L02736.doc

ISO/IEC 17025 认可证书 CNAS-PD19/06-A/3 中国合格评定国家认可委员会认 可 证 书 附 件（注册号：CNAS L2306）名称: 中国石油化工股份有限公司中原油田分公司技术监测中心化工产品监测总站 地址：河南省濮阳市中原路125号签发日期：2010年07月09日 有效期至：2013年07月08日更新日期：2011年11月08日附件1 认可的检测能力范围序号检测对象项目/参数领域代码检测标准（方法）名称及编号（含年号）限制范围说明序号名称1水基钻井液1密度0244石油天然气工业钻井液现场测试 第1部分：水基钻井液GB/T 16783.1-20062漏斗粘度02443表观粘度02444塑性粘度02445切力02446滤失量02447pH值02441水基钻井液8液相和固相含量0244石油天然气工业钻井液现场测试 第1部分：水基钻井液GB/T 16783.1-20062石油及 石油产品1凝点0209石油产品凝点测定法GB/T 510-1983（2004）2酸值0209石油产品酸值测定法GB/T 264-1983（2004）3粘度0209石油产品运动粘度测定法和动力粘度 计算法GB/T 265-1988（2004）4水分0209原油含水量测定方法（蒸馏法） GB/T 8929-20065密度0209原油和液体石油产品密度实验室测定法（密度计法）GB/T 1884-2000（2004）6原油有机氯0209原油中有机氯含量测定微库仑计法GB/T 18612-2001（2010）3油田化学剂1表面张力0244表面活性剂 用拉起液膜法测定 表面张力GB/T 5549-20102界面张力0244石油产品油对水界面张力测定法 （圆环法）GB/T 6541-1986（2004）3挥发性有机物液体蒸发残渣量0244有机化工产品试验方法 第2部分:挥发性有机液体水浴上蒸发后干残渣的测定 GB/T 6324.2-2004（2011）3油田化学剂4水不溶物0244化学试剂 水不溶物测定通用方法 GB/T 9738-20085防膨率0244注水用粘土稳定剂性能评价方法SY/T 5971-19946水泥浆密度0244油井水泥实验方法GB/T 19139-2003（2010）7稠化时间 试验02448抗压强度 试验02449静失水试验024410水泥浆稳定性试验024411挥发份0244钻井液用处理剂通用试验方法SY/T 5559-199212水不溶物024413酸不溶物024414pH值024415细度024416密度024417粘度效应024418烧失量0209水泥化学分析方法GB/T 176-200819不溶物020920三氧化硫020921二氧化硅020922三氧化二铁020923三氧化二铝02093油田化学剂24氧化钙0209水泥化学分析方法GB/T 176-2008 25氧化钾和氯化钠020926氧化镁02094油田回注水1水中钙含量0244水质钙的测定EDTA滴定法GB/T 7476-1987（2004）5钻井液用 重晶石粉1部分参数0244钻井液用重晶石粉技术要求：4.1Q/SH 0041-2007不做小于6um颗粒； 仅限于行业内或委托检验钻井液常用加重材料技术规范Q/SH 0282-2009不做小于6um颗粒；仅限于行业内或委托检验钻井液材料规范：3 GB/T 5005-20106钻井液用 铁矿粉1部分参数0244钻井液用铁矿粉技术要求Q/SH 0321-2009不做小于6um颗粒；仅限于行业内或委托检验6钻井液用 铁矿粉1部分参数0244钻井液常用加重材料技术规范：4.2 Q/SH 0282-2009不做小于6um颗粒；仅限于行业内或委托检验钻井液材料规范：4 GB/T 5005-20107钻井液用 造浆用土1全部参数0244钻井液材料规范： 5、7、8、9GB/T 5005-20108钻井液用技术级低粘羧甲基纤维素1全部参数0244钻井液用羧甲基纤维素钠盐技术要求Q/SH 0038-2007仅限于行业内或委托检验钻井液材料规范：10GB/T 5005-20109钻井液用技术级高粘羧甲基纤维素1全部参数0244钻井液用羧甲基纤维素钠盐技术要求Q/SH 0038-2007仅限于行业内或委托检验钻井液材料规范：11 GB/T 5005-201010钻井液用淀粉1全部参数0244钻井液材料规范：12GB/T 5005-201011油井水泥1部分参数0244油井水泥GB 10238-2005不做比表面积12钻井液用磺甲基酚醛树脂1全部参数0244钻井液用磺甲基酚醛树脂技术要求 Q/SH 0042-2007仅限于行业内或委托检验13干粉灭火剂1部分参数0244干粉灭火剂第1部分：BC干粉灭火剂 GB 4066.1-2004（2010）不做 吸湿率、 抗结块性、 粒度分布、 电绝缘性、 喷射性能 、 灭A、B、C类火灾性能干粉灭火剂第2部分：ABC干粉灭火剂 GB 4066.2-2004（2010）14工业用 氢氧化钠1部分参数0244工业用氢氧化钠GB 209-2006不做汞15工业用 合成盐酸1部分参数0244工业用合成盐酸GB 320-2006不做砷16工业碳酸钠1部分参数0244工业碳酸钠及其试验方法 第1部分:工业碳酸钠GB 210.1-2004（2010）工业碳酸钠及其试验方法 第2部分:工业碳酸钠试验方法GB 210.2-2004（2010）不做粒度17工业氢氟酸1部分参数0244工业氢氟酸GB 7744-2008只做类18工业无水 氟化氢1部分参数0244工业无水氟化氢GB 7746-1997（2011）不做水分19阳离子 交换树脂1部分参数02440017强酸性苯乙烯系阳离子交换树脂GB/T 13659-2008不做有效粒径、均一系数、磨后圆球率、粒度分布20氯化钾1部分参数0244氯化钾GB 6549-1996（2011）不做氯化钠 含量21水处理剂 聚丙烯酸1全部参数0244水处理剂聚丙烯酸GB/T 105332000（2011）22聚丙烯酰胺1部分参数0244聚丙烯酰胺GB/T 13940-1992（2011）残留单体含量的测定用溴化法；不做黑点数、粒度23钻井液用包被剂PAC-1411全部参数0244钻井液用包被剂PAC141、降滤失剂PAC142、增粘降滤失剂PAC143技术要求Q/SH 0049-2007仅限于行业内或委托检验24钻井液用包被剂PAC-1421全部参数0244钻井液用包被剂PAC141、降滤失剂PAC142、增粘降滤失剂PAC143技术要求 Q/SH 0049-2007仅限于行业内或委托检验25钻井液用包被剂PAC-1431全部参数0244钻井液用包被剂PAC141、降滤失剂PAC142、增粘降滤失剂PAC143技术要求 Q/SH 0049-2007仅限于行业内或委托检验26钻井液用 增粘剂（80A51）1全部参数0244钻井液用增粘剂（80A51）SY/T 5661199527钻井液用铁铬木质素磺酸盐1全部参数0244钻井液用铁铬木质素磺酸盐 SY/T 5702199528钻井液用磺化褐煤SMC1全部参数0244钻井液用磺化褐煤SMCSY/T 5092200229钻井液用页岩抑制剂改性沥青FT3411全部参数0244钻井液用页岩抑制剂改性沥青 （FT341、FT342）SY/T 5665-199530钻井液用抑制剂改性沥青FT3421全部参数0244钻井液用改性沥青FT342技术要求 Q/SH 0044-2007仅限于行业内或委托检验31钻井液用聚丙烯酰胺钾盐1全部参数0244钻井液用聚丙烯酰胺钾盐技术要求Q/SH 0048-2007仅限于行业内或委托检验32解卡剂1全部参数0244钻井液用解卡剂 SY/T 5659-1993不做破乳电压33钻井液用 褐煤树脂1全部参数0244钻井液用褐煤树脂SY/T 5679-199334钻井液用两性离子聚合物降粘剂XY271全部参数0244钻井液用两性离子聚合物降粘剂 XY27SY/T 5695-199535钻井液用强包被剂FA3671全部参数0244钻井液用两性离子聚合物强包被剂 FA367SY/T 5696-199536油井水泥 减阻剂1全部参数0244油井水泥外加剂评价方法第3部分： 减阻剂SY/T 5504.3-200837油井水泥 降失水剂1全部参数0244油井水泥外加剂评价方法第2部分: 降失水剂SY/T 5504.2-200538油井水泥 缓凝剂1全部参数0244油井水泥外加剂评价方法第1部分： 缓凝剂SY/T 5504.1-200538油井水泥 缓凝剂1全部参数0244油井水泥缓凝剂技术要求 Q/SH 0322-200939原油破乳剂1全部参数0244原油破乳剂通用技术条件SY/T 5280-200040杀菌剂1全部参数0244油田注入水杀菌剂通用技术条件SY/T 5757-20101全部参数0244油田采出水处理用杀菌剂技术要求 Q/SH 0355-201041水处理剂十二烷基二甲基苄基氯化铵1全部参数0244水处理剂十二烷基二甲基苄基氯化铵HG/T 2230-200642采油用 清防蜡剂1部分参数0244采油用清防蜡剂技术要求Q/SH 0052-2007不做防蜡率； 仅限于行业内或委托检验43钻井液用 超细碳酸钙1部分参数0244钻井液用超细碳酸钙技术要求Q/SH 0045-2007不做粒度； 仅限于行业内或委托检验44钻井液用 磺化栲胶1全部参数0244钻井液用磺化栲胶SY/T 5091-199345钻井液用页岩抑制剂KAHm1全部参数0244钻井液用页岩抑制剂KAHMSY/T 5668-199546油田采出水用缓蚀剂1部分参数0244油田采出水用缓蚀剂通用技术条件SY/T 6301-1997不做开口闪点47钻井液用 合成聚合物降滤失剂1全部参数0244钻井液用合成聚合物通用技术条件 Q/SH 1025 0523-2008仅限于 中原油田内 或委托检验48钻井液用合成聚合物增粘剂1全部参数0244钻井液用合成聚合物通用技术条件 Q/SH 1025 0523-2008仅限于 中原油田内 或委托检验49钻井液用 抗盐抗高温降滤失剂1全部参数0244钻井液用抗盐抗高温降滤失剂通用 技术要求 Q/SH 0047-2007仅限于行业内或委托检验50钻井液用两性离子磺甲基酚醛树脂1全部参数0244钻井液用两性离子磺甲基酚醛树脂 Q/SH 1025 0037-2003仅限于 中原油田内 或委托检验51钻井液用 水解聚丙烯腈-铵盐1全部参数0244钻井液用水解聚丙烯腈铵盐技术要求Q/SH 0039-2007仅限于行业内或委托检验52钻井液用沥青1全部参数0244钻井液用磺化沥青技术要求Q/SH 0043-2007仅限于行业内或委托检验2部分参数0244钻井液用沥青类评价方法SY/T 5794-2010不做 电动电位、 软化点3磺基含量0244钻井液用处理剂中磺基含量的测定方法SY/T 5242-199153随钻堵漏剂1全部参数0244SD型随钻堵漏剂Q/ZY 0412-1999仅限于行业中原油田内或委托检验54G502油井水泥膨胀剂1全部参数0244油井水泥气锁膨胀剂通用技术规定 Q/SH 1025 0455-2007仅限于 中原油田内 或委托检验55粘土稳定剂1全部参数0244粘土稳定剂技术要求Q/SH 0053-2010仅限于行业内或委托检验56助排剂1部分参数0244压裂酸化用助排剂技术要求Q/SH 0054-2007仅限于行业内或委托检验；不做界面张力、热稳定性、返排性能 提高率57油井水泥 早强剂1全部参数0244油井水泥早强剂技术要求Q/SH 0320-2009油井水泥早强剂通用技术规定 Q/SH 1025 0176-2004仅限于 中原油田内 或委托检验58油井热洗 添加剂1全部参数0244油井热洗添加剂技术条件Q/SH 1025 0332-2004仅限于 中原油田内 或委托检验59钻井液用聚丙烯酰胺1全部参数0244钻井液用聚丙烯酰胺技术要求Q/SH 0046-2007仅限于行业内或委托检验60钻井液用 降滤失剂1淡水室温中压滤失量0244水基钻井液用降滤失剂评价程序SY/T 5241-1991 （2007）60钻井液用 降滤失剂2淡水高温高压滤失量0244水基钻井液用降滤失剂评价程序SY/T 5241-1991 （2007）34%盐水及饱和盐水室温中压滤失量024444%盐水及饱和盐水高温高压滤失量024461钻井液用 润滑剂1润滑系数0244钻井液用润滑剂评价程序SY/T 6094-199462钻井液用 页岩抑制剂1膨胀率0244钻井液用页岩抑制剂评价方法SY/T 6335-19971全部参数0244钻井液用页岩抑制剂技术要求Q/SH 0323-200963钻井液用 絮凝剂1絮凝时间0244钻井液用絮凝剂评价程序SY/T 5233-199164钻井液用 消泡剂1密度恢复率0244钻井液用消泡剂评价程序SY/T 5560-19921全部参数0244钻井液用消泡剂技术要求Q/SH 0324-200965钻井液用聚合物降粘剂1全部参数0244钻井液用聚合物降粘剂技术要求 Q/SH 0318-200966钻井液用 聚合物类包被絮凝剂1全部参数0244钻井液用聚合物类包被絮凝剂技术要求 Q/SH 0319-2009No. CNAS L2306 第 15 页 共 39 页 The scope of the accreditation in Chinese remains the definitive version.ISO/IEC 17025 认可证书 CNAS-PD19/06-A/3 CHINA NATIONAL ACCREDITATION SERVICE FOR CONFORMITY ASSESSMENTAPPENDIX OF ACCREDITATION CERTIFICATE(Registration No. CNAS L2306) NAME: Chemical Product Inspection Station of Technical Inspection Center, Zhongyuan Oilfield Branch of SINOPEC ADDRESS: No.125, Zhongyuan Road, Puyang, Henan, ChinaDate of Issue: 2010-07-09 Date of Expiry: 2013-07-08Date of Update：2011-11-08APPENDIX 1 SCOPE OF ACCREDITED TESTINGTest ObjectItem/ParameterCode of Field Title, Code of Standard or Method Limitation NoteItem/ Parameter1Water-based fluids1density0244Petroleum and natural gas industries-Field testing of drilling fluidsPart 1:Water-based fluidsGB/T 16783.1-20062funnel viscosity02443apparent viscosity02444plastic viscosity02445shearing force02446filtration02447PH value02441Water-based fluids8The liquid and solid contain0244Petroleum and natural gas industries-Field testing of drilling fluidsPart 1:Water-based fluidsGB/T 16783.1-20062Crude oil and petroleum products1Solidifying point0209Petroleum products-Determination of solidification pointGB/T 510-1983（2004）2Acid value0209Petroleum products-Determination of acid numberGB/T 264-1983（2004）2Crude oil and petroleum products3viscosity0209Petroleum products-Determination of kinematic viscosity and calculation of dynamic viscosityGB/T 265-1988（2004）4moisture content0209Crude petroleum Determination of water-Distillation methodGB/T 8929-20062Crude oil and petroleum products5Density0209Crude petroleum and liquid petroleum products Laboratory determination of density-Hydrometer methodGB/T 1884-2000（2004）6Determination of organic chloride content in crude oil0209Determination of organic chloride content in crude oil by combustion and microcoulometryGB/T 18612-2001（2010）3Chemical of oil field1Surface tension0244Surface active agents-Determination of surface tension by drawing up liquid filmsGB/T 5549-20102interfacial tension0244Petroleum products Mineral oils Determination of interfacial tension of oil against water-Ring methodGB/T 6541-1986（2004）3Chemical of oil field3Dry residue after evaporation for volatile organic liquids0244Test method of organic chemical products-Part 2:Determination of dry residue after evaporation on a water bath for volatile organic liquidsGB/T 6324.2-2004（2011）4Water insoluble matter0244Chemical reagent - General method for the determination of water insoluble matterGB/T 9738-20085Anti-expansion rate0244Evaluation of clay inhibitors for water injectionSY/T 5971-19946slurry density0244Procedure for testing well cementsGB/T 19139-2003（2010）7thickening time02448compression strength02449Static Filtration02443Chemical of oil field10Stability of Cement Slurry0244Procedure for testing well cementsGB/T 19139-2003（2010）11Volatile Matter0244General test methods for additives used in drilling fluidsSY/T 5559-199212Water insoluble matter024413Acid insoluble matter02443Chemical of oil field14pH value0244General test methods for additives used in drilling fluidsSY/T 5559-199215Fineness024416density024417Viscosity Effect024418Loss on ignition0209Methods for chemical analysis of cementGB/T 176-200819insoluble substance020920sulfur trioxide02093Chemical of oil field21silicon dioxide0209Methods for chemical analysis of cementGB/T 176-2008 22ferric oxide020923aluminium sesquioxide020924calcium oxide0209Methods for chemical analysis of cement GB/T 176-200825potassium chloride and sodium chloride020926magnesium oxide02094Oilfield reinjection water1Content of calcium in water0244Water quality-Determination of calcium-EDTA titrimetric methodGB/T7476-1987（2004）5Barite powder for drilling fluids1Part parameter0244Technical specifications of the Barite powder for drilling fluids: 4.1Q/SH 0041-2007Except for less than 6m particle Restricted in Sinopec or entrusted inspection5Barite powder for drilling fluids1Part parameter0244The Specifications of general use drilling fluid weight materialQ/SH 0282-2009Except for less than 6m particle Restricted in Sinopec or entrusted inspection Specifications of drilling fluid materials: 3GB/T 5005-20106Hematite for drilling fluids1Part parameter0244Technical specifications of hematite for drilling fluidsQ/SH 0321-2009Except for less than 6m particle ;Restricted in Sinopec or entrusted inspectionThe Specifications of general use drilling fluid weight material Q/SH 0282-2009Except for less than 6m particle ;Restricted in Sinopec or entrusted inspectionSpecifications of drilling fluid materialsGB/T 5005-20107Bentonite for drilling fluid1All parameter0244Specifications of drilling fluid materialsBentonite for drilling-chapter 5、OCMA bentonite-chapter 7、Palygorskite-chapter 8、Sepiolite-chapter 9GB/T 5005-20108Low viscosity Sodium carboxymethylcellulose for drilling fluid1All parameter0244Technological requirements of sodium carboxymethyl cellulose for drilling fluidQ/SH 0038-2007Restricted in Sinopec or entrusted inspectionSpecifications of drilling fluid materials:10GB/T 5005-20109High viscosity Sodium carboxymethylcellulose for drilling fluid1All parameter0244Technological requirements of Sodium carboxymethyl cellulose for drilling fluidQ/SH 0038-2007Restricted in Sinopec or entrusted inspectionSpecifications of drilling fluid materials:11GB/T 5005-201010Starch for drilling fluid1All parameter0244Specifications of drilling fluid materials:12GB/T 5005-201011Oil well cement1Part parameter0244Oil well cementGB 10238-2005Except for specific surface area12Sulfonated methyl pheuo-formaldehyde used in drilling fluids1All parameter0244Technological requirements of sulfonated methypheuo formald-ehyde used in drilling fluidsQ/SH 0042-2007Restricted in Sinopec or entrusted inspection13Fire extinguishing media1Part parameter0244 Extinguishing powder-Part 1：BC powder GB 4066.1-2004（2010）Except for moisture rate、Resist the lumping、particle size distribution、The electrical insulation、Spray performance、extinguish A、B、Cfire performanceExtinguishing powderPart 2：ABC powderGB 4066.2-2004（2010）14Sodium hydroxide for industrial use1Part parameter0244Sodium hydroxide for industrial useGB 209-2006Except for Hydrargyrum15Synthetic hydrochloric for industrial use1Part parameter0244Synthetic hydrochloric acid for industrial useGB 320-2006Except for Arsenic16Industrial sodium carbonate1Part parameter0244Specification and determination methods of sodium carbonate for industrial usePart 1:Sodium carbonate for industrial useGB 210.1-2004（2010） Specification and determintion methods of sodium carbonate for industrial usePart 2:specification and determintion methodsGB 210.2-2004（2010）Except for particle size distribution17Hydrofluoric acid for industrial use1Part parameter0244Hydrofluoric acid for Industrial useGB 7744-2008Accredited Only for 18Anhydrous hydrogen fluoride for industrial use1Part parameter0244Anhydrous hydrogen fluoride for industrial useGB 7746-1997（2011）Except for moisture content19Cation exchange resin1Part parameter02440017 Strong acid polystyrene cation exchange resinGB/T 13659-2008Except for Effective particle diameter、Uniform coefficient、Round ball rate after whetting、distribution of particle size20Potassium chloride1Part parameter0244Potassium chlorideGB 6549-1996（2011）Except for the content of sodium chloride21Water treatment chemical-polyacrylic acid1All parameter0244Water treatment chemicals-Polyacrylic acidGB/T 105332000（2011）22Polyacrylamide1Part parameter0244PolyacrylamideGB/T 13940-1992（2011）The determination of residual monomer content （bromation procedure）;Except for freckle、particle size23Encapsulating agent PAC141 used in drilling fluids1All parameter0244Technical requirements of encapsulating agent PAC141 and fluid loss reducers PAC142/PAC143 used in drilling fluidsQ/SH 0049-2007Accredited only for Restricted in Sinopec or entrusted inspection24Encapsulating agent PAC142 used in drilling fluids1All parameter0244Technical requirements of encapsulating agent PAC141 and fluid loss reducers PAC142/PAC143 used in drilling fluidsQ/SH 0049-2007Accredited only for Restricted in Sinopec or entrusted inspection25Encapsulating agent PAC143 used in drilling fluids1All parameter0244Technical requirements of encapsulating agent PAC141 and fluid loss reducers PAC142/PAC143 used in drilling fluidsQ/SH 0049-2007Accredited only for Restricted in Sinopec or entrusted inspection26Viscosifier used in drilling fluids（80A51）1All parameter0244Viscosifier used in drilling fluids (80A51)SY/T 5661199527Feerochromo lignosulfonate used in drilling fluids1All parameter0244Feerochromo lignosulfonate used in drilling fluidsSY/T 5702199528Sulfonated lignite for drilling fluid(SMC)1All parameter0244Sulfonated lignite for drilling fluid(SMC)SY/T 5092200229Modified asphalts FT341/FT342 u