TitroLine easy滴定仪中文说明书.doc

说明书Titration Unit TitroLine easyC O N T E N T S PAGE 1TitroLine easy滴定仪符合规范介绍.12各配件参数 .23设置和试用 .33.1拆卸和安装 TitroLine easy滴定仪 .33.2安装搅拌器 .33.3安装支架.33.4安装滴定管.43.5安装鼠标和打印机 / 电脑 (PC) (accessories) .53.6连接电极.63.7开关，连接 .63.8键盘 / 显示器 /参比 .64设置之前我们要注意什么?.74.1语言功能设置 .74.2滴定液 (标准液). 74.3清洗和第一次填充 . 74.4填充. 74.5最终值.84.6中和 . 84.7内部方式 .94.8手动滴定 .104.9校准. 104.10还有什么不能被遗忘? . 105TitroLine easy滴定仪滴定 .116TitroLine easy滴定仪校准.127设置 .137.1设置计算公式和输入值 .147.2设置 mV 滴定“ .157.3工作的内部方式 .158RS-232 参数.168.1连接打印机.178.2连接电脑 .178.3命令设置.188.4RS-232 参数 道具.189错误信息 .1910TitroLine easy滴定仪维修.1911替换活塞单元 (拆除和安装).2011.1替换滴定液.20Version 040107 E301Properties of the Titration Unit TitroLine easyNote on disclaimer of liabilityThe measurement or analysis results depend on a multitude of factors. So please verify the plausibility of the measurement or analysis results on a regular basis, accompanied by appropriate reliability tests. In this regard, please adhere to the usual methods.With the Titration Unit TitroLine easy it is possible to perform all common titrations.The most important prerequisite for accurate titration is the accurately functioning dosing technology. In ad- dition to the high-precision glass cylinder made of DURAN borosilicate glass, the virtually play-free spindle ensure correct titration results.All parts coming into contact with the titration and dosing solutions are made of chemically resistant materi- als. Analysis accuracy is guaranteed by the high-precision glass cylinder and the spindle for the piston feed. The controlled three/two-way valve, the easy-to-read consumption display with ist additional status messages, the stand/stirrer system, and the practical manual key button make the Titration Unit Titro- Line easy a device with a comfortable use properties.1.1 Titration solutionsTo save titration solution and to render the disposal of the chemicals after the analysis as simple as possi- ble, we recommend to select any titration-solutions consumption between 5 ml and 15 ml for titration.Solutions to be used:In practice, any solutions and liquids with the viscosity of = 10 mm / s can be used, such as e.g. non aqueous titration (for example perchloric acid in glacial acetic acid). However, chemicals attacking glass, PTFE or FEP, or which are explosive, such as e.g. hydrofluoric acid, sodium acid or bromine must not be used! Suspensions with a high solid contents may block or damage the dosing system.General rules:The respectively applicable safety guidelines on handling chemicals are to be observed under all circum- stances. This applies in particular to inflammable and/or etching liquids.1SCHOTTKONFORMITTSERKLRUNG DECLARATION OF CONFORMITY DCLARATION DE CONFORMITWirerklren in alleiniger Verantwortung, dadas ProduktWe declare under our sole responsibility that the productsNous dclarons sous notre seule responsabilit que le produitTitratorTitration UnitTitrateurTitroLineeasyTitroLineeasyTitroLineeasyauf das sich diese Erkl- rung bezieht, bereinstimmt mit den Normento which this declaration re- lates is in conformity with the standardsauquel se rfre cette dclaration est conforme aux normesDIN EN ISO 8655, Teil 3und mit dem normativenDokumentand the normative documentet au document normatifTechnische Daten Titrator TitroLine easy13. Dezember 2000SCHOTT Instruments GmbHHattenbergstrasse 1055122 MainzDeutschland, Germany, Allemagne07. Januar, January 07th, 07 Janivier 2004AGQSF 0000-A068-01/04010732SCHOTTTranslation of the legally binding German versionTechnical data of the Titration Unit TitroLine easyState December 13, 2000Conformity:DIN EN ISO 8655, Part 5, Conformity markCE mark:according to the Council Directive 89/336/EMC(electromagnetic compatibility);generic emission according to standard EN 50 081, Part 1generic immunity according to standard EN 50 082, Part 2according to the Council Directive 73/23/EMC (low-voltage directive) Country of origin:Made in GermanyPropriety rights:Patents for the valve system and the titration regulation are applied forBurette parts:Cylinder:20 ml DURAN borosilicate glass cylinderUV protection:Protective coating material: Ultem 1000, amberValve: Motor-driven 3/2-way valve made of PTFE/ETFEHoses:FEP with UV protectionDosing accuracy:DIN EN ISO 8655, Part 3, or better typical: systematic error 0,1%random error 5 1012mV 1400 . + 140012 1 digit 5 1012Measuring input:Connection of temperature measuring sensor for Resistance Thermometer Pt 1000, connection: 2 x 4 mm sockets and 1 x 2 mm socket Measuring rangeDisplay resolutionAccuracy*without sensorTC 30 . 1150,10,5 K 1 digit*Accuracy:indicated in terms of measuring incertainty with a confidence of 95 %.In addition the measuring incertainty of the sensor has to be taken in account as well.For instance, it is for pH electrodes: pH = 0.012 . 0.03 according DIN 19 266, Part 3.连接 :电极:DIN 插头 DIN 19 262 或 BNC 参比电极。1 x 4 mm 插头温度. Meas.传感器电阻温度计 Pt 1000: 2 x 4 mm 插座 和 1 x 2 mm 插座搅拌器: TM 96搅拌器低电压的 TM 96 装置在 TitroLine easy滴定仪里 参数 RS-232-C: 连接打印机和电脑 (PC)使用 参数 RS-232-C电源线:符合2级保护认证 DIN EN 61 010, Part 1, 不要在适合危险的环境下进行主体部分: 230 V, 50 / 60 Hz or 115 V, 50 / 60 Hz;更改内部的设置电力: 24 VA缓冲液以 DIN 19 266 和 NBS为标准或者整个PH值pH = 2.00; 4.00; 4.01; 6.87; 7.00; 9.18; 10.00; 12.45显示器:矩形 LCD 64 x 128 像素的显示版,可调节的旋钮( 3.8 键盘 / 显示器)校准:自动校准2到8的缓冲液.2SCHOTTRS-232-C参数:固定设置: 4800波特, 字长 7 位, 2 stop bits, 无奇偶包装材料:Polypropylen 防火保护前部外壳:Polyester外包装的尺寸:135 x 310 x 205 mm (w x h x d), 包括活塞腔体, 不包括搅拌器重量:大约. 2.2 kg使用环境： 温度: + 10 . + 40 C 进行操作和保存湿度依照 EN 61 010, Part 1:最大相对湿度 80 % 在温度在 31 oC以上,减少到50 %以下的相对湿度温度要在40 oC 已注册商标 SCHOTT GLAS, Mainz342Warning and safety informationThe Titration Unit TitroLine easy corresponds to protection class II. It was manufactured and tested accord- ing to DIN EN 61 010, Part 1, Protective Measures for Electronic Measurement Devices and has left the factory in an impeccable condition as concerns safety technology. In order to maintain this condition and to ensure safe operation, the user should observe the notes and warning information contained in the present operating instructions. Development and production is done within a system which meets the requirements laid down in the DIN EN ISO 9001 standard.For reasons of safety, the Titration Unit TitroLine easy must be opened by authorised persons only; this means, for instance, that work on electrical equipment must only be performed by qualified specialists.! In the case of nonobservance of these provisions the Titration Unit TitroLine easy may constitute a danger: electrical accidents of persons or fire hazard. Moreover, in the case of unauthorised in- tervention in the Titration Unit TitroLine easy as well as in the case of negligently or deliberately caused damage, the warranty will become void. Prior to switching the device on it has to be ensured that the operating voltage of the Titration Unit TitroLine easy matches the mains voltage. The operating voltage is indicated on the specification plate. Nonobservance of this provision may result in damage to the Titration Unit TitroLine easy or in personal in- jury or damage to property.If it has to be assumed that safe operation is impossible, the Titration Unit TitroLine easy has to be put out of operation and secured against inadvertent putting to operation. In this case please switch the Titration Unit TitroLine easy off, pull plug of the mains cable out of the mains socket, and remove the Titration Unit TitroLine easy from the place of work.Examples for the assumption that a safe operation is no longer possible, the package is damaged, the Titration Unit TitroLine easy shows visible damages, the Titration Unit TitroLine easy does not function properly, liquid has penetrated into the casing.The Titration Unit TitroLine easy must not be stored or operated in humid rooms.For reasons of safety, the Titration Unit Titroline easy must only be used for the range of application described in the present operating instructions. In the case of deviations from the intended proper use of the device, it is up to the user to evaluate the occurring risks.! The relevant regulations regarding the handling of the substances used have to be observed: The Decree on Hazardous Matters, the Chemicals Act, and the rules and information of the chemicals trade. It has to be ensured on the side of the user that the persons entrusted with the use of the Titration Unit TitroLine easy are experts in the handling of substances used in the environment and in the Titration Unit TitroLine easy, or that they are supervised by specialised persons, respectively.Liquids with a high vapour pressure and/or matters or mixed matters not qualified for use in the technical data of the titration unit must not be used.During all work with titration solutions: ! Please wear protective glasses! !When the piston moves upwards within the cylinder, owing to the design of the system, a microfilm of dos- ing liquid or titration solution will always remain adhered to the inner wall of the cylinder, but this has no influence on the dosing accuracy. This small residue of liquid, however, may evaporate and thus penetrate into the zone underneath the piston, and if inadmitted liquids are being used, the materials of the Titration Unit TitroLine easy may be dissolved or corroded (please refer also to Maintenance and Care).The Titration Unit TitroLine easy is equipped with integrated circuits (EPROMs). X rays or other high- energy radiation may penetrate through the devices casing and delete the program.Please note also the corresponding operating instructions for the devices to be connected.Fig. 2:TitroLine easy滴定仪下面的图试:33安装和试用3.1拆除和安装 Titration Unit TitroLine easy请注意包装里小型的配件.安装 Titration Unit TitroLine easy要在平稳的表面上进行。然后将主线的插头插在插座上., 它可以确保在操作过程中主线的电压符合标准电压. 操作电压简要的说明在 Titration Unit TitroLine easy.底部的说明版上。3.2安装搅拌器将搅拌器插入主机的右下边 然后向后扣紧 ( Fig. 1). 自动连接电源到 Stirrer TM 96.Fig. 1:安装搅拌器插入搅拌器下部的孔和滴定仪的下面扣紧同时向上推搅拌器 TM 96后面直到锁上。Fig. 3:拆除搅拌器:轻轻的揭开锁, 向前推动搅拌器，滴定仪向后移动。.3.3安装支架将 TZ 3665支架插入右侧的孔里 (Fig. 4) 然后将其与 TitroLine easy 滴定仪后面的面版扣紧然后用两个螺丝钉 紧固M 3 x 10 mm (slot-screw driver). 安装电极和滴定管的图为 Fig. 5.Fig. 4Fig. 5滴定管 装备次序:1. 均匀的剪断软管.2. 将固定套管滑动地方连接起来穿在软管上。.3. 将引导管穿过杆状物.4. 挤压滴定管里面的软管底部直接向上推到滴定头5. 按住滴定管里的软管.6. 稳固的拿住管子, 用螺丝连接杆状物和固定套管.杆状物滴定头43.4安装滴定管滴定管是以杆状物为基础加上固定管套连接起来的,然后用软管一串起来.Fig. 6 分解滴定管:Fig. 7 组装滴定管 滴定头固定管套警告: 设备的侧面有两个一样的插座. 如果互相插错了, Titration Unit TitroLine easy 的电极很可能会被损坏。灰色按键53.5安装鼠标和打印机/电脑 (PC)(accessories)紫色按键Fig. 8手动滴定是必须需要鼠标的 它也可以远程控制 (紫键) 和 (灰键)自动滴定。Fig. 9上面的插孔: 鼠标,下面的插孔: 打印机/电脑 (PC).63.6连接电极普通的电极测量线就直接连接到 Electrode“ DIN 插孔. 如果设备是 BNC 插孔,您就要通过提供的说明书来操作 只要将电极的BNC 插头连接到相同的位置就可以。 电极具有完整的温度传感器 (Resistance Thermometer Pt 1000): 电极插头 (DIN or BNC 插头) 插在电极孔里, 依照电极的设计, the Pt 1000 插头直接连接 Pt 1000“ 插孔 也可以插到Ref.“ 的插口。电极指示器 (玻璃电极不是参比电极) 连接 Electrode“孔, 然后将参比电极单独的连接到“REF”的孔里。3.7开关的连接pH 电极温度感应器 2 mm 孔参比电极孔4 mm 温度感应器4 mm 孔鼠标打印机 / 电脑的插口(PC)主开关 (on / off)主线Fig. 10连接后面的面版3.8键盘 / 显示器 /对比Fig. 11:手动键盘键 (accessory)FILL F1CAL F2SET F3F4STARTSTOPTitroLine easy 滴定仪的所有功能是通过键盘来操作控制的. 显示器会显示按键的对话模式. 如果鼠标是以被连接好的 鼠标也可以像 Start/Stop“和 FILL“ 键一样进行运行。通过Titration Unit TitroLine easy.前面底部右侧的一个螺旋钮可以调试显示屏对比度。 F54开始前该注意什么？4.1设置语言滴定仪器设置在EX操作要求的语言下.如果想安装不同的语言设置，可以按住开始菜单中的SET键持续3秒，在菜单中，按F1键选择不同的语言。 = 德语, = 法语, = 英语, = 西班牙语.如果没有选择到你想要设置的语言，可以按STOP键退出菜单。4.2滴定液（标准液体）滴定液是确保在连接滴定过程中将吸管浸入在烧杯中的滴定液里抽出多余的空气。如果 TitroLine easy 滴定仪器刚开始是被充满, the Rinsing/Initial filling“ 运行按照顺序在开始时按相应的按键. 在滴管下放置一个容量最少100ml的容器, 因为滴定液会从这里滴出。.长期驻留在管路的标准液，它的组分会由于空气的影响而发生变化。为了排除以上问题，仪器可以在RINSING AND INITIAL FILLING程序下进行自动润洗。4.3Rinsing and initial filling（润洗和初次填充）在打开开关键, 按 键就可以进入 Rinsing / initi