sgs食品安全测试foodgradepresentation.ppt

1、Ivan C.K. Chan 10 August 2004,It is governed under French Decret 92-631 It is identical to EU requirement 89/109/EEC 89/109/EEC Material and Article in contact with food Regulation It states the general requirement 1) All product shall be manufactured with good manufacturing practice so that under f

2、oreseeable conditions of use. They do not transfer their constituents in quantities that endanger human health; cause any unacceptable change in the composition of the foodstuff.,Food grade safety compliance in France,89/109/EEC 2) In article 2, it states that any products in compliance with any EU

3、national requirement (such as French national requirement, German national requirement, Swedish national requirement) is also in compliance with the said Directive.,Food grade safety compliance in France,When placed on the market, marking requirement as follows : The words “for food use” or “food gr

4、ade symbol” Instruction on how to use the products (unless their nature they are clearly shown) Any special conditions to be observed when they are being use (eg. not for microwave usage; not suitable for fatty foodstuff) Company information : 1) Name or trade mark and the address of registered offi

5、ce or registered trade mark.,Food grade safety compliance in France,Food grade Symbol,According to EU 80/590/EEC Directive Any product in compliance with food grade Safety can display the following symbol on the packing or surface of the products. It is defined as “product for food use”.,Testing req

6、uirement in France Well established in French DGCCRF 2004-64 published on 2004 May 6 and French food regulation book no. 1227 French Arrete French Decret French Avis French BOCCRF,Food grade safety compliance in France,(A) Plastics Overall migration test according to 2002/72/EC Directive (follow EU

7、requirement) Specify 4 foodstuff simulant : Distilled water as aqueous foodstuff (pH 4.5); eg. Milk, coffee, egg 3 % acetic acid as aqueous and acidic foodstuff (pH 4.5); eg. Processed fruit, juice, meat and fish 10 % ethanol as alcoholic foodstuff; eg. Wine, beer,Food grade safety compliance in Fra

8、nce,(A) Plastics 4) Rectified olive oil (or alternative substitute : 95 % ethanol and iso-octane) as fatty foodstuff; eg. Meat and fish, cake, nuts Specified maximum permissible limit : 10 milligram per square decimeter 60 milligram per kilogram of foodstuff in contact with Test condition : Follow t

9、he guideline as described in EN 1186-1 : 2002,Food grade safety compliance in France,(A) Plastics Test condition : b) When product in contact with food at 0 to 5 C for maximum as 24 hours, choose condition as 5 C for 24 hours c) When product in contact with food at room temperature for maximum as 2

10、hours, choose condition as 40 C for 2 hours d) When product in contact with food in microwave oven for maximum as 30 minutes or cooking purpose as 1 hour maximum, choose condition as 100 C for 2 hours for aqueous foodstuff; 175 C for 2 hours for fatty foodstuff,Food grade safety compliance in France

11、,(A) Plastics Test condition : e) When product in prolonged contact with food at room temperature (time is not unknown), choose condition as 40 C for 10 days f) Test condition as 40 C for 10 days is the worst foreseeable condition amongst all test condition (except those at temperature greater than

12、70 C),Food grade safety compliance in France,(A) Plastics Specific migration test according to French DGCCRF 2004-64 (French national regulation Not so well defined in EU) PVC plastics residual vinyl chloride monomer a) Maximum permissible limit : not more than 1 mg/kg 2) Melamine plastics formaldeh

13、yde in 3 % acetic acid at 70 C, 2 hours Maximum permissible limit : not more than 15 mg/kg of foodstuff in contact with 3) others,Food grade safety compliance in France,(B) Ceramics, glass and crystal Extractable lead and cadmium according to 84/500/EEC Directive (follow EU requirement) Specify 4 ca

14、tegory : Flatware or article cannot be filled up Maximum permissible limit : lead 0.8 mg/sq. dm Maximum permissible limit : cadmium 0.07 mg/sq. dm 2) Hollow ware (capacity 3L) Maximum permissible limit : lead 4.0 mg/L Maximum permissible limit : cadmium 0.3 mg/L,Food grade safety compliance in Franc

15、e,(B) Ceramics, glass and crystal 3) Cooking ware or hollow ware with capacity over 3 L Maximum permissible limit : lead 1.5 mg/L Maximum permissible limit : cadmium 0.1 mg/L 4) Lip and rim region (apply for cup and mug with external colour decoration within 20 mm region from the rim) Maximum permis

16、sible limit : lead 2 mg per article Maximum permissible limit : cadmium 0.2 mg per article,Food grade safety compliance in France,(C) Enameled ware Extractable lead, cadmium and chromium (VI) according to French recommendation DGCCRF 2004-64 (French national requirement EU only specify requirement f

17、or extractable lead and cadmium) Specify 4 category : Flatware or article cannot be filled up Maximum permissible limit : lead 0.8 mg/sq. dm Maximum permissible limit : cadmium 0.07 mg/sq. dm Maximum permissible limit : chromium (VI) 0.005 mg/sq. dm,Food grade safety compliance in France,(C) Enamele

18、d ware 2) Hollow ware (capacity 3L) Maximum permissible limit : lead 4.0 mg/L Maximum permissible limit : cadmium 0.3 mg/L Maximum permissible limit : chromium (VI) 0.03 mg/L 3) Cooking ware or hollow ware with capacity over 3 L Maximum permissible limit : lead 1.5 mg/L Maximum permissible limit : c

19、admium 0.1 mg/L Maximum permissible limit : chromium (VI) 0.03 mg/L,Food grade safety compliance in France,(C) Enameled ware 4) Lip and rim region (apply for cup and mug with external colour decoration within 20 mm region from the rim) Maximum permissible limit : lead 2 mg per article Maximum permis

20、sible limit : cadmium 0.2 mg per article Maximum permissible limit : chromium (VI) 0.015 mg per article,Food grade safety compliance in France,(D) Rubber Specific migration test according to 93/11/EC Directive (follow EU requirement) 1) N-nitrosamine content : not more than 0.01 mg/kg 2) N-nitrosata

21、ble substances : not more than 0. 1 mg/kg Special test according to French Arrete 9 november 1994 (French national requirement no such requirement in EU) 1) Volatile organic matter at 103 C for 4 hours a) Maximum permissible limit : 0.5 % w/w,Food grade safety compliance in France,(D) Rubber Special

22、 test according to French Arrete 9 november 1994 (French national requirement no such requirement in EU) 2) Extractive test according to 2002/72/EC Directive. a) Distilled water as aqueous foodstuff (pH 4.5); eg. Milk, coffee, egg b) 3 % acetic acid as aqueous and acidic foodstuff (pH 4.5); eg. Proc

23、essed fruit, juice, meat and fish c) 10 % ethanol as alcoholic foodstuff; eg. Wine, beer d) Rectified olive oil (or substitute of fatty foodstuff simulant : 95 % ethanol and isooctane,Food grade safety compliance in France,(D) Rubber Special test according to French Arrete 9 november 1994 (French na

24、tional requirement no such requirement in EU) 3) Aromatic amines in 3 % acetic acid extractives at 40 C, 2 hours Maximum permissible limit : 1 milligram per kilogram of foodstuff in contact with 4) Formaldehyde in 3 % acetic acid extractives at 40 C, 2 hours Maximum permissible limit : 3 milligram p

25、er kilogram of foodstuff in contact with 5) Peroxide value : not detected,Food grade safety compliance in France,(E) Silicon rubber Special test according to French Arrete 25 november 1992 (French national requirement no such requirement in EU) 1) Volatile organic matter at 200 C for 4 hours Maximum

26、 permissible limit : 0.5 % w/w 2) Overall migration test according to 2002/72/EC Directive. a) Distilled water as aqueous foodstuff (pH 4.5); eg. Milk, coffee, egg b) 3 % acetic acid as aqueous and acidic foodstuff (pH 4.5); eg. Processed fruit, juice, meat and fish,Food grade safety compliance in F

27、rance,(E) Silicon rubber 2) Overall migration test according to 2002/72/EC Directive. c) 10 % ethanol as alcoholic foodstuff; eg. Wine, beer d) Rectified olive oil (or substitute of fatty foodstuff simulant : 95 % ethanol and isooctane) e) Test condition : Follow the guideline as described in EN 118

28、6-1 : 2002 f) Maximum permissible limit : similar to that of plastics (10 mg per sq. dm or 60 mg per kg of foodstuff in contact with),Food grade safety compliance in France,(E) Silicon rubber 3) Peroxide value : not detected 4) Organotin specific migration of tin in 3 % acetic acid, 40 C, 2 hours a)

29、 Maximum permissible limit : not more than 0.1 mg-tin per kilogram of foodstuff in contact with,Food grade safety compliance in France,(F) Wood without any varnishing (paint, lacquer) Special test according to French Decret 94-647 (French national requirement no such requirement in EU) 1) Pentachlor

30、ophenol - PCP Maximum permissible limit : 0.1 mg/kg,Food grade safety compliance in France,(G) Wood with varnishing (paint, lacquer) Special test according to French DGCCRF 2004-64 (French national requirement no such requirement in EU) 1) Pentachlorophenol - PCP Maximum permissible limit : 0.1 mg/k

31、g 2) Extractive test according to 2002/72/EC Directive. 3 % acetic acid as aqueous and acidic foodstuff 10 % ethanol as alcoholic foodstuff 95 % ethanol as fatty foodstuff Isooctane as fatty foodstuff,Food grade safety compliance in France,(H) Paper Special test according to French DGCCRF 2004-64 (F

32、rench national requirement no such requirement in EU) 1) Pentachlorophenol - PCP Maximum permissible limit : 0.1 mg/kg 2) Polychlorinated biphenyls - PCBs Maximum permissible limit : 2 mg/kg 3) Formaldehyde release in cold water or hot water a) Maximum permissible limit : 1 milligram per square deci

33、meter,Food grade safety compliance in France,(H) Paper 4) Sensory test for taste and odour Robinsons test using a 5 point scale 0,1,2,3,4 by a 5 member panelist Maximum permissible limit : average point scale not more than 2.5 5) Extractable heavy metal in cold water or hot water Mercury : not more

34、than 0.3 mg/kg Lead : not more than 3 mg/kg Cadmium : not more than 0.5 mg/kg Chromium (VI) : not more than 0.25 mg/kg,Food grade safety compliance in France,(H) Paper 6) Transfer of antimicrobic constituents Test method : EN 1104 : 1996 using Bacillus subtilis and Aspergillus niger as challenging c

35、ulture Specification : absence of zone inhibition. That is, no transfer of antimicrobic constituents from paper surface to foodstuff in contact with,Food grade safety compliance in France,(I) Metal without any coating or electroplating Special test according to French DGCCRF 2004-64 (French national

36、 requirement no such requirement in EU) Copper metal or copper alloy is not allowed to be in contact with foodstuff Specific migration of copper into foodstuff : not allowed Define into different kind of metal Stainless steel = INOX Carbon steel Aluminium Other metal alloys such as cast iron, tin al

37、lloy, zinc alloy,Food grade safety compliance in France,Stainless steel Composition check according to French Arrete 13 january 1976 and DGCCRF 2004-64 (French national requirement no such requirement in EU) Total chromium (Cr) : not less than 13 % Total tantalum (Ta): not more than 1 % Total niobiu

38、m (Nb) : not more than 1 % Total zirconium (Zr) : not more than 1 % Total molybdenum (Mo) : not more than 4 % Total titanium (Ti) : not more than 4 % Total aluminium (Al) : not more than 4 %,Food grade safety compliance in France,Stainless steel 8) Total copper (Cu) : not more than 4 % 9) Classifica

39、tion of stainless steel grade (additional, not define clearly whether it is compulsory or not) Ferritic stainless steel with symbol and number notation; eg. X6Cr17, number 1.4016 Marstenitic stainless steel with symbol and number notation; eg. X12CrS13, number 1.4005 Austhenitic stainless steel with

40、 symbol and number notation; eg. X10CrNi18-8, number 1.4310 Classification by determination of carbon, silicon, sulfur, maganese, nickel.,Food grade safety compliance in France,Carbon steel Composition check according to DGCCRF 2004-64 (French national requirement no such requirement in EU) Total Co

41、balt (Co) : not more than 0.05 % Total copper (Cu) : not more than 4 % Total molybdenum (Mo) : not more than 4 % Total Niobium (Nb) : not more than1 % Total Zirconium (Zr) : not more than1 % Total lead (Pb) : not more than 0.01 % Total cadmium (Cd) : not more than 0.01 % Total arsenic (As) : not mor

42、e than 0.03 %,Food grade safety compliance in France,Aluminium - Composition check according to French Arrete 27 august 1987 and DGCCRF 2004-64 (French national requirement no such requirement in EU) Aluminium metal (aluminium content as not less than 99 %) Check for 13 metal parameters including al

43、uminium 2) Aluminium alloy (aluminium content as not less than 13 %) Check for 19 metal parameters including aluminium,Food grade safety compliance in France,Others - Indesirable element according to DGCCRF 2004-64 (French national requirement no such requirement in EU) Total lead (Pb) : not more th

44、an 0.05 % Total cadmium (Cd) : not more than 0.01 % Total arsenic (As) : not more than 0.03 %,Food grade safety compliance in France,(J) Metal with electroplating Special test according to French DGCCRF 2004-64 (French national requirement no such requirement in EU) Test divided into 2 parts Metal b

45、ase substrate (surface not in contact with food, but it will in contact with food after prolonged usage ?) Composition test for compliance with requirement for stainless steel Composition test for compliance with requirement for carbon steel Composition test for compliance with requirement for alumi

46、nium,Food grade safety compliance in France,(J) Metal with electroplating 1) Metal base substrate (surface not in contact with food, but it will in contact with food after prolonged usage ?) d) Composition test for compliance with requirement for other metal alloy 2) Electroplating surface (surface

47、in contact with food directly) Extractable Nickel (Ni) : not more than 0.5 milligram per kilogram of foodstuff in contact with Extractable Chromium (VI) (Cr) : not more than 5 milligram per kilogram of foodstuff in contact with Extractable Zinc (Zn) : not more than 10 milligram per kilogram of foods

48、tuff in contact with Condition: duplicate: 2hours, Water, 0.05%citric acid, 10% ethanol,Food grade safety compliance in France,(K) Metal with organic coating (eg. non-stick surface) Special test according to French DGCCRF 2004-64 (French national requirement no such requirement in EU) Test divided i

49、nto 2 parts Metal base substrate (surface not in contact with food, but it will in contact with food after prolonged usage ?) Composition test for compliance with requirement for stainless steel Composition test for compliance with requirement for carbon steel Composition test for compliance with requirement for carbon steel,Food grade safety compliance in France,(K) Metal with organic coating (eg. non-stick surface) 1) Metal base substrate (surface not in contact with food, but it will in contact with food after prolonged usage