidene)- $ p-Mentha-1,4(8)-diene $ Terpinolen $ Terpinole100931211367941271056720命中#:4 SI:95406080100120140160180200220240260280300320340输入:9637 谱库:NIST05.LIB式:C10H16 CAS:99-86-5 摩尔质量:136 保留指数:998组分名称:1,3-Cyclohexadiene, 1-methyl-4-(1-methylethyl)- $ .

43、alpha.-Terpinen $ .alpha.-Terpinene $ p-Men10012193136273977431056520命中#:5 SI:95406080100120140160180200220240260280300320340输入:9615 谱库:NIST05.LIB式:C10H16 CAS:554-61-0 摩尔质量:136 保留指数:948组分名称:Bicyclo4.1.0hept-2-ene, 3,7,7-trimethyl- $ 2-Carene $ (+)-2-Carene $ 3,7,7-Trimethylbicyclo1009312113679411052

44、76720406080100120140160180200220240260280300320340<< 目标组分 >>行号#:8保留时间:4.975(扫描数#:298) 质量峰:180原始模式:平均 4.967-4.983(297-299)背景模式:峰校准 组 1 -1基峰:119.10(2407626)1001191349165 775110340148 158181 192 207 220 232 244 258 267 282 2973153351030507090110130150170190210230250270290310330命中#:1 输入:5934

45、 谱库:NIST05s.LIBSI:97式:C10H14 CAS:527-84-4 摩尔质量:134 保留指数:1042组分名称:Benzene, 1-methyl-2-(1-methylethyl)- $ o-Cymene $ o-Cymol $ o-Isopropyltoluene $ 1-Isopropyl-1001191349141776510327511030507090110130150170190210230250270290310330命中#:2 输入:5930 谱库:NIST05s.LIBSI:96式:C10H14 CAS:535-77-3 摩尔质量:134 保留指数:104

46、2组分名称:Benzene, 1-methyl-3-(1-methylethyl)- $ m-Cymene $ .beta.-Cymene $ m-Cymol $ m-Isopropyltoluen100119134913965 7751103271030507090110130150170190210230250270290310330命中#:3 输入:5933 谱库:NIST05s.LIBSI:96式:C10H14 CAS:527-84-4 摩尔质量:134 保留指数:1042组分名称:Benzene, 1-methyl-2-(1-methylethyl)- $ o-Cymene $ o-Cymol $ o-Isopropyltoluene $ 1-Isopropyl-100119134913965 7751271031030507090110130150170190210230250270290310330命中#:4 输入:5915 谱库:NIST05s.LIBSI:95式:C10H14 CAS:99-87-6 摩尔质量:134 保留指数:1042组分名称:Benzene, 1-methyl-4-(1-methylethyl)- $ p-Cymene $ p-Cimene $ p-Cymol $ p-I