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专业英语词汇总结Section1生药部分中药研究现状及中药现代化一、加强中国药用植物基础研究及其与中药现代化的联系/StrengtheningbasicresearchesonChineseMedicinalPlantsanditsrelationstorealizingthemodernizationofCMM记载berecorded来源derivedfrom中医药TraditionalChineseMedicine,shortforTCM卫生事业healthcare,healthundertakings中草药Chinesetraditionalmedicinalherbs疗效reliabletherapeuticaleffectstherapeutic[,θer?'pju:t?k]adj.治疗(学)的;疗法的;对身心健康有益的副作用side-effectsl中医药的健康理念和临床医疗模式体现了现代医学的发展趋势。Thehealthconceptandclinicalpracticereflectthetrendofmodernscience新的科学技术潮流(thenewtideofscienceandtechnology)二、中药资源及其研究成果/ChineseMedicinalPlantresourcesandachievementofitsscientificresearch中药资源(medicinalplantresources)普查(surveys)专项研究(specialprojects)药用植物资源(theChinesemedicinalresources)科学鉴定(scientificidentification)化学成分(chemicalconstituents)药理实验(pharmacologicalexperiments临床适应症(clinicalapplications)研究(projects)新著作(newworks)各论(monographs)手册(manuals)《中国药典》Thepharmacopoeiaofthepeople’sRepublicofChina药典Pharmacopoeia药用植物学PharmaceuticalBotany本草学Herbology中药学TheChineseMateriaMedica药用植物分类学PharmaceuticalPlantTaxonomy植物化学Phytochemistry植物化学分类学PlantChemotaxonomy药用植物志FloraofMedicinalPlant中药药剂学traditionalChinesePharmaceutics中药炮制学ScienceofprocessingChineseCrudeDrugs中药鉴定学IdentificationofTraditionalChineseMedicine中药药理学PharmacologyofTraditionalChineseMedicines青蒿素artemisin奎宁quinine、氯奎宁chloroquine衍生物derivatives氯奎宁耐受性疟疾chloroquineresistantmalaria急性疟疾perniciousmalaria脑部疟疾cerebralmalaria显著疗效markedeffectchloroquineresistantmalaria/抗氯喹啉疟疾Pernicious(有害的)malaria/急性疟疾cerebralmalaria/脑疟疾derivatives/衍生物quinine/喹啉含有氮原子的化合物,在英文命名中多以-ine结尾Mono-/一Di-/二Tri-/三Tetra-/四Petan-/五Hexa-/六Hepta-/七Octa-/八Nona-/九Deca-/十三尖杉酯碱harringtonine、高三尖杉酯碱homoharringtonine白血病leukemia和恶性淋巴瘤malignantlymphoma银杏黄酮ginkgetin丹参酮tanshinonIIA治疗冠心病coronaryheartdiseasesNewdrugdevelopments/新药开发Healthproducts/保健品质量控制Qualitycontrol修订revise常用中药common-usedChinesemateriamedica国家标准thenationalstandards三、中药所面临的挑战/ChineseMedicinalHerbsFacingaChallenge中成药及其制剂traditionalChinesepatentmedicinesandpreparations基础研究basicresearches生产production、流通marketing研究researchIdentificationofspecies/品种鉴定鉴定和鉴别identifyingandclarifying变种varieties伪品falsematters。益胃benefitthestomach、生津promotetheproductionofbodyfluid、清热removetheexcessiveheat不同属differentgenera种species伪品fakes假货adulterationsQualitycontrolandevaluation/质量的控制和评价大量的努力intensiveeffort重金属heavymetalcontent农药残留pesticideresidueTheChinaPharmacopoeia/中国药典qualitativeandquantitativeanalysis/定性定量分析TLC/ThinLayerChromatographyHPLC/HighPerformanceLiquidChromatographyqualityspecificationandevaluation/质量规范与评价3.Themethodsofresearch/研究手段Botany/植物学Biology/生物学biotechnology/生物技术molecularbiology/分子生物学四、中药现代化的规划/ProgramsonModernizationofCMMseedqualitystandards/种子质量标准cultivationtechniquerules/栽培技术规范productionofpollution-freeandgreenmedicinalmaterials/无污染,绿色processingrulesandregulations质量标准criteria草案protocolApplymoderncomprehensivemultidisciplinarystudiesonChinesemedicinalplants/将先进应用型多学科技术应用到药用植物研究中。DNAfingerprintingandsequencing/DNA指纹谱及其基因序列advancedanalyzers/先进的分析仪器exploitasigle-itemactivecomponent/单一活性成分theintegratedandharmonizingeffectsofmanydifferentcomponentsinaplant/同一植物中多个成分的综合协调作用complexprescription/复杂的处方EstablishinformationsystemsinmodernresearchofChinesemedicinalherbs/建立现代药用植物的全息系统TomodernizaeCMMneedsmoderninformationtechnology/中药现代化需要现代信息技术activeingredients/活性物质pharmacologicalaction/药理功效traditionalandmoderntherapeuticalindication/古老和现代的适应症TERMINOLOGY细胞壁cellwall初生壁primarywall次生壁secondarywall细胞核nucleus质体plastid叶绿体chloroplast染色体chromoplast纹孔pit结晶体crystal淀粉粒starchgranule脐点hilum层纹striation单粒singlestarchgranule复粒compoundstarchgranule半复粒semi-compoundstarchgranule蛋白质protein类脂化合物lipid挥发油volatileoil精油essentialoil苷glycoside生物碱alkaloid皂苷saponin萜terpene三萜皂苷triterpenoid黄酮flavonoid醌quinone蒽醌anthraquinone酚phenol香豆素coumarin木脂素lignan鞣质tannin肽peptide酶enzyme内酯lectone有机酸organicacid单糖monosaccharide低聚糖oligosaccharide多糖polysaccharide菊糖inulin树脂resin甾醇sterol维生素vitamin抗菌素antibiotic草酸钙结晶calciumoxalatecrystal簇晶clustercrystal针晶needle组织tissue基本组织groundtissue薄壁组织parenchyma薄壁细胞parenchymatouscell表皮组织epidermaltissue表皮细胞epidermalcell气孔stoma保卫细胞guardcell副卫细胞subsidiarycell非腺毛non-glandularhai腺毛glandularhair腺鳞glandularscale周皮periderm木栓层cork木栓形成层corkcambium(phellogen)栓内层phelloderm皮层cortex皮孔lentical油管vitta油室oilcavity纤维fibre韧皮纤维phloemfibre木纤维xylemfibre晶鞘纤维crystalfibre石细胞stonecell纹孔pit纹孔道pitcanal层纹striation木化lignified导管vessel环纹导管annularvessel螺纹导管spiralvessel梯纹导管scalariformvessel网纹导管reticulatedvessel孔纹导管pittedvessel具缘纹孔导管borderedpittedvessel维管束vascularbundle外韧维管束collateralbundle形成层cambiumring主根mainroot须根fibrousroot细根rootlet块根tuberousroot中柱stele初生木质primaryxylem初生韧皮部primaryphloem髓部pith射线ray木栓形成层corkcombium次生木质secondaryxylemRadixPolygoniMultiflori(何首乌)FleeceflowerRootperennialtwiningherb多年生的缠绕草本herbaceous草质的Leavesalternate叶互生petiole:叶柄blade叶片cordate心形的ocrea托叶鞘membranous膜质的terminal:顶生axillary:腋生panicles:圆锥花序perianth:花被achene:瘦果persisting宿存的fusiform纺锥形的横断面transverseelongatedsection横切面:transversesection纵切面:longitudinalsectionlenticel-likeprotrusions:皮孔样凸起starchy:粉性的viscous:粘性的horny:角质样fracture使折断;破碎abnormalvascularbundles异形维管束brocadedpatterns云锦样花纹subroundedring类圆形的环scatteredwith散在collateraltype外韧型clustersofcalciumoxalate草酸钙簇晶starchgranules淀粉粒ammoniaTS氨试液saturatedsolutionofantimonytrichlorideinchloroform三氯化锑的氯仿饱和溶液黄芪AstragaliRadix[EnglishName]MilkvetchRootodd-pinnatelycompound:奇数羽状复叶pinnae:小叶,由拉丁语转变而来,复数stipule:托叶lanceolate:披针形的racemes:总状花序calyx:花萼campanulate:钟状的corolla:花冠standard:旗瓣wing:翼瓣keel:龙骨瓣diadelphous:二体雄蕊stalked:柄furrow:皱纹cork:木栓层exfoliate:脱落cortex:皮部reticulate:网状的tenacious:粘性的striation:纹理fissure:裂隙tenacious:粘性的striation:纹理fissure:裂隙phelloderm栓内层collenchymatouscells厚角细胞sievetubegroups筛管群parenchymatouscells薄壁细胞lignified木质化primarywalls:初生壁tassel:穗borderedpittedvessels:具缘纹孔导管referencesolution对照品溶液10%sulfuricacidinethanol10%的硫酸乙醇溶液Correspondvi.相符合,相一致;相当,相类似;通信sodiumhydroxide:NaOHhydrochloricacid:HClanhydrous:无水的甘草GlycyrrhizaeRadixetRhizoma[EnglishName]LiquoriceRootharmonize:调和mollify:缓和pubescences:软毛,绒毛,到达青春期;glandular:腺体的racemes:总状花序stamens:雄蕊calyx:花萼ovary:子房corolla:花冠style:花柱legume:荚果prickly:多刺的calcareousglasslands:钙质草原ventilated:通风的bales:大包,捆furrows:沟纹sparse:稀疏的cleft:裂隙;budscars:芽痕;pith:髓stout[staut]adj.粗壮的;结实的;坚固的;坚定的;勇敢的;(指人)肥胖的lignifiedfibres:木化纤维glycyrrhizicacid甘草酸glycyamarin甘草苦苷丹参SalviaeMiltiorrhizaeRadixetRhizomaDanshenrootvermillion:朱红色serrate:锯齿状的verticillate:轮生angled:棱pseudo-:假的retuse:浅凹形falcate:钩状的filament:花丝style:花柱anther:花粉囊gynobasic:着生于基部的racemes总状花絮apex顶端fragile:脆的astringent:收敛性的dissolvedonmountinginchloralhydratesolutionferricchloride:三氯化铁TS:testsolutiondull:暗的astopperedtesttube:具塞试管standfor:静置residue:残渣referencedrug:对照药材CRS:ChemicalReferenceStandardusingsilicagelGasthecoatingsubstanceandamixtureofbenzene-ethylacetate(19:1)asthemobilephase用硅胶G作为固定相,苯-乙酸乙酯的混合溶液(19:1)作为展开剂甲苯(toluene)clearheart-fireandremoverestlessness.养心安神usingsilicagelGasthecoatingsubstanceandamixtureofbenzene-ethylacetate(19:1)asthemobilephase用硅胶G作为固定相,苯-乙酸乙酯的混合溶液(19:1)作为展开剂六味地黄丸Liuweidihuangwanpulverize:研磨sift:评审,过筛makepills:泛丸cleft:裂缝hyphae:菌丝epidermal:表皮的pericarp:果皮beadedanticlinalwalls:垂周壁连珠状增厚kieselguhr:硅藻土triturate:研匀paeonol:丹皮酚cyclohexane:环己烷ferricchloride:三氯化铁hydrochloricacid:盐酸distil:蒸馏volumetricflask:容量瓶spectrophotometry:分光光度法disintegrate/溶解;grind/成粉末;Soxhelt’sextractor/索氏提取器macerate:浸软decant:倒出absoluteethanol:无水乙醇ursolicacid:熊果酸formicacid:甲酸integrationvalues:吸光度值Thebluish-brownspotinthechromatogramobtainedwiththetestsolutioncorrespondsinpositionandcolourtothespotinthechromatogramobtainedwiththereferencesolution.供试品色谱中,在与对照品色谱相应的位置上,日光下显相同的棕褐色斑点usingsilicagelGasthecoatingsubstanceandamixtureofcyclohexane-chloroform-ethylacetate-formicacid(20:5:8:0.1)asthemobilephase分别点于同一硅胶G薄层板上,以溶液为展开剂10%solutionofsulfuricacidinethanol.Heatat105℃for5~7minutestothespotsclear10%的硫酸乙醇溶液,在105℃加热5~7分钟至斑点显色清晰。thinlayerchromatographicscanningmethodSection2天然药化部分PaperChromatography(PC)chromatographyn.色谱法,层析法chromatographicadj.色谱法的,色谱仪的chromatogramn.色谱,色谱图(谱)chromatographn.色谱仪v.用色谱法分析partitioncoefficientn.分配系数retardationfactor:Rfvaluen.比移值fluorescencen.荧光dissociationn.离解parameter(n)(限定性的)因素,特性,界限;〈物〉〈数〉参量,参数separation:分离、分析filterpaper:滤纸medium:介质、媒介;培养基、媒介物reproducibility:可重现性,再生性Rfvalue:比移值retardationfactor(Rf)compound:化合物constituent成分、构成component成分、组成的、构成的anthocyanins:花色素苷,花青苷pigments:色素、颜料、染料partition:n.分割,分配v.分割,分裂,划分partitionchromatography分配色谱adsorptionchromatography吸附色谱water-immiscible水不溶性的alcoholic醇的,乙醇的,酒精的alcoholn.酒精,乙醇solventn.溶剂n-butanoln.正丁醇n:normal正(链)的iso:isotropic异,各向同性的,同t:tertiary特,叔,第三isopropanoln.异丙醇t-butanol叔丁醇BAW:n-butanol-aceticacid-water4:1:5(上层)正丁醇-醋酸-水aqueous:水的,水溶性的versatile:通用的,万能的,多用途的,多方面的purines:嘌呤pyrimidines:嘧啶phenolic:酚性的glycoside:苷,配糖物['glaik?said]glycose单糖glycosidase糖苷酶['glaik?usideis]glycosidation糖苷化glycosyl糖基['glaik?sil]horizontalPC:水平纸色谱circularPC:环形纸色谱TLC:ThinLayerChromatography薄层色谱resolution:分辨率carotenoids:类胡萝卜素,类叶红素descendingPC:下行纸色谱法descendingdevelopment下行展开法ascendingdevelopment上行法two-dimensionaldevelopment二维分离over-run:过度展开cellulose:纤维素silicicacid:硅酸silicagel:硅胶silicon:硅siliconeoil:硅油alumina:[?'lju:min?]氧化铝,矾土lipids:脂,类脂paraffin:石蜡油,煤油['p?r?fin]reversed-phasechromatography:反相色谱milligram:毫deci(分)dm,centi(厘)cm,milli(毫)mm,mg,mlmicro(微)μm,μg,μlnano(纳)nm,ngUV-fluorescent:紫外荧光UV:ultraviolet紫外fluorescent:荧光chromogenicreagent:显色剂chromogenic发色的发色体的diffusion:扩散developthecolors:显色developingagent(solvent)/tank/time展开溶剂/缸/时间developmentagent/rate/system/solution展开溶剂/速度/系统/液solventfront:溶剂前沿origin:原点fraction:分数;部分,馏份structurallyrelated:结构相关性的1.2薄层色谱ThinLayerChromatography(TLC)TLC:thinlayerchromatography薄层色谱sensitivity:n.灵敏度adsorbent:吸附剂(物质)a.能吸附的adsorption:n.吸附(作用)silicagel:硅胶celite:n.硅藻土ionexchangeresin:离子交换树脂polyamide:聚酰胺Sephadex:葡聚糖凝胶polyvinylpyrrolidone:聚乙烯吡咯烷酮polyvinyl:n.a.聚乙烯基化合物(的)pyrrolidone:吡咯烷酮aluminium铝calcium钙calciumhydroxide:氢氧化钙calciumchloride:氯化钙calciumoxide:氧化钙calciumphosphate:磷酸钙calciumsulphate:硫酸钙magnesium镁sodium钠spreadingglassplates:铺板automaticspreadingdevices:自动铺板器acetone:丙酮petroleumether:石油醚ether:乙醚chloroform:氯仿ethylacetate:乙酸乙酯methanol:甲醇ethanol:乙醇butanol:正丁醇grease:n.油脂(状物)slurry:n.浆,泥浆hemihydrate:半水合物airdried:a.风干的,晾干的activated:a.活化的,活性的,激活的inorganicsalt:无机盐inorganic:a.无机的,无生物的organic:a.有机的,有机体的inorganicacid/chemistry无机酸/无机化学organicacid/solvent/chemistry有机酸/有机溶剂/有机化学silvernitrate硝酸银nitrate硝酸根precoatedplates:预制板aluminiumsheets:铝片fluorescentindicator:荧光指示剂quenchthefluorescence:荧光淬灭wavelength:波长microparticlesofsilica:硅胶微粒HPLC:highperformanceliquidchromatography高效液相色谱HPTLC:highperformancethinlayerchromatography高效薄层色谱solventsystem:溶剂系统referencecompounds:参照(对照)化合物paper-lined:衬上滤纸saturated:a.饱和的HorizontalTLC:水平薄层色谱over-run:过度展开electrophoresis:电泳byspraying:喷雾,喷洗conc.H2SO4:浓硫酸sulphuricacid:硫酸nitricacid:硝酸hydrochloricacid:盐酸detectionreagent:检测试剂steroids:甾体,甾族类化合物steroidal:a.甾族的sterol:n.甾醇,固醇preparativeTLC:制备薄层色谱adsorbent:n.吸附剂eluting:洗脱elute:v.洗脱(提),流出elution:n.洗脱,流出,淋洗bufferelution缓冲洗脱gradientelution梯度洗脱isocraticelution等度(无梯度)洗脱eluant:n.洗脱(提)液,展开剂eluate:n.洗脱液,提取液(物)centrifuging:离心(centrifuge)1.3高效液相色谱HighPerformanceLiquidChromatography(HPLC)GLC:气相色谱Gasliquidchromatographysensitivity:灵敏度、灵敏性quantitative:定量的qualitative:定性的linearityandlimitofdetection(LOD)线性和检测限precision(精密度)reproducibility(重复性)recovery(加样回收率)stability(稳定性)bond:键,结合bonded:键合的,化合的stationaryphase:固定相C18orODS;C8;silicagel;Sephadex;ionexchangeresin;octadecylsilylsilicagelmobilephase:流动相misciblesolventmixture:可互溶的混合溶剂methanol,acetonitrile(乙腈)distilledwateraceticacidphosphoricacid(磷酸)buffersalt(缓冲盐)polymer:聚合物polymerase聚合酶hydrolase水解酶polymerization聚合作用decomposition分解作用isocraticelution:等度洗脱gradientelution:梯度洗脱elute:洗脱,流出,流出物eluting:洗脱,流出elution:洗脱,流出elutiontime/volume/program/systemdetector:检测器UVD:ultraviolet-visibledetector(紫外可见吸收检测器)PDAD:photodiodearraydetector(光电二极管阵列检测器)RID:refractiveindexdetector(示差折光检测器)FD:fluorescencedetector(荧光检测器)ECD:electrochemicaldetector(电化学检测器)ELSD:evaporativelight-scatteringdetector(蒸发光散射检测器)atambienttemperature常温,室温,环境温度besubjectedto:使遭受,使属于,可能thermalre-arrangement:热重排thermostaticallycontrolledjacket:温度控制护套coated:被包裹的,覆盖的precoated:预制的poisoning:污染,毒害impurities:杂质,不纯物purify:纯化,精练putification:精制,纯化plantextracts:植物提取物extract:v.提取,萃取,抽提n.提取液,萃取液,浸膏extractant:提取剂,萃取剂extraction:提取(法),萃取(法)extractive:n.提取物,浸出物,浸出制剂a.抽提的,浸出的non-volatile:非挥发性的spectrum:n.光谱,波谱,谱refractiveindexdetector:示差折光检测器terpenoids:萜类化合物terpene:萜,萜烯terpane:萜烷alkaloids:生物碱carbohydrates:碳水化合物flavonoids:黄酮类化合物coumarins:香豆素quinone:醌-----benzoquinone苯醌naphthoquinone萘醌anthraquinone蒽醌steroids:甾体类化合物lignanoid:木脂素prepackedcolumns:预填充柱-----prepacked:预先装入的silicamicroporousparticlecolumn:硅胶微孔粒柱non-polarcompounds:非极性化合物polarcompounds:极性化合物ultrapure:超纯------ultra:超,过,越,极端,异常degas:脱气chromatographictechnique:色谱技术phytochemist’s:植物化学家的;phytochemistry:植物化学armoury:装备,武器库,军械库quantitative:定量的separationsonapreparativescale:制备分离Spectralidentification光谱鉴定1,Ultraviolet-Visible(UV-VIS)spectroscopy紫外-可见吸收光谱Electromagneticspectrum电磁波Infrared红外Visiblelight可见光Wavenumber波数Proportionaltoenergy与能量成正比Violetlight紫外线Conjugateddiene共轭二烯Absorptionmaxima最大吸收峰Absorptionpeak吸收峰AbsorbanceA吸收值AItsconcentrationinsolution溶液浓度Molarabsorptivity摩尔吸收系数Literaturereference参考文献Thestructuralinformation结构信息2,infraredspectroscopy红外光谱Nmrspectroscopy核磁共振光谱Spectroscopicmethods光谱(仪器)方法Functionalgroup官能团Electromagneticspectrum电磁波光谱Microwaves微波Reciprocalcentimeters厘米的倒数Beinverselyproportionalto与。。。。。。成反比Electromagneticradiation电磁波辐射Vibrationalenergystates振动能级状态Photon光子Methylene亚甲基Fingerprints指纹Hexane己烷Carbon-hydrogenstretchingvibrations碳-氢伸缩振动Sodiumchloride氯化钠Vibrationccharacteristic振动特征Patternofpeaks峰形Frequencies频率3,massspectroscopy质谱Molecule分子Bombardedwithhigh-energyelectrons高能电子轰击Electron-volts电子伏特Collidewith与。。。。。碰撞Dislodge转移;电离Ionized使离子化Electronimpact电子轰击Positivelycharged带正电Oddnumberofelectrons奇数电子Cationradica正离子lImpart传递Dissipate消耗Neutralfragment中性碎片Fragmentation分裂Ionizationandfragmentation电离和裂解Electron-impactmassspectrometer电子轰击质谱分光仪Schematic示意图Molecularion分子离子Magnet磁铁Originaltrajectory起始轨道Mass/charge质/荷比Magneticfieldstrength磁场强度Beinterfacedwith连用,连接Bargraph棒图Relativeintensity相对丰度Benzene苯4,protonnuclearmagneticresonance(1H-NMR)1H核磁共振谱Coincidewith与。。。。。。。相一致Downfield低场Thesignalduetotheproton氢信号Chemicalshifts化学位移Chemicalshiftfortheprotoninchloroform氯仿中氢的化学位移Nuclearspin核自旋Irrespectiveof不考虑5,常见有机化合物结构类型Acetaldehyde乙醛Aceticacid乙酸Aceticanhydride乙酸酐Acetone丙酮Acetonitrile乙腈Acetylchloride乙酰氯Acidanhydrides酸酐Acylhalides酰卤化合物Alcohols醇类Aldehydes醛类Alkanes烷烃Alkenes烯烃Alkenylhalides卤代烯烃Alkylhalides卤代烷Alkynes炔烃Amides酰胺类Amines胺类Arenes芳香烃Arylhalides卤代炔烃Benzene苯Carboxylicacids羧酸类Chlorobenzene氯苯Chloroethane氯乙烷Chloroethene氯乙烯Dienes二烯烃Diethylether乙醚Epoxides环氧化合物Epoxyethane环氧乙烷Ester酯类Ethane乙烯Ethers醚类Ethyne乙炔Ketones酮类Nitriles腈类Nitrocompounds硝基化合物Nitrobenzene硝基苯Phenol苯酚Phenols酚类6,Appendix3.4AlkaloidsfromOriciopsisglaberrimaEngl.(Rutaceae)stem茎干bark树皮roomtemperature室温agar琼脂chromatographic色谱法的methyl甲基methylene亚甲基methine次甲基carbonyls羰基vibration振动,摆动hydroxyl羟基methine次甲基carbonyl羰基alkaloid生物碱skeleton骨架trisubstituted三取代的benzenering苯环hydroxyl羟基hydroxyl,dimethyl,chroman色原酮units骨架,片段lowfield低场deshieldedby去屏蔽phenolichydroxyl酚羟基chromatographic结晶,晶体reacted起反应phenolic酚的hydroxyl羟基acridone吖啶酮skeleton骨架chelated螯合的hydroxyl羟基protons质子resonances共振aromatic芬芳的substituted取代的,代替的pyranring吡喃环cross-peaks相关峰(此词易错翻译成交叉峰)Angular角的acridone吖啶酮hydroxylsignal羟基信号correlations相关性dihydro二氢的Nitrogen氮medicinalplant药用植物Infections传染病Hypotension血压过低Dermatitis皮炎Phytochemical植物化学的Furoquinoline呋喃喹啉Alkaloid生物碱Elucidation说明,阐明Antimicrobial抗菌的optical光学的rotations旋转polarimeter旋光计偏振器spectrometer分光计HRMS高分辨质谱仪fraction部分eluted洗脱silicagelcolumn硅胶柱hexane–EtOAc正己烷-乙酸乙酯Bacteria细菌Fungi真菌fungi培养皿algae藻类,海藻roomtemperature室温diameter直径Section3药典相关内容一、药材来源1.植(动)物来源的药材的来源部分的一般译法为:药材英文名称isthe药用部位(名词单数)of植(动)物拉丁学名[属名和种(变种)加词为斜体字](科名).例:PummeloPeelisthedriedunripeoralmostripeexocarpofCitrusgrandis“Tomentosa”orCitrusgrandis(L.)Osbeck(Fam.Rutaceae).本品为芸香科植物化州柚Citrusgrandi“Tomentosa”或柚Citrusgrandis(L.)Osbeck的未成熟或近成熟的干燥外层果皮。2.药材的采收与产地加工部分的一般译法为:用Thedrug作主语,单数。用被动语态,不用主动语态。“采收”用“tobecollected”(不用“tobepicked”,“tobedugup”等)。“除去杂质”等(名词单数)用“removedfromforeignmatter”,“洗净”用“washedclean”,“干燥”用“dried”,“晒干”为“driedinthesun”,“阴干”为“driedintheshade”,“低温干燥”为“driedatalowertemperature”。“栽培变种”为“cultivar”。“泥砂”为“soil”。“须根.细根”:“fibrousroot”用于单子叶植物、根茎上的不定根,“rootlet”用于双子叶植物主根上的细小侧根、支根。例1Thedrugiscollectedinautumn,removedfromforeignmatter,washedclean,anddriedinthesun.例2Thedrugiscollectedatfloweringtofruitingstage,removedfromthickstem,cutintosection,anddried.(注:中国药典2005年版一部英文版药用部位采用名词单数,如stem,leaf,fibrousroot,rootlet等).二、理化鉴别1.化学鉴别Shake0.5gofthepowderwith5mlofethanolfor5minutesandfilter.Evaporatethefiltratetodryness,adddropwiseantimonytrichloridesaturationsolutioninchloroformandevaporateagaintodryness.Aviolet-redcolourisproduced.取本品粉末0.5g,加乙醇5ml,振摇5分钟,滤过,滤液蒸干,滴加三氯化锑饱和的三氯甲烷溶液,再蒸干,即显紫红色。2.薄层鉴别(1)经常用到需统一的词汇和短语:a.超声处理用ultrasonicateb.提取用extractc.温浸用warmmacerated.水浴加热用heatonawaterbathe.对照品(对照品溶液)用“对照品名”加“CRS”表示(referencesolution);对照药材(对照药材溶液)用referencedrug(referencedrugsolution);供试品溶液用testsolutionf.薄层板:硅胶G薄层板...usingsilicagelGasthecoatingsubstance用1%氢氧化钠溶液制备的硅胶G薄层板...usingsilicagelGmixedwith1%solutionofsodiumhydroxideasthecoatingsubstance含4%醋酸钠的羧甲基纤维素钠溶液为黏合剂的硅胶G薄层板上...usingsilicagelGmixedwithsodiumcarboxymethylcellulosecontaining4%solutionofsodiumacetateasthecoatingsubstance.g.斑点用spot(s),条斑用band(s)h.分别置日光及紫外光灯(365nm)下检视,日光下显…色的斑点;紫外光灯下显…色的斑点用…spotindaylightand…spotunderultravioletlightat365nmrespectively.(2)薄层鉴别基本的四个步骤,即供试品溶液制备;对照品溶液制备;点样、展开、显色;结果判断。a.供试品溶液制备常见以下几种情况:超声处理提取To9g,cutintopieces,add20mlofether,ultrasonicatefor20minutes,andfilter.Evaporatethefiltratetodryness,anddissolvetheresiduein0.5mlofn-hexaneasthetestsolution.取本品9g,切碎,加乙醚20ml,超声处理20分钟,滤过,滤液挥干,残渣加0.5ml正己烷溶解,作为供试品溶液。(艾附暖宫丸)加热回流提取Heatunderreflux2g,cutintopieces,with20mlofethanolfor1hour,coolandfilter,usethefiltrateasthetestsolution.取本品2g,剪碎,加乙醇20ml,加热回流1小时,放冷,滤过,滤液作为供试品溶液。萃取、过柱纯化Extractthefiltratewithtwo15-mlquantitiesofn-butanolsaturatedwithwater,combinethen-butanolextracts,andevaporatetodryness.Dissolvetheresiduein1mlofdehydratedethanol,addaquantityofalumina,stirwellonawaterbath,dry,andapplytoasmall(10-15mmindiameter)或SepackC18columnpackedwithneutralalumina(200mesh,1g,10~15mmindiameter),pre-elutewith30mlofamixtureofethylacetateandmethanol(3:1).Elutewith30mlofamixtureofethylacetateandmethanol(1:1),andcollecttheeluate.Evaporatetodrynessanddissolvetheresiduein0.5mlofethanolasthetestsolution.滤液用水饱和的正丁醇提取二次,合并正丁醇提取液,蒸干,残渣加无水乙醇1ml使溶解,加适量氧化铝在水浴上拌匀,干燥,装入一预先装填好的中性氧化铝小柱(200目,1g,内径10-15mm)或C18小柱上,用乙酸乙酯-甲醇(3:1)30ml预洗,再用乙酸乙酯-甲醇(1:1)30ml洗脱,收集洗脱液,残渣加乙醇0.5ml使溶解,作为供试品溶液。浸渍、水解Macerate0.5gofthepillsin20mlofmethanolfor1hour,andfilter.Evaporate5mlofthefiltratetodryness,dissolvetheresiduein10mlofwater,add1mlofhydrochloricacid,heatonawaterbathfor30minutes,andcoolimmediately.取本品0.5g,加甲醇20ml浸泡1小时,滤过。取5ml滤液蒸干,残渣加10ml水溶解,加1ml盐酸,水浴加热30分钟,立即冷却。b.对照品(对照药材)溶液的制备化学对照品作对照DissolvechlorogenicacidCRSinmethanoltoproduceasolutioncontaining1mgpermlasthereferencesolution.取绿原酸对照品,加甲醇溶解制成每1ml含1mg的溶液,作为对照品溶液。多个化学对照品混合对照DissolveginsenosidesRb1,ReandRg1CRSinmethanoltoproduceamixturecontaining2mgofeachpermlasthereferencesolution.对照药材作对照Prepareasolutionof0.5gofRheiRadixetRhizomareferencedrugand20mlofmethanolinthesamemannerasthereferencedrugsolution.另取大黄对照药材0.5g,加甲醇20ml,同法制成对照药材溶液。c.点样、展开、显色、检视点样、展开Carryoutthemethodforthinlayerchromatography(AppendixVIB),usingsilicagelGasthecoatingsubstanceandtheupperlayerofamixtureofbutylacetate,formicacidandwater(7:2.5:2.5)asthemobilephase.Applyseparately10μlofthetestsolutionand2μlofthereferencesolutiontotheplate.照薄层色谱法(附录ⅥB)试验,吸取供试品溶液10μl,对照品溶液2μl,分别点于同一硅胶G薄层板上,以醋酸丁酯-甲酸-水(7:2.5:2.5)为展开剂,展开,.......。显色、检视Spraywith5%sulfuricacidinethanolandheattothespotclear.Examineunderultravioletlightat365nm.以5%硫酸乙醇溶液显色,热风加热至斑点显色清晰。置紫外光灯(365nm)下检视。d.结果判断Thefluorescentspotsinthechroma
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