第三批国产催化剂生产装置运行情况

1、R-101生产装置运行情况（2010.国产第三批催化剂.一期运行）日期1.291.301.312.12.22.32.4反应器负荷（kg/h）640640/6406401013温度147.7147.8138.4140.6140.6149.8149.51014温度146.1146.1140.3142.6143.2148.7148.41015温度143.2143.2139.7141.9142.2145.6145.21018温度139.5139.5138.4140.8140.8141.6141.5AAL产量（吨）FI-2520/19.2426.5631.1353.0758.5645.19气相O22.8

2、74.230.390.440.455.725.37CO215.1329.861.701.381.3832.7427.85C3H635.9740.198.892.320.6726.5337.96液相油相ACR0.020.050.14/0.270.10AAC5.2463.4369.20/19.5560.47AAL5.770.260.32/10.110.73HOAC35.7021.7320.78/31.5623.02HACR/H2O53.1612.6011.55/37.9615.01水相AAC/AAL/HOAC/HACR/H2O/备注11:55投氧，负荷640 kg/hLV-9610表有问题，造成T

3、-211蒸汽波动,停车（23:00）20:16投氧开车R-101生产装置运行情况（国产催化剂）日期2.52.62.72.82.92.102.11反应器负荷（kg/h）6406406406407507507501013温度149.6149.8149.6149.9149.6151.4150.91014温度148.5148.8148.6148.9150.4150.9150.91015温度145.1145.5145.1145.4146.4146.9146.81018温度141.5141.9141.5141.5143.1143.1143.0AAL产量（吨）FI-252044.6148.4346.9457

4、.7257.9862.8061.83气相O25.525.575.155.756.476.856.87CO222.1928.0529.9030.4429.4328.5027.76C3H636.7538.4236.8036.4541.1340.0838.60液相油相ACR0.240.160.110.130.190.170.18AAC48.6246.6344.3748.3753.6455.4655.16AAL1.690.991.231.620.482.162.39HOAC26.9327.1429.5728.4224.2124.7025.07HACR/H2O21.6024.8324.3821.0519

5、.9016.5916.47水相AAC11.4811.42AAL0.160.17HOAC30.4727.59HACR/H2O57.5860.57备注8:05提负荷至750.14:09降负荷至700，14:40恢复至750R-101生产装置运行情况（国产催化剂）日期2.122.132.142.152.162.172.18反应器负荷（kg/h）7507507507508608608601013温度151.5151.4151.5154.7153.9153.5153.41014温度150.9150.8150.9153.7155.5155.5155.41015温度146.9146.8146.7149.91

6、51.4151.6151.41018温度143.0142.6142.8146.0148.0148.0148.1AAL产量（吨）FI-252067.0964.6366.5169.3877.9272.9973.54气相O26.696.736.836.916.446.446.47CO231.6829.7427.9828.9631.5428.3930.67C3H638.2138.3341.2638.2438.2939.4738.76液相油相ACR0.120.140.130.120.110.120.13AAC56.3658.9260.6557.9262.3862.5064.56AAL2.320.102.

7、402.302.280.151.83HOAC21.7024.3922.0123.0721.7921.4019.98HACR/H2O18.9514.4814.1616.0612.5314.1612.80水相AAC10.759.01AAL0.200.10HOAC26.8128.09HACR/H2O62.0562.63备注2:30左右T-211蒸汽波动，O2浓度急度上升，临时降负荷，1h后正常8:15开始提负荷，9:30至860kg/hR-101生产装置运行情况（国产催化剂）日期2.192.202.212.222.232.242.25反应器负荷（kg/h）8608608608609509509501

8、013温度153.3153.6153.5157.5157.4157.6157.51014温度155.5155.4155.4159.6159.7159.7159.91015温度151.5151.3151.3155.9155.9155.9156.01018温度148.1148.2148.1151.7151.7151.7151.8AAL产量（吨）FI-252076.2377.7676.3176.7883.983.7381.01气相O26.566.876.736.086.046.076.04CO229.2128.4430.5929.1028.3228.7428.46C3H638.9938.4938.7

9、439.0038.5338.1338.12液相油相ACR0.120.090.120.120.090.030.11AAC62.7655.8659.4364.8564.2764.1862.99AAL2.011.700.261.331.491.381.39HOAC21.5724.8223.4519.1721.4621.6421.67HACR/H2O12.6017.0615.1714.0212.0912.0213.16水相AAC8.7911.25AAL0.120.16HOAC21.0127.94HACR/H2O69.8560.42备注8:23开始提负荷，8:53至970kg/hR-101生产装置运行情

10、况（国产催化剂）日期2.262.272.283.13.23.33.4反应器负荷（kg/h）9509509509501050105010501013温度157.5157.6158.0160.8161.5161.5161.41014温度159.8159.9160.1162.7163.4163.3163.31015温度155.8156156.2159.1160.4160.4160.31018温度151.6151.8151.9154.1154.8155.0154.9AAL产量（吨）FI-252083.9982.3582.2183.4491.9292.2590.62气相O26.185.976.216.0

11、45.825.866.00CO227.8329.1127.7028.9730.6230.7931.07C3H639.2737.4139.1337.6939.3639.5838.42液相油相ACR0.130.110.150.120.220.160.20AAC66.6965.2365.9767.5669.9620.0165.72AAL1.251.201.141.070.891.001.02HOAC19.8520.7820.6719.0416.8817.4819.80HACR/H2O11.2411.9211.4111.5311.2410.5212.56水相AAC8.718.92AAL0.140.06

12、HOAC26.8523.66HACR/H2O64.1267.15备注8：00开始提负荷，9：00提到1050kg/hR-101生产装置运行情况（国产催化剂）日期3.53.63.73.83.93.103.11反应器负荷（kg/h）10501050105010501050105010501013温度161.5161.6162.0162.8162.6163.0164.21014温度163.5163.7163.9164.5164.6164.7166.01015温度160.3160.8161.0161.4161.7161.9163.21018温度154.9155.1155.3155.8155.9156.

13、3157.3AAL产量（吨）FI-252089.8390.8789.4988.9891.4788.7490.87气相O26.216.286.136.406.236.266.25CO230.2728.7929.9831.6027.4627.3129.05C3H637.9140.2239.0737.2939.4140.2039.73液相油相ACR0.160.150.150.160.150.200.17AAC68.4070.4968.9769.0471.0872.1166.86AAL0.990.930.950.970.900.780.81HOAC18.5917.1717.9716.3817.5416

14、.2720.10HACR/H2O10.9610.3611.1012.469.489.7911.26水相AAC8.716.55AAL0.070.20HOAC23.3721.49HACR/H2O67.5871.62备注R-101生产装置运行情况（国产催化剂）日期3.123.133.143.153.163.173.18反应器负荷（kg/h）10501050105010501050105010501013温度164.5164.4164.2164.6165.5166.0166.21014温度166.5166.4166.4166.8167.4168.1168.21015温度163.8163.8163.61

15、64.0165.0165.1165.61018温度157.7157.6157.5157.8158.8159.0159.3AAL产量（吨）FI-252090.4190.1988.2390.9591.3191.6687.79气相O2 6.196.196.326.366.296.076.21CO229.25 30.4330.1129.8030.4929.4629.87C3H640.2639.2439.4640.5040.1041.1239.21液相油相ACR0.150.150.140.120.170.13AAC70.8371.7170.8572.4865.8170.11AAL0.670.800.76

16、0.730.740.77HOAC16.9216.3417.0616.2917.7916.83HACR/H2O10.6710.0610.329.6012.1511.26水相AAC7.977.56AAL0.040.04HOAC21.0420.78HACR/H2O70.6671.38备注R-101生产装置运行情况（国产催化剂）日期3.193.203.213.223.233.243.25反应器负荷（kg/h）10501050105010501050105010501013温度166.0166.5167.1167.3168.4168.3168.81014温度168.1168.5169.3169.5170

17、.7170.6171.11015温度165.5166.0166.7167.0168.3168.4168.91018温度159.0159.6160.2160.6161.6161.5161.9AAL产量（吨）FI-252091.1687.8290.7388.790.0692.987.89气相O26.296.266.286.366.296.196.28CO230.0329.9731.1739.6930.2130.3230.57C3H638.2139.8038.9230.4341.0340.5540.96液相油相ACR0.130.12AAC71.4674.09AAL0.800.67HOAC17.011

18、4.14HACR/H2O9.7510.13水相AACAALHOACHACRH2O备注R-101生产装置运行情况（国产催化剂）日期3.263.273.283.293.303.314.1反应器负荷（kg/h）10501050105010501050105010501013温度169.4169.8170.1170.1170.3170.8171.21014温度171.8172.4172.5172.6173.0173.4173.91015温度169.6170.0170.5170.6170.9171.4171.91018温度162.7163.0163.3163.2163.7164.2164.6AAL产量（

19、吨）FI-252091.4188.389.5889.9988.2288.5389.36气相O26.306.236.276.186.266.226.38CO230.0031.5328.6931.1129.5930.8530.21C3H641.4038.1240.4040.2041.3841.3141.10液相油相ACR0.170.120.130.140.150.110.11AAC71.3571.6569.1971.7773.3173.5369.12AAL1.010.810.770.820.630.680.71HOAC17.0517.1816.3816.3115.5715.5615.74HACR/

20、H2O9.759.4812.6710.089.749.3813.64水相AAC7.107.39AAL0.030.03HOAC20.0522.67HACR/H2O69.6169.68备注R-101生产装置运行情况（国产催化剂）日期4.24.34.44.54.64.74.8反应器负荷（kg/h）10501050105010501050105010501013温度171.6171.9172.3172.7173.4173.6174.11014温度174.4174.7175.1175.7176.4176.6177.21015温度172.8173173.3174.0175.3175.8176.41018温

21、度165.1165.4165.9166.3167.0167.3167.8AAL产量（吨）FI-252086.9789.4589.0286.9888.0988.6088.05气相O26.236.266.376.286.226.346.36CO231.0531.3032.0530.5631.1432.2531.17C3H639.2739.8540.1841.1839.3239.9840.25液相油相ACR0.150.130.110.180.130.170.12AAC72.0674.7373.0671.6175.4174.0173.31AAL0.770.660.690.830.720.710.72H

22、OAC16.3914.5215.9517.1213.6515.3015.51HACR/H2O9.709.169.689.659.209.049.50水相AAC8.978.51AAL0.450.04HOAC20.4817.52HACR/H2O69.9873.69备注R-101生产装置运行情况（国产催化剂）日期4.94.104.114.124.134.144.15反应器负荷（kg/h）10501050105010501000100010001013温度174.5175.4175.5176.0176.4175.9176.51014温度177.6178.4178.6179.3179.8179.2179

23、.71015温度177.0178.3178.6179.5180.1179.5180.51018温度168.3169.3169.6170.2170.9170.4171.2AAL产量（吨）FI-252087.3187.6488.0785.6985.2984.8283.48气相O26.306.186.376.376.166.476.44CO231.3832.4331.5231.9131.4932.5331.99C3H641.8040.5041.4341.4742.2141.0941.71液相油相ACR0.160.130.140.120.120.150.21AAC69.6574.0371.0373.8

24、373.0472.4772.76AAL0.700.820.790.780.680.840.91HOAC15.0214.8316.2415.1214.5816.2715.73HACR/H2O13.749.2510.839.3510.779.259.42水相AAC5.7313.61AAL0.130.05HOAC18.0112.50HACR/H2O76.0273.58备注8:00负荷降至1000 kg/hR-101生产装置运行情况（国产催化剂）日期4.164.174.184.194.204.214.22反应器负荷（kg/h）1000100010001000100010009101013温度176.4

25、177.0177.7178.1178.8179.9178.11014温度179.8180.5180.6181.2181.6182.5180.91015温度180.6181.8182.5183.3184.0185.6184.01018温度171.3172172.9173.5174.3175.8174.4AAL产量（吨）FI-252082.4383.8283.9181.2381.2579.1373.58气相O26.476.556.496.496.496.346.74CO232.7133.0132.7933.7232.1732.7132.11C3H641.8841.4940.9440.7040.64

26、43.0043.42液相油相ACR0.140.120.150.150.110.130.15AAC71.9872.9974.873.3368.8970.1770.78AAL0.920.900.881.041.080.811.10HOAC17.1416.3814.4215.0018.2517.4016.36HACR/H2O8.839.048.889.5110.8310.8910.72水相AAC7.405.82AAL0.300.38HOAC20.2418.59HACR/H2O71.9075.10备注10:41负荷降至910 kg/hR-101生产装置运行情况（国产催化剂）日期4.234.244.25

27、4.264.274.284.29反应器负荷（kg/h）9109109109108608608601013温度178.5179.1179.6180.6179.5180.4180.91014温度181.1181.3181.7182.7181.6182.2182.51015温度184.8185.8186.6188.3187.6188.8189.81018温度175.0175.7176.5177.8177.1178.1178.7AAL产量（吨）FI-252074.8572.3973.0971.7773.0470.6671.39气相O26.786.736.786.806.927.067.02CO232.

28、3733.9233.4035.6932.6833.9333.83C3H643.2941.4043.9144.0442.5742.8643.75液相油相ACR0.150.150.150.180.230.140.16AAC72.2070.2672.7474.4872.4169.9768.38AAL1.081.151.230.901.161.101.11HOAC15.8416.2915.3213.4615.4715.8519.72HACR/H2O9.8511.269.4810.009.249.149.80水相AAC6.176.32AAL0.420.47HOAC16.5617.24HACR/H2O76

29、.7375.85备注10:45开始降负荷，11：00降至860kg/hR-101生产装置运行情况（国产催化剂）日期4.305.15.25.35.45.55.6反应器负荷（kg/h）8608608608608607507501013温度182.0182.4179.0182.9184.8184.1184.21014温度183.5183.6180.9184.6186.4185.9185.81015温度191.2191.9180.5193.2195.5193.6194.31018温度180.0180.0179.7181.4183.3182.9183.0AAL产量（吨）FI-252070.3134.7431.458.655.5565.7874.09气相O26.997.007.077.077.006.697.27CO232.7133.2423.2135.2136.5931.733.21C3H643.5943.3546.5842.6540.5741.