普通化学实验授课纲要

1、普通化學實驗授課綱要授課節次:第_1_週上課課程主題: Introduction講授目的: 1. Laboratory safety2. Cleaning apparatus3. The knowledge of operation of chemical instruments at laboratory4. Familiarize with the lab授課綱要:1. General Safety Rules2. Classifications for hazardous Materials and Wastes3. Chemical waste disposal4. Online Ma

2、terial Safety Data Sheets (MSDS)5. Proper laboratory clothing6. Safety Equipment in the lab: fume hood, safety shower, eyewash, fire blanketetc. 7. Emergency Procedures8. Data Analysis and Lab Reports9. Lab tour 普通化學實驗授課綱要授課節次:第_2_週上課課程主題: Calibration of thermometer & Melting Point apparatus講授目的: Ca

3、librate a thermometer and determine the melting point of an unknown substance with a melting point determination apparatus授課綱要:(請條列該堂課之授課大綱內容)1. Definition of melting point and boiling point2. Thermometer calibration for use in cold process and products (ice water method)3. Simple distillation appar

4、atus4. Boiling point of water with relationship to altitude5. Melting point determination apparatus and method6. Experiment protocol7. Problem-solving practice普通化學實驗授課綱要授課節次:第_3_週上課課程主題:Chromatography(I) : PPC(Paper Partition Chromatography )講授目的: Paper Chromatography, Analysis the ion mixture授課綱要:(

5、請條列該堂課之授課大綱內容)1. Paper Chromatography2. Stationary Phase3. Mobile Phase4. Retention Factor (RF) Determination5. Purpose6. Procedure7. Develpomenting8. Identification of the ions9. Questions普通化學實驗授課綱要授課節次:第_4_週上課課程主題: Chromatography(II) : TLC(Thin Layer Chromatography )講授目的: Identity of a compound in

6、 a mixture授課綱要:(請條列該堂課之授課大綱內容)1. Introduction2. TLC Adsorbent3. TLC Solvents or Solvent Systems4. Interactions of the Compound and the Adsorbent5. The Rf value6. Advanced TLCFluore-coating TLC7. Two-dimensional TLC8. Purpose9. Procedure10. Trouble shooting TLC11. Questions普通化學實驗授課綱要授課節次:第_5_週上課課程主題:

7、 Titration of acids & bases: volumetric analysis講授目的:Back titration, titration curve, determine pH value, prepare an acid-base indicator from anthocyanin授課綱要:(請條列該堂課之授課大綱內容)1. Basic concept of acid and base2. Titration curve3. Back titration4. Acid-base indicator5. Graduated pipette, volumetric flas

8、k, burette, electric balance, pH meter6. Analysis of stomach antacid tablets7. Prepare an acid-base indicator from anthocyanin8. Experimental protocol9. Problem-solving practice普通化學實驗授課綱要授課節次:第_6_週上課課程主題: Chemical oxygen demand (COD) of polluted water講授目的: Determine COD of polluted water 授課綱要:(請條列該堂

9、課之授課大綱內容)1. Introduction of water pollution2. Determination of water pollution3. Chemical oxygen demand (COD)4. Oxidation-Reduction Titration5. Primary standard6. Titration: standardization of potassium permanganate (KMnO4)7. Reflux8. Experimental protocol9. Problem-solving practice普通化學實驗授課綱要授課節次:第_

10、7_週上課課程主題: Chemical equilibrium講授目的: Determine Equilibrium constant, spectrophotometer授課綱要:(請條列該堂課之授課大綱內容)1. Equilibrium Chemical Reaction2. Concentration of reactants and products at equilibrium.3. LeChateliers Principle4. Equilibrium constants, Kc5. Beers Law6. Use of a spectrophotometer for color

11、imetric assays7. Preparation of standard solutions8. Linear regression9. Experimental protocol10. Problem-solving practice普通化學實驗授課綱要授課節次:第_8_週上課課程主題: Chemical kinetics講授目的: To determine the order of a reactant in the rate expression for a chemical reaction, use of micropipette.授課綱要:(請條列該堂課之授課大綱內容)1.

12、 Initial reaction rate2. Iodine clock reaction3. Method of initial rates 4. Determine the order of a reactant5. Use of micropipette6. Experimental protocol7. Problem-solving practice8. Data analysis普通化學實驗授課綱要授課節次:第_9_週上課課程主題: Chromatography(III) : IEC (Ion Exchange Chromatography) 講授目的: The ion-exch

13、ange chromatography process allows the separation of ions and polar molecules based on the electrical properties of the molecules.授課綱要:(請條列該堂課之授課大綱內容)1. Major classifications of chromatography 2. Ion exchange chromatography Cation exchange resin Anion exchange resin 3. Column Packing 4. Column Washi

14、ng 5. Sample applying 6. Sample elution 7. 普通化學實驗授課綱要授課節次:第_10_週上課課程主題:Clinical chemistry: plasma protein concentration determination講授目的: Determining protein concentrations , BCA Protein Assay 授課綱要:(請條列該堂課之授課大綱內容)1. The methods available rely on absorption spectroscopy and fall into two general cat

15、egories, which depend on different chromophores:Natural chromophores present in proteins:UV SpectroscopyChemical reactions of proteins that produce chromophores for Spectrophotometric analysis:Biuret ReactionLowry assayBCA assayBradford assay2. BCA Protein assay3. BCA structure4. BCA and protein rea

16、ction5. Experimental Protocol6. Data Analysis8. Principle of Spectroscopy9. Principle of centrifuge and application普通化學實驗授課綱要授課節次:第_11_週上課課程主題: Colloidal suspensions講授目的:Preparation and characteristics of colloidal suspensions授課綱要:(請條列該堂課之授課大綱內容)1. Basic principles of the colloid science2. Special p

17、roperties of disperse phases3. Stability of disperse systems4. Coagulation5. Experimental protocol6. Problem-solving practice普通化學實驗授課綱要授課節次:第_12_週上課課程主題:Preparation of soaps; Preparation of hand sanitizing gel講授目的: To learn the surfactant agent, saponification and polymers for pharmaceutical applica

18、tions授課綱要:(請條列該堂課之授課大綱內容)1. Whats surfactant agent?a. Define of surfactants b. Surfactants structurec. Classification of surfactantsd. Properties of Surfactantse. Surfactants Functionsf. Application of surfactants2. Saponification.a. What is the saponification?b. In the process of making soap, anima

19、l fat, which is a fatty acid, is hydrolyzed by the action of a strong base, such as sodium hydroxide, and heat.c. Saponification valued. Lye calculatione. Reflux apparatusf. Salting out g. Making soap raw materials h. Procedurei. Problem-Solving Practice3. Polymers for Pharmaceutical Applicationsa.

20、Typical Properties of Carbopol Polymersb. Rheology modifier, Viscosity Modifierc. Protective Colloids - viscous agent d. Making sanitizing gel raw materials e. Proceduref. Problem-Solving Practice普通化學實驗授課綱要授課節次:第_13_週上課課程主題:Preparation of Shampoo & face cream講授目的: To learn the emulsion, emulsifier and synthetic detergent授課綱要:(請條列該堂課之授課大綱內容)1. Preparation of Shampoo a.