2022 锆化合物化学分析方法 钙、铪、钛、钠、铁、铬、镉、锌、锰、铜、镍、铅含量的测定 电感耦合等离子体原子发射光谱法

!"!#!""#$""%""

!!!"

!!!"#$%!"!#$%$"&'&'#&'()*+,!-$./$&'("#0123456,%067

45&

89:!"#0;<=>?@ABCD&!"#0EFG2HIJKLCD0MN&

!"#OPQRSTU)VWXYZ&

!"#O[QRSTU&'(\]^_X'()*!#*&+,(`a&

!"#45bc$defghijklmnopqrPs)detuvw\xyRz{|)deT

}RS~m€Rz{|)‚ƒ'„d(…VRz{|)†‡ˆPT‰ŠRSTUxyRz{|&

!"#‹Œ45$Ž)")‘’)“)Ž”•)–—˜)™š›)œ)žŸ

)¡¢£)¤¥¦)

§¨—&

!

书

!"!#!""#$""%""

#$%&$'()*+

,)-).)/)0)1)2)3)4)

5)6)789:;<

=>?%@ABCDBEFGH+

&!IJ

!"#©ª«¬­®¯°±²³´µ³E¶·¸¹7…(°ºP»)¼)½)¾)¿)À)Á)Â)

Ã)Ä)Å3ÆÇn0ȹ&

!"#ɬÊËÌ(…)Í΅)Ï΅)ÐË(…P»)¼)½)¾)¿)À)Á)Â)Ã)Ä)Å3ÆÇ

n07&7ÑÒÓÔ$&

K&!;<IJ

mn/×mn/×

ÕÖÕÖ

--

*.'%'''/"'%'/'*0'%'''/"'%'/'

12'%$''"&%'''34'%'''/"'%'/'

#5'%'''/"'%'/'64'%'''/"'%'/'

7.'%'''/"'%'/'*8'%'''/"'%'/'

9:'%'''/"'%'/'75'%'''/"'%'/'

*;'%'''/"'%'/'<='%'''/"'%'/'

"!LIMNOPQ

ØÙ"#P0=>ÚÛ"P06ÑÜݬÞ2ß!"#àH?á0âã&äP*9åæ0ݬ"

#*çèåæéê0ë!ɬÊ!"#+H9åæ0ݬ"#*äìíë!'îïðR0ñòb(ɬÊ

!"#&

!"!#>>?&!/óôrõ¬ö6‚3€rȹ

!"!#?$@'!×÷ñø6,hùz×÷0Ôú3û7

!"!#$@+,,!üTkl(ý/óþÿ]!

$!RST<U

!"!#$@+,,"70]!37#ɬÊ!"#&

!!DV

€$%&Î'(*)i&Î*mP*¬­®¯°±²³´µ³E¶·¸¹+,7*Ê-ÕÖ.7

$

!"!#!""#$""%""

0/01näE¶23&4¬)*56¹78-ÕÖ0mn93*:mn/×Ôú71;&

'!WXTYZ

<=>R?@*)/óPçA¬BCDEFG0€H&

'%&!ö$!"!#>>?&*IF&

'%"!&Î$!A$%$BC!DE&

'%$!&'JK'L$»)¼)½)¾)¿)À)Á)Â)Ã)Ä)Å)Æ4¬RMæ=RNO0bÕÖ&'JK

'L*mn93D$'''#C!DE&

'%!!»)½)¾)¿)À)Á)Â)Ã)Ä)Å)ÆP°&''L$/LQR/%''DE»)½)¾)¿)À)Á)Â)

Ã)Ä)Å)Æ&'JK'L'/%,(Ê$''DES$>nTP*UV/DE&Î'/%&(*:öiWXY3*P

Z&['L$DE/LÇR/'#C»)½)¾)¿)À)Á)Â)Ã)Ä)Å)Æ&

'%'!¼&''L$QR$'%''DE¼&'JK'L'/%,(Ê$''DE>nTP*UV/DE&Î'/%&(*:

öiWXY3*PZ&['L$DEÇR$''#C¼&

'%(!Ë(…þ´'»)½)¾)¿)À)Á)Â)Ã)Ä)Å)ÆÕÖ0mn/×H\Ê'%'''&-($]R&&%&&C

vGËÌ(…'Ë(…ÇnH^Ê,>-(*UV$'DE&Î'/%&(*U_'(*`a*bV$''DES$>

nTP*:öiWXY3*PZ&['L$DEÇR?'DCË(…&

'%#!cd$´e/×H^ÊBB%BB-&

(![\]^

­®¯°±²³´µ³E¶·¸f*gh/ó6ÓÔ&&

K"!_`()a

bcDij

ÕÖ/0ÕÖ/0

*.,B,%,>>*0&$+%+,?

12&@@%,,>34&'&%//$

#5,,+%B+$64&/@%>$'

7./?B%/B&*8,&+%@/+

9:&/B%B+'75&&$%>+@

*;&'/%//&<=&&'%,/,

#!bc

klDl&m*nopqr]n&

)!Wdef

)%&!WZ

$Ô,]Rkl*sBX'%'''$C&tu-klP0Ë(…Çn*]Rvê€$n*wxXþ´'

&

!"!#!""#$""%""

Lmn93?C!E&

K$!WZ9

Ë(…Çn'mn/×(€$n

kly]

-C

,/&%&B

ËÌ(…

,>&%&&

,&&%/'

Í΅

,,&%+&

,?&%$$

Ï΅+'&%''

+&$%B'

ÐË(…,?&%$$

)%"!ghWd

z{y,€r*Rä|÷&

)%$!ijWd

]Rv}n0Ë(…þ´*~€$z€€r&

)%!!()Wk:l^

)%!%&!,).)/)0)1)2)3)4)5)6)7()Wk:l^

‚€$'?%$(ƒÊ&''DE„…†‡ˆ‰ŠP*UVánö*UV/DE&Î'/%&(*‹ŒU_X'(

[*`aXõŒ*QV$''DES$>nTP*¬öiWXY3*PZ&

)%!%"!-()Wk:l^

QR/%''DE€L'?%+%$(Ê$''DE0>nTP*UV/DE&Î'/%&(*:öiWXY3*PZ&

)%'!mnopqk:rl

)%'%&!,).)/)0)1)2)3)4)5)6)7mnopqk:rl

'BQR'%''DE)'%&'DE)$%''DE)+%''DE)$'%''DE)&'%''DEP°&''L'/%+(ʎ

$''DES$>nTP*/Lʐ‘S$>nTPUV$'%''DEË(…þ´'/%>(*UV/DE&Î

'/%&(*¬öiWXY3*PZ&[’Ù&''Lmn93D'%''#C!DE)'%$'#C!DE)'%/'#C!DE)

&%''#C!DE)/%''#C!DE)$'%''#C!DE&

)%'%"!-mnopqk:rl

'BQR'%''DE)$%''DE)&%''DE)/%''DE)$'%''DE)&'%''DE¼&''L'/%/(ʎ

$''DE>nTP*UV/DE&Î'/%&(*¬öiWXY3*PZ&[’Ù&''Lmn93D

'%''#C!DE)$%''#C!DE)&%''#C!DE)/%''#C!DE)$'%''#C!DE)&'%''#C!DE&

,

!"!#!""#$""%""

)%(!;<

$Ô&ðúf“0/ó6*Ê­®¯°±²³´µ³E¶·¸f”*n)*56’Ù&''

L*})*566Üv•’×!"'%BBB–*€€€LB/ó€L'?%+%$—?%+%&(P˜ÕÖ0E¶

23*f“tu&')*56*78™šZ-ÕÖÇn&

*!WdstuV

-ÕÖÇn:-ÕÖ0mn/×'"#(7*$›'$(78$

%>

'!%!'(&,&$'$'

"#$'$''-----------'$(

(,&&

!!›P$

!"""œ)*56”ž0/ó€LPŸÕÖ0mn93*bcD

¡¢£'#C!DE(+

!'"""œ)*56”ž0€€LPŸÕÖ0mn93*bcD

¡¢£'#C!DE(+

&"""€L¤´e*bcD¢£'DE(+

&$"""Ÿ€L´e*bcD¢£'DE(+

("""kl0mn0×÷*bcD¡'C(+

&&"""/R€L´e*bcD¢£'DE(+

#"""˜ÕÖ&

}mn/×^Ê'%''$'-–*781;¥¦$cRMק+mn/×D'%''$'-"'%'/'-–*7

81;¥¦&cRMק+mn/×\Ê'%$'-–*781;¥¦^רp{c&×÷ñø$

!"!#?$@'067©,&

&%!vwx

&%%&!yzM

)ª«Üâ#جž0{­®q€1;07÷*)Ô+¯Z0|÷ÑÒ=*°{‘€1;

0±é²÷H³Ûª«Üz')(*³Ûª«Üz')(0´µH³Û/-*ª«Üz')($Ô+×u4¬6

Ü=¶¹—·¸¹¹ž&sº3€rµ»×u¼Ó½¾)&

K!!yzM{'!(

"*.!-'%'''/'%''&/'%''+?'%'&/

)!-'%'''$'%'''&'%'''/'%''$?

"12!-'%$,'%>/$%>,"

)!-'%'$'%'&'%'+"

"#5!-'%'''/'%''&/'%''/''%'&/

)!-'%'''$'%''','%'''+'%'''B

"7.!-'%'''/'%''&/'%''+B'%'&/

)!-'%'''$'%''','%'''+'%''$&

"9:!-'%'''/'%''&/'%''/''%'&/

+

!"!#!""#$""%""

K!!yzM{'!('¿(

)!-'%'''$'%''','%'''+'%''$/

"*;!-'%'''/'%''&/'%''/''%'&/

)!-'%'''$'%''','%'''/'%''$,

"*0!-'%'''/'%''&/'%''+B'%'&/

)!-'%'''$'%''','%'''+'%''$@

"34!-'%'''/'%''&/'%''+B'%'&/

)!-'%'''$'%''','%'''+'%''$,

"64!-'%'''/'%''&/'%''+B'%'&/

)!-'%'''$'%''','%'''+'%''$/

"*8!-'%'''/'%''&/'%''+?'%'&/

)!-'%'''$'%'''&'%'''+'%''$/

"75!-'%'''/'%''&/'%''+B'%'&/

)!-'%'''$'%''','%'''+'%''$&

"<=!-'%'''/'%''&+'%''+?'%'&/

)!-'%'''$'%''','%'''+'%''$$

&%%"!|}M

)ÀÁÜâ#جž0{­®q€1;07÷*)Ô/¯Z0|÷ÑÒ=*°{‘€1;

0±é÷²H³ÛÀÁÜz'*(*³ÛÀÁÜz'*(0´µH³Û/-*ÀÁÜz'*($Ô/×u4¬6

Ü=¶¹—·¸¹¹ž&

K'!|}M{'"(

"*.!-'%'''/'%''&/'%''+?'%'&/

*!-'%'''$'%'''+'%'''@'%''&&

"12!-'%$,'%>/$%>,"

*!-'%'$'%','%'>"

"#5!-'%'''/'%''&/'%''/''%'&/

*!-'%'''$'%'''+'%'''/'%''$>

"7.!-'%'''/'%''&/'%''+B'%'&/

*!-'%'''$'%''','%'''@'%''$/

"9:!-'%'''/'%''&/'%''/''%'&/

*!-'%'''$'%'''+'%'''/'%''&,

"*;!-'%'''/'%''&/'%''/''%'&/

*!-'%'''$'%''','%'''>'%''&,

"*0!-'%'''/'%''&/'%''+B'%'&/

/

!"!#!""#$""%""

K'!|}M{'"('¿(

*!-'%'''$'%''','%'''/'%''&@

"34!-'%'''/'%''&/'%''+B'%'&/

*!-'%'''$'%''','%'''>'%''$B

"64!-'%'''/'%''&/'%''+B'%'&/

*!-'%'''$'%'''+'%'''/'%''&'

"*8!-'%'''/'%''&/'%''+?'%'&/

*!-'%'''$'%''','%'''/'%''&'

"75!-'%'''/'%''&/'%''+B'%'&/

*!-'%'''$'%''','%'''>'%''$B

"<=!-'%'''/'%''&+'%''+?'%'&/

*!-'%'''$'%''','%'''>'%''&'

&&!Wd~

€rÂÃê¯Z$

.(!€réÄ+

=(!!"#ÅÆ+

F(!/ó1;BäÔú+

0(!hþ!€rÇÈ0²É+

:(!ÊËÌ0ÉÍÁÄ+

2(!€råæ&

>

!"!#!""#$""%""

€!!$

'‚ZM(

vwxWdDƒst

!!sº3×uÎ)&'&$ÏO/Ðôrõé…(°ºP»)½)¾)¿)À)Á)Â)Ã)Ä)Å)Æ0+‘

Hökl*¼,‘Hökl+,Ñ€rB70&‘ôrõ鐑ö0kl)ª«Üâ

#Ø®q7$$­&n0µ»×uÓÔ)%$&

K$%&!vwxWdDƒst

|÷ª«Ü&'²ÀÁÜ&'²ª«Üz')(ÀÁÜz'*(

ÕÖö×

-'+)('+*(--

*.'%'''/'%''''&'%'''','%''''>'%''''?

#5'%'''/'%''''&'%'''','%''''/'%''''?

7.'%'''/'%''''&'%''''&'%''''/'%''''@

9:'%'''/'%''''&'%''''&'%''''/'%''''@

*;'%'''/'%''''&'%'''','%''''/'%''''?

*0$'%'''/'%''''&'%''''&'%''''+'%''''+

34'%'''/'%''''&'%''''&'%''''/'%''''/

64'%'''/'%''''&'%'''','%''''>'%''''?

*8'%'''/'%''''&'%''''&'%''''+'%''''>

75'%'''/'%''''&'%'''','%''''/'%''''?

<='%'''/'%''''&'%''''&'%''''/'%''''>

*.'%''&/'%''''@'%'''$,'%'''$B'%''',>

#5'%''&/'%''''@'%'''$,'%'''&''%''',@

7.'%''&/'%''''?'%''''B'%'''&,'%'''&/

9:'%''&/'%''''B'%'''$/'%'''&>'%'''+&

*;'%''&/'%''''?'%''''B'%'''&+'%'''&>

*0&'%''&/'%''''?'%''''B'%'''&$'%'''&+

34'%''&/'%''''?'%'''$''%'''&$'%'''&?

64'%''&/'%''''?'%'''$$'%'''&$'%''',$

*8'%''&/'%''''>'%''''@'%'''$@'%'''&$

75'%''&/'%''''@'%'''$''%'''&''%'''&?

<='%''&+'%''''?'%''''B'%'''&,'%'''&>

*.'%''+?'%'''$>'%'''&&'%'''++'%'''>,

#5'%''/''%'''$+'%'''$@'%''',B'%'''+?

,

7.'%''+B'%''''B'%'''&+'%'''&+'%'''>?

9:'%''/''%'''$+'%'''$?'%''',B'%'''+B

@

!"!#!""#$""%""

K$%&!vwxWdDƒst'¿(

|÷ª«Ü&'²ÀÁÜ&'²ª«Üz')(ÀÁÜz'*(

ÕÖö×

-'+)('+*(--

*;'%''/''%'''$/'%'''$/'%'''+$'%'''+&

*0'%''+B'%'''$+'%'''$@'%'''+''%'''+