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DearEditorandReviewers:
Onbehalfofmyco-authors,weareverygratefultoyouforgivingusanopportunitytoreviseourmanuscript.weappreciateyouverymuchforyourpositiveandconstructivecommentsandsuggestionsonourmanuscriptentitled“ThermalProcessandMechanismofPhaseTransitionandDetoxificationofGlass-ceramicsfromAsbestosTailings”(ID:NOC-D-18-01200).
Wehavestudiedreviewers’commentscarefullyandtriedourbesttoreviseourmanuscriptaccordingtothecomments.ThefollowingaretheresponsesandrevisionsIhavemadeinresponsetothereviewers'questionsandsuggestionsonanitem-by-itembasis.Thanksagaintothehardworkoftheeditorandreviewer!
ResponsetothecommentsofReviewer#1
CommentNo.1:Pagenumbershouldbeincludedinthemanuscript.
Response:ThankstoReviewerforreminder,weaddedthepagenumbertothemanuscript.
CommentNo.2:Isitdifferentialthermalanalysisordifferentialscanningcalorimetry?(Abstract)
Response:Thecrystallizationandphasechangeofthesampleswereinvestigatedbythermogravimetry-differentialscanningcalorimetry(TG-DSC),andtheresultswereshowninfigure2.
CommentNo.3:Pleaseclarify:"Asbestostailingsaretailingsproducedduringtheminingandbeneficiationofchrysotile(fibridasbestos)"GiventhefactthatchrysotileiscarcinogenicpleaseincludeintheIntroductionpartsomeaspectsabouthealthregulations/concernstotakecareduringsynthesisofchrysotilecontainingmaterials.Forinstance,whichisthesafety/allowedthresholdforchrysotilecontentinbuildingmaterials?(Introduction)
Response:ItisreallytrueasReviewermentionedthatduetothehazardsofchrysotile,theuseofchrysotilecontainingmaterialshavebeenbannedcompletelyinmanycountries,andfortherecyclingofchrysotilecontainingmaterials,therearesomelegalrestrictionswhichIhaveaddedtothesectionofIntroduction.Therearesomesafetyhazardsinthesynthesisanduseofasbestos-containingmaterialsinevitably,howeverthisconcerndoesn'texistinourexperiment,becausethesamplespreparedintheexperimentarecompletelyfreeofasbestos,whichisexplainedintheresponsetoReviewer#2below.
CommentNo.4:Magnificationwithin1000-500rangeincludedintheexperimentalpart,butx5000magnificationismetinFigs6.(Experimentalcharacterization)
Response:Weareverysorryforournegligenceofmistakenlywritingthemagnificationrangeas500-1000intheexperimentalcharacterization,actuallythemagnificationrangeis500-5000.
ResponsetothecommentsofReviewer#2
CommentNo.1:Manuscriptdealswithtransformationofunhealthychrysotile(serpentine)intoforsteriteand/orenstatite-containingmaterialsfordecorativebuildingpurposes.However,chrysotilecontentoftheobtainedmaterialsshouldbethoroughlycontrolled.
Response:Thankyouforyourvaluablecomment,itisdefinitelyacriticalissuethatchrysotilecontentoftheobtainedmaterials(glass-ceramics)shouldbethoroughlycontrolled.Actually,thechrysotileinserpentinestartsat600℃andcompletelyremoveshydroxylat700℃resultingthedecompositionoforiginalmineralsandthedisintegrationofstructure,andformharmlesssubstancesincludingamorphoussilicaandforsterite.Sointheexperiment,thefiberstructurechrysotilecanbecompletelydestroyedafterpre-firingat700℃.Furthermore,inthethermaltreatmentofcrystallizationandsinteringathighertemperatures,theresiduethathasnotbeencompletelydecomposedcanbefurtherdecomposedandtotallyconvertedintoharmlessphasesincludingforsterite,enstatite,etc.bysolidphasereactionandsolid-liquidreaction.Ultimately,theproductwasentirelyasbestos-freeandwhichcanbeseenfromthemorphologyofthesamplesinfigure6.
ResponsetothecommentsofReviewer#3
CommentNo.1:GivesomereferenceforthechemicalcontentofAsbestostailingsforthebenefitofthereader.(Introduction)
Response:AsReviewersuggestedthatitisindeedbettertogivesomereferenceforthechemicalcontentofAsbestostailings.Tworeference(reference2andreference3)wereaddedtoconfirmthechemicalcontentandphasecompositionofasbestostailings.
CommentNo.2:Howdoyoudistinguishbetweenthemaincrystalphaseandthesubcrystallinephase?
Response:wearesorrythatwemayhavenotexpresseditclearly,theword“subcrystalline”usedinmymanuscriptmaybenotaccurate.Ithinkitwouldbesuitabletochangeittotheword“minor”.ThecontentofdifferentcrystalphasesinthesampleweredeterminedbyrietveldrefinementusingGSAS,andtheresultsareshownbelow(withtheweightfractionofforsteritebeing39.44%,enstatite24.92%,diopside21.18%andmagnesioferrite14.45%respectively).Accordingtotheresult,itcanbeseenthatthemaincrystalphasesareforsteriteandenstatite,andtheminorphasesarediopsideandmagnesioferrite.
Fig1.Rietveldrefinementofthesamplecrystallizedat850℃andsinteredat1200℃
Table1.QualityofRefinementAnalysis
Rwp(%)
Rp(%)
Rexp(%)
GOF
8.61
6.32
8.44
1.02
CommentNo.3:Englishha
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