ABI Support Training - 岛津仪器培训资料.ppt

1、ABI Support Training,Shimadzu Scientific Instruments,Prominence Set-up and Configuration,Feeding the MS,ABI Shimadzu Relationship,Sales Agreement ABI can sell Shimadzu HPLC with ABI MS SSI sales fully compensated Demo Lab Support Toronto Demo lab projects with Dr. Sakuma Foster City and Framingham s

2、upport Presentations,Control of the Prominence HPLC,There are 3 ways to interface and control a Shimadzu HPLC CBM-20A CBM-20A Lite SIL-HT (SCL-10Avp) Communications settings are the same for all three sort of,Control of the Prominence HPLC,Please communicate with your local Shimadzu reps to coordina

3、te installations and training. The Shimadzu Engineer will have either already set-up the HPLC or, ideally, is there with you to assist in the installation. Shimadzu is your partner in this endeavor. Please use the resources available to you. Having said this, we all no that the world is not an ideal

4、 place and “stuff happens”,Setting Comms SIL-HT(SCL-10Avp),From MENU Screen: Press 4 (system) Set RELAY 1 to start with arrow keys Press F3 (next) Set: CLASSvp to 5 or 6 Interface to RS-232C Baud Rate to 19200 Level to ENHANCED POWER CYCLE the unit to save settings ROM version 5.33 OR LATER is accep

5、table.,Setting Comms CBM-20A (Lite),From the front panel of either a pump or autosampler where the CBM Lite is installed: Press VP key 4X to CALIBRATION Press FUNC Enter 00000 (five zeroes) followed by ENTER Press BACK Press ENTER,Setting Comms CBM-20A (Lite),Press FUNC 2X and begin entering the fol

6、lowing. After entering a value press enter, then FUNC to move to next parameter. INTERFACE: 1 for RS-232C 2 for Ethernet (PREFERRED) ETHERNET SPEED 0 for auto-detect,Setting Comms CBM-20A (Lite),The following 4 settings should be set up by the Shimadzu engineer USE GATEWAY (only if connected to netw

7、ork) 0 for NO 1 for YES IP ADDRESS SUBNET MASK DEFAULT GATEWAY Important to you: TRS MODE 2 for ANALYST communication POWER CYCLE the unit,Supplied by customers IT group,Preferred to use Ethernet for Comms,We have recently learned that the MIMIC Driver in Analyst does not work with USB/RS232 convert

8、ers. If RS232 is desired please use a Serial expansion board Better to add another Network Card and set it up as a peer-to-peer network.,Setting IP address on PC,Right click My Network Places, “properties” Right click on the desired Local Area Connection Select PROPERTIES Highlight Internet Protocol

9、 (TCP/IP) Click PROPERTIES Click on “Use the following IP address” and fill in the info,Settings for Peer-to-Peer,Default settings on CBM-20A (Lite) IP Address: 192.168.200.99 Subnet Mask: 255.255.255.0 Default Gateway: Not Used Set the PC up as a “different house on the same street” IP Address: 192

10、.168.200.97 Subnet Mask: 255.255.255.0 Default Gateway: Not Used,Prominence Patch,Ready for release in December of 2005 MUST have previous patches (April and July) installed. Old Methods and Configurations DO NOT work. Methods must be re-created Remind customers to review RELEASE NOTES,Prominence Pa

11、tch,If Upgrading to Prominence Patch make sure all units in LC-20 mode NOT VP VP CalibrationOP MODE20A Quick Check look for all remote LEDs to be lit to ensure proper link to controller. Make HPLC run longer than MS run - 30 Sec.,Analyst 1.4.1 Set-up,Analyst 1.4 on WindowsXP SP2,Analyst 1.4 on Windo

12、wsXP SP2,System Controller Selection,System Controller Configuration,System Controller Configuration,System Controller Configuration,Pump Selection,Pump Configuration,Pump Configuration,Detector Selection,Detector Configuration - UV,Column Oven Selection,Column Oven Configuration,Sub-Controller Sele

13、ction,Sub-Controller Configuration,Autosampler Selection,Autosampler Configuration SIL-HT,Autosampler Configuration SIL-20,Ready to RUN,Setting up a method in Analyst Some Shimadzu info and tips,LC Sync,Pump Set-up,Pump Set-up,Detector Set-up,Autosampler Set-up,Analyst does not support Control Rack!

14、,Oven Set-up,FCV-12AH Positions,Position “0”,Position “1”,EVENT Checked means contact closed at initial conditions,Time Program,Time Program,Solvent Selection Set-up,Wiring Connections,Sciex General connection cable 25 pin Green/ Black and White/Black (pins 21 & 22) are connected to any of the Shima

15、dzu relays typically RELAY/EVENT 1 for a start signal. Must Short out (twist the pair together) Pins 9 (Red/Black) & 10 (Orange/Black) standard procedure for Sciex installs.,Resources Available to you,Your local Shimadzu support structure Sales Tech support Service Regional Office We can provide you

16、 with names and numbers 9 Regional offices 50 Sales people 30 Tech Support 40 Service They are all compensated on ABI sales and are available to help you.,Shimadzu Corporate 800-477-1227 Extension: 1300 Gets Customer Service to direct the call to Phone Tech support. Excellent at troubleshooting comms Familiar with Analyst basics. 1994 Gets Me. I travel a lot 1366 Gets Sue Steinike, MRKT Specialist, familiar with Analyst,Regional Offices,North Atlantic New England, NY (800) 396-4943 New Jersey NJ and NYC (800) 439-8555 Mid-Atlantic PA, DE, VA, WV, So NJ, MD, NE OH (800) 388-6996 Southea