中国药典中药材中农残检测.pdf

15 100 2000 6000 2014 01 v1 tel 010 83130651tel 020 38811673tel 0755 26075073tel 027 59812739tel 028 85254001 2tel 025 83737312 83716726 fax 010 83130098fax 020 38811631fax 0755 26075056fax 027 59812738fax fax 025 83701408 cdgg 131116 06 4pak 25 gcms 1 50 mg l 4 x 1 ml cas 16alpha hchalpha 319 84 6 211beta hchbeta 319 85 7 312gamma hch lindane gamma 58 89 9 413quintozene 82 68 8 515delta hchdelta 319 86 8 618pentachloraniline 527 20 8 737heptachlor exo epoxide exo 1024 57 3 838oxychlordane 27304 13 8 939heptachlor endo epoxide endo 28044 83 9 1045trans chlordane 5103 74 2 1147cis chlordane 5103 71 9 1248o p ddeo p dde3424 82 6 1349alpha endosulfanalpha 959 98 8 1452o p dddo p ddd53 19 0 1553p p ddep p dde72 55 9 1657p p dddp p ddd72 54 8 1758o p ddto p ddt789 02 6 1859beta endosulfanbeta 33213 65 9 1960endosulfan sulfate 1031 07 8 2061p p ddtp p ddt50 29 3 2165methoxychlor 72 43 5 2266mirex 2385 85 5 2322heptachlor 76 44 8 2428aldrin 309 00 2 2554endrin 72 20 8 cdgg 131113 06 4pak 10 gcms 2 50 mg l 4 x 1 ml cas 11dichlorvos 62 73 7 214terbufos 13071 79 9 320chlorpyrifos methyl 5598 13 0 421parathion methyl 298 00 0 524fenchlorphos 299 84 3 626fenitrothion 122 14 5 731chlorpyrifos 2921 88 2 832parathion 56 38 2 935bromophos 2104 96 3 1046bromophos ethyl 4824 78 6 cdgg 130995 06 4pak 30 lcms 1 50 mg l 4 x 1 ml cas 112azinphos methyl guthion 86 50 0 220cadusafos 95465 99 9 333diazinon 333 41 5 434dichlofenthion 97 17 6 539dimethoate 60 51 5 645epn 2104 64 5 747ethion 563 12 2 848ethoprophos 13194 48 4 950etrimfos 38260 54 7 1051fenamiphos 22224 92 6 1158fensulfothion 115 90 2 1262fenthion 55 38 9 1372fonofos 944 22 9 1473fosthiazate 98886 44 3 1582isazofos 42509 80 8 1683isofenphos 25311 71 1 1788malathion 121 75 5 1892methacrifos 62610 77 9 1994methidathion 950 37 8 20101mevinphos 7786 34 7 21114phenthoate 2597 03 7 22115phorate 298 02 2 23119phosalone 2310 17 0 24121phosphamidon 13171 21 6 25126pirimiphos methyl 29232 93 7 26129profenofos 41198 08 7 27136prothiophos 34643 46 4 28140quinalphos 13593 03 8 29150tolclofos methyl 57018 04 9 30152triazophos 24017 47 8 wg 2014022101 v1 tel 010 83130651tel 020 38811673tel 0755 26075073tel 027 59812739tel 028 85254001 2tel 025 83737312 83716726 fax 010 83130098fax 020 38811631fax 0755 26075056fax 027 59812738fax fax 025 83701408 15 100 2000 6000 wg 2014022101 v1 cdgg 131114 06 4pak 10 gcms 3 50 mg l 4 x 1 ml cas 117 79538 32 2 263bifenthrin 82657 04 3 367phenothrin 26002 80 2 468acrinathrin 103833 18 7 569cyhalothrin 68085 85 8 670permethrin 52645 53 1 771 68359 37 5 872cypermethrin 52315 07 8 973flucythrinate 70124 77 5 1075fenvalerate 51630 58 1 1176deltamethrin 52918 63 5 cdgg 131115 06 4pak 10 gcms 4 50 mg l 4 x 1 ml cas 12diphenylamine 122 39 4 23tecnazene 117 18 0 37dicloran 99 30 9 48hexachlorobenzene 118 74 1 516chlorothalonil 1897 45 6 619vinclozolin 50471 44 8 727 1085 98 9 833triadimefon 43121 43 3 942triadimenol baitan 55219 65 3 1044procymidone 32809 16 8 cdgg 131117 06 4pak 18 gcms 5 50 mg l 4 x 1 ml cas 14chlordimeform 6164 98 3 25 1582 09 8 39pentachloranisole 1825 21 4 423octachlorodipropyl ether s421 127 90 2 525 1825 19 0 630dicofol deg dcbp 115 32 2 734chlorthal dimethyl 1861 32 1 836dibutalin butralin 33629 47 9 940pendimethalin 40487 42 1 1041dimepiperate 61432 55 1 1143fipronil 120068 37 3 1250flumetralin 62924 70 3 1351dieldrin 60 57 1 1455nitrofen 1836 75 5 1556chlorfenapyr 122453 73 0 1662bromopropylate 18181 80 1 1764fenpropathrin 39515 41 8 1874quizalofop ethyl quizalofop p ethyl 76578 14 8 cdgg 130996 06 4pak 18 lcms 2 50 mg l 4 x 1 ml cas 14aldicarb 116 06 3 25aldicarb sulfone 1646 88 4 36aldicarb sulfoxide 1646 87 3 421carbaryl 63 25 2 523carbofuran 1563 66 2 646ethiofencarb 29973 13 5 774furathiocarb 65907 30 4 880indoxacarb 173584 44 6 985isoprocarb 2631 40 5 1089mecarbam 2595 54 2 1195methiocarb 2032 65 7 1296methomyl 16752 77 5 1399metolcarb 1129 41 5 14110oxamyl 23135 22 0 15124pirimicarb 23103 98 2 16130promecarb 2631 37 0 17135propoxur 114 26 1 1824carbofuran 3 hydroxy3 16655 82 6 wg 2014022101 v1 tel 010 83130651tel 020 38811673tel 0755 26075073tel 027 59812739tel 028 85254001 2tel 025 83737312 83716726 fax 010 83130098fax 020 38811631fax 0755 26075056fax 027 59812738fax fax 025 83701408 cdgg 130997 06 4pak 37 lcms 3 50 mg l 4 x 1 ml cas 11acephate 30560 19 1 211azinphos ethyl 2642 71 9 329coumaphos 56 72 4 432demeton o s 8065 48 3 535dicrotophos 141 66 2 641disulfoton 298 04 4 742disulfoton sulfone 2497 06 5 843disulfoton sulfoxide 2497 07 6 952fenamiphos sulfone 31972 44 8 1053fenamiphos sulfoxide 31972 43 7 1156fenchlorphos oxon 3983 45 7 1259fensulfothion oxon 6552 21 2 1360fensulfothion oxon sulfone 6132 17 8 1461fensulfothion sulfone 14255 72 2 1563fenthion d6 o o dimethyl d6 1189662 83 6 1664fenthion oxon 6552 12 1 1765fenthion oxon sulfone 14086 35 2 1866fenthion oxon sulfoxide 6552 13 2 1967fenthion sulfone 3761 42 0 2068fenthion sulfoxide 3761 41 9 2184isofenphos methyl 99675 03 3 2287malaoxon 1634 78 2 2393methamidophos 10265 92 6 24103monocrotophos 6923 22 4 25106n desethyl pirimiphos methyln 67018 59 1 26112paraoxon ethyl 311 45 5 27113paraoxon methyl 950 35 6 28116phorate oxon 2600 69 3 29117phorate oxon sulfone 2588 06 9 30118phorate sulfone 2588 04 7 31120phosmet 732 11 6 32122phoxim 14816 18 3 33125pirimiphos ethyl 23505 41 1 34142sulfotep 3689 24 5 35107omethoate 1113 02 6 36133propetamphos 31218 83 4 37153trichlorfon 52 68 6 15 100 2000 6000 wg 2014022101 v1 cdgg 130998 06 4pak 24 lcms 4 50 mg l 4 x 1 ml cas 1127pretilachlor 51218 49 6 2131propanil 709 98 8 33alachlor 15972 60 8 48ametryn 834 12 8 59atrazine 1912 24 9 610atrazine d5 ethyl d5 163165 75 1 719butachlor 23184 66 9 828clethodim 99129 21 2 938dimethenamid p p163515 14 8 1069fluazifop p butyl 79241 46 6 1175haloxyfop methyl 69806 40 2 1277hexazinone 51235 04 2 1398metolachlor 51218 45 2 14100metribuzin 21087 64 9 15102molinate 2212 67 1 16105napropamide 15299 99 7 177allethrin 584 79 2 1830cyhalofop butyl 122008 85 9 1949etofenprox 80844 07 1 20143tau fluvalinate 102851 06 9 21146tetramethrin 7696 12 0 22108oxadiazon 19666 30 9 23111paclobutrazol 76738 62 0 24123piperonyl butoxide 51 03 6 15 100 2000 6000 wg 2014022101 v1 tel 010 83130651tel 020 38811673tel 0755 26075073tel 027 59812739tel 028 85254001 2tel 025 83737312 83716726 fax 010 83130098fax 020 38811631fax 0755 26075056fax 027 59812738fax fax 025 83701408 cdgg 130999 06 4pak 29 lcms 5 50 mg l 4 x 1 ml cas 1109oxadixyl 77732 09 3 2128prochloraz 67747 09 5 3134propiconazole 60207 90 1 4137pyraclostrobin 175013 18 0 5144tebuconazole 107534 96 3 6147thiabendazole 148 79 8 7151 731 27 1 814benalaxyl 71626 11 4 916bitertanol 55179 31 2 1017boscalid 188425 85 6 1122carbendazim 10605 21 7 1231cyprodinil 121552 61 2 1336difenoconazole 119446 68 3 1440diniconazole 83657 24 3 1544edifenphos 17109 49 8 1654fenarimol 60168 88 9 1755fenbuconazole 114369 43 6 1870flusilazole 85509 19 9 1971flutolanil 66332 96 5 2076hexaconazole 79983 71 4 2178imazalil 35554 44 0 2281iprodione 36734 19 7 2386isoprothiolane 50512 35 1 2490mepronil 55814 41 0 2591metalaxyl 57837 19 1 26104myclobutanil 88671 89 0 27154tricyclazole 41814 78 2 2813azoxystrobin 131860 33 8 29155 141517 21 7 cdgg 131112 06 4pak 17 lcms 6 50 mg l 4 x 1 ml cas 1132propargite 2312 35 8 2138pyridaben 96489 71 3 3139pyriproxyfen 95737 68 1 4141rh 5849 112225 87 3 5145tebufenozide 112410 23 8 6148thiacloprid 111988 49 9 7149thiamethoxam 153719 23 4 82acetamiprid 135410 20 7 918buprofezin 69327 76 0 1025chinomethionat 2439 01 2 1126chlorantraniliprole 500008 45 7 1227chlorfenvinphos 470 90 6 1337 35367 38 5 1479imidacloprid 138261 41 3 1597methoxyfenozide 161050 58 4 1615bifenazate 149877 41 8 1757fenpyroximate 111812 58 9 cas 162 73 7 dichlorvos剧毒 不能提供 2122 39 4 diphenylaminecdct c12890000 3117 18 0 tecnazenecdct c17200000 46164 98 3 chlordimeformcdct c11240000 51582 09 8 cdct c17850000 6319 84 6alpha alpha hchcdct c14071000 799 30 9 diclorancdct c12560000 8118 74 1 hexachlorobenzenecdct c14160000 91825 21 4 pentachloranisolecdct c15950000 10319 85 7beta beta hchcdct c14072000 1158 89 9gamma gamma hch lindane cdct c14073000 1282 68 8 quintozenecdct c16730000 1313071 79 9 terbufos剧毒 不能提供 14319 86 8delta delta hchcdct c14074000 151897 45 6 chlorothalonilcdct c11510000 1679538 32 2 cdct c17213000 17527 20 8 pentachloranilinecdct c15940000 1850471 44 8 vinclozolincdct c17920000 195598 13 0 chlorpyrifos methylcdct c11601000 20298 00 0 parathion methyl剧毒 不能提供 2176 44 8 heptachlor剧毒 不能提供 22127 90 2 octachlorodipropyl ether s421 cdct c16900000 23299 84 3 fenchlorphoscdct c13460000 241825 19 0 cdct c15120000 25122 14 5 fenitrothion剧毒 不能提供 261085 98 9 cdct c12300000 27309 00 2 aldrincdct c10090000 28115 32 2 dicofol deg dcbp cdct c12570000 292921 88 2 chlorpyrifoscdct c11600000 3056 38 2 parathion剧毒 不能提供 3143121 43 3 triadimefoncdct c17610000 321861 32 1 chlorthal dimethylcdct c11620000 332104 96 3 bromophoscdct c10745000 3433629 47 9 dibutalin butralin cdct c10910000 351024 57 3 exo heptachlor exo epoxidecdct c14101000 3627304 13 8 oxychlordanecdgg 030353 05 3728044 83 9 endo heptachlor endo epoxidecdct c14102000 3840487 42 1 pendimethalincdct c15930000 163165 75 1 d5 atrazine d5 cdgg 130983 06 1ml 1189662 83 6 fenthion d6 cas 130560 19 1 acephatecdct c10010000 2135410 20 7 acetamipridcdct c10013000 315972 60 8 alachlorcdct c10060000 4116 06 3 aldicarb 51646 88 4 aldicarb sulfonecdct c10080000 61646 87 3 aldicarb sulfoxidecdct c10080500 7584 79 2 allethrincdct c10100000 8834 12 8 ametryncdct c10150000 91912 24 9 atrazinecdct c10330000 10163165 75 1 atrazine d5 ethyl d5 112642 71 9 azinphos ethylcdct c10360000 1286 50 0 azinphos methylcdct c17320000 13131860 33 8 azoxystrobincdct c10413000 1471626 11 4 benalaxylcdct c10440000 15149877 41 8 bifenazatecdct c10579500 1655179 31 2 bitertanolcdct c10660000 17188425 85 6 boscalidcdct c10663000 1869327 76 0 buprofezincdct c10854000 1923184 66 9 butachlorcdct c10860000 2095465 99 9 cadusafoscdct c10934000 2163 25 2 carbarylcdct c10980000 2210605 21 7 carbendazimcdct c10990000 231563 66 2 carbofuran 2416655 82 63 carbofuran 3 hydroxycdct c11011000 252439 01 2 chinomethionatcdct c11080000 26500008 45 7 chlorantraniliprolecdct c11145000 27470 90 6 chlorfenvinphos 2899129 21 2 clethodimcdct c11669000 2956 72 4 coumaphos 30122008 85 9 cyhalofop butylcdct c11858000 31121552 61 2 cyprodinil 328065 48 3 demeton o s 33333 41 5 diazinoncdct c12210000 3497 17 6 dichlofenthioncdct c12290000 35141 66 2 dicrotophos 36119446 68 3 difenoconazolecdct c12609000 3735367 38 5 cdct c12630000 38163515 14 8 pdimethenamid pcdct c12678000 3960 51 5 dimethoatecdct c12700000 4083657 24 3 diniconazolecdct c12777000 41298 04 4 disulfoton 422497 06 5 disulfoton sulfonecdct ca12985000 432497 07 6 disulfoton sulfoxide 4417109 49 8 edifenphoscdct ca13110000 452104 64 5 epn 15 100 2000 6000 wg 2014022101 v1 tel 010 83130651tel 020 38811673tel 0755 26075073tel 027 59812739tel 028 85254001 2tel 025 83737312 83716726 fax 010 83130098fax 020 38811631fax 0755 26075056fax 027 59812738fax fax 025 83701408 cas 3961432 55 1 dimepiperatecdct c12665000 4055219 65 3 triadimenolcdct c17620000 41120068 37 3 fipronilcdct c13645000 4232809 16 8 procymidonecdct c16310000 435103 74 2 trans chlordanecdct c11202000 444824 78 6 bromophos ethylcdct c10740000 455103 71 9 cis chlordanecdct c11201000 463424 82 6o p ddeo p ddecdct c12040000 47959 98 8alpha alpha endosulfan剧毒 不能提供 4862924 70 3 flumetralincdct c13720000 4960 57 1 dieldrin剧毒 不能提供 5053 19 0o p dddo p dddcdct c12030000 5172 55 9p p ddep p ddecdct c12041000 5272 20 8 endrin剧毒 不能提供 531836 75 5 nitrofencdct c15560000 54122453 73 0 chlorfenapyrcdct c11247500 5572 54 8p p dddp p dddcdct c12031000 56789 02 6o p ddto p ddtcdct c12081000 5733213 65 9beta beta endosulfan剧毒 不能提供 581031 07 8 endosulfan sulfatecdct c13133000 5950 29 3p p ddt p p ddtcdct c12082000 6018181 80 1 bromopropylatecdct c10762000 6182657 04 3 bifenthrincdct c10584000 6239515 41 8 fenpropathrin剧毒 不能提供 6372 43 5 methoxychlorcdct c15060000 642385 85 5 mirexcdct c15270000 6526002 80 2 phenothrincdct c16040000 66101007 06 1 acrinathrincdct c10044000 6768085 85 8 cyhalothrincdfy 52904 6852645 53 1 permethrincdct c15990000 6968359 37 5 cdct c11850000 7052315 07 8 cypermethrincdct c11890000 7170124 77 5 flucythrinatecdct c13700000 7276578 14 8 quizalofop ethyl quizalofop p ethyl cdct c16740000 7351630 58 1 fenvaleratecdct c13630000 7452918 63 5 deltamethrin剧毒 不能提供 75163165 75 1 d5 atrazine d5 cdgg 130983 06 1ml 761189662 83 6 fenthion d6 15 100 2000 6000 wg 2014022101 v1 tel 010 83130651tel 020 38811673tel 0755 26075073tel 027 59812739tel 028 85254001 2tel 025 83737312 83716726 fax 010 83130098fax 020 38811631fax 0755 26075056fax 027 59812738fax fax 025 83701408 cas 4629973 13 5 ethiofencarbcdct c13250000 47563 12 2 ethion 4813194 48 4 ethoprophos 4980844 07 1 etofenproxcdct c13363000 5038260 54 7 etrimfoscdct ca13380000 5122224 92 6 fenamiphos 5231972 44 8 fenamiphos sulfonecdct c13421000 5331972 43 7 fenamiphos sulfoxidecdct c13422000 5460168 88 9 fenarimolcdct c13430000 55114369 43 6 fenbuconazolecdct c13448500 563983 45 7 fenchlorphos oxoncdct c13460500 57111812 58 9 fenpyroximatecddm f248880 500mg 58115 90 2 fensulfothion 596552 21 2 fensulfothion oxoncdct c13570013 606132 17 8 fensulfothion oxon sulfonecdct c13570016 6114255 72 2 fensulfothion sulfonecdct c13570020 6255 38 9 fenthioncdct c13580000 631189662 83 6 fenthion d6 o o dimethyl d6 646552 12 1 fenthion oxoncdct xa13585000cy 6514086 35 2 fenthion oxon sulfonecdct l13585200al 666552 13 2 fenthion oxon sulfoxidecdct l13585400al 673761 42 0 fenthion sulfonecdct c13586000 683761 41 9 fenthion sulfoxidecdct c13586500 6979241 46 6 fluazifop p butyl 7085509 19 9 flusilazolecdct c13860000 7166332 96 5 flutolanilcdct c13863500 72944 22 9 fonofos 7398886 44 3 fosthiazatecdct ca13944500 7465907 30 4 furathiocarbcdct c13970000 7569806 40 2 haloxyfop methylcdct c14062000 7679983 71 4 hexaconazolecdct c14190000 7751235 04 2 hexazinonecdct c14200000 7835554 44 0 imazalilcdct c14280000 79138261 41 3 imidaclopridcdct c14283700 80144171 61 9 indoxacarbcdct c14325500 8136734 19 7 iprodionecdct c14370000 8242509 80 8 isazofoscdct c14377000 8325311 71 1 isofenphos 8499675 03 3 isofenphos methyl 852631 40 5 isoprocarbcdct c14450000 8650512 35 1 isoprothiolanecdct c14467500 871634 78 2 malaoxoncdct c14700000 88121 75 5 malathion cas 892595 54 2 mecarbam 9055814 41 0 mepronilcdct c14890000 9157837 19 1 metalaxylcdct c14920000 9262610 77 9 methacrifoscdct c14970000 9310265 92 6 methamidophos 94950 37 8 methidathion 952032 65 7 methiocarbcdct c15020500 9616752 77 5 methomyl 97161050 58 4 methoxyfenozidecdct l15080500al 9851218 45 2 metolachlorcdct c15170000 991129 41 5 metolcarbcdct l15175000cy 10021087 64 9 metribuzincdct c15200000 1017786 34 7 mevinphos 1022212 67 1 molinatecdct c15280000 1036923 22 4 monocrotophos 10488671 89 0 myclobutanilcdct c15390000 10515299 99 7 napropamidecdct c15480000 10667018 59 1n n desethyl pirimiphos methylcdct ca16270300 1071113 02 6 omethoate 10819666 30 9 oxadiazoncdct c15760000 10977732 09 3 oxadixylcdct c15770000 11023135 22 0 oxamyl 11176738 62 0 paclobutrazolcdct c15840000 112311 45 5 paraoxon ethyl 113950 35 6 paraoxon methyl 1142597 03 7 phenthoate 115298 02 2 phorate 1162600 69 3 phorate oxoncdct xa16085000cy 1172588 06 9 phorate sulfonecdct xa1608550