离子计检定记录

JJG757200X离子计检定/校准原始记录检定校准日期 2016 年 1 月 24 日 共 4 页 第 1 页记录编号20160048证书编号化学 字第 20160048 号结 论合格送检单位国营814厂检定员陈 宇核验员倪德志样品名称离子分析仪型号规格PXSJ-216等 级0.001级制造厂上海精密科学仪器有限公司出厂编号050157生产日期2005.9环境条件温度：19 湿度：54 RH备 注主要基标准器名 称直流电位差计型号规格UJ-21编 号079有效期2006.6.13证书号电位字第20050091号等 级0.01级依据的技术文件： JJG 757-200X(一) 外观和初步检查(二) 离子计示值误差 PXl 等电位值：/ 温度补偿器值： 输入值00.20.40.60.81234567示值10.0020.2020.4020.6020.8021.0002.0013.0014.0015.0026.0027.00020.0020.2020.4020.6020.8021.0002.0013.0014.0015.0026.0027.000平 均0.0020.2020.4020.6020.8021.0002.0013.0014.0015.0026.0027.000px-0.002-0.002-0.002-0.002-0.0020.000-0.001-0.001-0.001-0.002-0.0020.000输入值891011121313.213.413.613.8-示值17.9988.9999.99910.99912.00013.00013.20013.40013.60013.800-27.9988.9999.99910.99912.00013.00013.20013.40013.60013.800-平 均7.9988.9999.99910.99912.00013.00013.20013.40013.60013.800-px0.0020.0010.0010.0010.0000.0000.0000.0000.0000.000-PX2输入值00.20.40.60.81234567示值10.0030.2030.4030.6030.8030.9961.9962.9973.9964.9975.9966.99620.0030.2030.4030.6030.8030.9961.9962.9973.9964.9975.9966.996平 均0.0030.2030.4030.6030.8030.9961.9962.9973.9964.9975.9966.996px-0.003-0.003-0.003-0.003-0.0030.0040.0040.0030.0040.0030.0040.004输入值891011121313.213.413.613.8-示值17.9968.9969.99510.99511.99412.99413.19413.39413.59413.794-27.9968.9969.99510.99511.99412.99413.19413.39413.59413.794-平 均7.9968.9969.99510.99511.99412.99413.19413.39413.59413.794-px0.0040.0040.0050.0050.0060.0060.0060.0060.0060.006- mV + 输入024681020406080100示值10.01.93.95.97.99.919.939.959.979.999.920.01.93.95.97.99.919.939.959.979.999.9平均0.01.93.95.97.99.919.939.959.979.999.9误差/%FS0.000-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.05 + 输入200300400500600700800900100011001200示值1199.9300.0400.0500.1600.0700.1800.1900.11000.21100.21200.22199.9300.0400.0500.1600.0700.1800.1900.11000.21100.21200.2平均199.9300.0400.0500.1600.0700.1800.1900.11000.21100.21200.2误差/%FS-0.0050.000.000.0050.000.0050.0050.0050.010.010.01 + 输入130014001500160017001720174017601780示值11300.21400.21500.31600.31700.31720.31740.41760.41780.321300.21400.21500.31600.31700.31720.31740.41760.41780.3平均1300.21400.21500.31600.31700.31720.31740.41760.41780.3误差/%FS0.0100.0100.0150.0150.0150.0150.020.020.015 - 输入024681020406080100示值10.02.04.05.97.99.920.020.060.080.0100.020.02.04.05.97.99.920.040.060.080.0100.0平均0.01.93.95.97.99.919.939.959.979.999.9误差/%FS0.000-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.05 - 输入200300400500600700800900100011001200示值1199.9300.0400.1500.1600.1700.1800.1900.21000.21100.21200.22199.9300.0400.1500.1600.1700.1800.1900.21000.21100.21200.2平均199.9300.0400.0500.1600.1700.1800.1900.21000.21100.21200.2误差/%FS-0.050.000.000.050.050.050.050.100.100.100.10 - 输入130014001500160017001720174017601780示值11300.21400.31500.31600.31700.31720.41740.41760.51780.521300.21400.31500.31600.31700.31720.41740.41760.51780.5平均1300.21400.31500.31600.31700.31720.41740.41760.51780.5误差/%FS0.100.050.150.150.150.020.020.0250.025C 浓度 或 离子pX值输入电位17.80935.61846.03553.42759.16076.96887.38694.777100.510105.195112.587标准值 20406080100200300400500600800示值120.0340.0360.0480.03100.02200.02300.12400.12500.37599.92799.92220.0340.0360.0480.03100.02200.02300.12400.12500.37599.92799.92平 均20.0340.0360.0480.03100.02200.02300.12400.12500.37599.92799.92Cw0.030.030.040.030.020.0020.0120.0120.0370.0080.008输入电位118.32123.003126.964130.395133.421134.810136.128153.937164.355171.749177.479标准值100012001400160018001900200040006000800010000示值11000.51200.01400.01598.01798.01900.01999.03998.05987.07997.09988.021000.51200.01400.01598.01798.01900.01999.03998.05987.07997.09988.0平 均1000.51200.01400.01598.01798.01900.01999.03998.05987.07997.09988.0Cw0.0500-0.02-0.020-0.01-0.02-0.03-0.03-0.12注 (三) 输入电流 温度补偿器示值 25 串联电阻电 计 示 值 /pX输入电流123平均变化量 0 7.0007.0007.0007.0000.0017 0.10 pA 996 M6.9986.9986.9996.9983(四) 输 入 阻 抗串联电阻输入电位电计示值 /mV平均 /mV范围 /mV变化量 /mV阻 抗0 +1000 mV1000.21000.2 1000.2 1000.202000.430.832.4 T-1000 mV-1000.2-1000.2 -1000.3 -1000.23996 M+1000 mV999.9999.8 999.8 999.831999.60-1000 mV-999.8-999.7 -999.8 -999.77(五) 离子计重复性输入电位/mV电 计 示 值s123456300.000300.0300.0200.9300.0300.0200.90.05 mV354.9605.9965.9975.9965.9965.9975.9970.0005 pX (六) 温度补偿误差温度补偿示值 /输入电位/mV电 计 示 值 /pX标称值/pX误差/pX12平 均5331.1466.0016.0016.0016.000-0.000515343.0566.0016.0026.0026.000-0.00125354.9606.0026.0026.0026.000-0.00145378.7686.0026.0026.0026.000-0.00160396.6306.0026.0036.0026.000-0.001(七) 温度测量误差 输入量标准温度 /5.025.045.0示 值 /5.125.145.0T /+0.1+0.10.0 (八) 输出误差 /输入值012345678910示 值无输出值12平 均误差 (九) 稳定性时间 /min0102030405060pXmaxpX00.0030.0030.0020.0020.0030.0030.0030.001pXh6.0026.0026.0036.0026.0036.0026.0020.001 (十) 电源电压适应性电源电压标准电压仪器示值+10 % 仪器示值-10 % 仪器示值pXmaxpX00.003 pX0.002 Px0.003 Px0.001 pXpXh6.002 pX6.002 pX6.002 pX0.000 pX(十一) 斜率补偿范围 斜率补偿器位置输入电位 / mV 范围备 注12平 均数字计算100上限下限(十二) 等电位调节范围 调节器位置上限中下限调节范围备 注示 值无(十三) 定位调节范围调节器位置上限中下限调节范围示 值数字调节 (十四) 绝缘电阻 60 M离子计检定/校准原始记录检定校准日期 2016 年 1 月 27 日 共 4 页 第 1 页记录编号20160090证书编号化学 字第 20160090 号结 论合格送检单位四川省冶金工业环境保护监测所检定员陈 宇核验员倪德志样品名称离子活度计型号规格PXS-215等 级0.001级制造厂上海精科雷磁仪器厂出厂编号90054生产日期1999.5环境条件温度：18 湿度：54 RH备 注主要基标准器名 称直流电位差计型号规格UJ-21编 号079有效期2006.6.13证书号电位字第20050091号等 级0.01级依据的技术文件： JJG 757-200X(一) 外观和初步检查(二) 离子计示值误差 PXl 等电位值： 温度补偿器值：25 输入值-7-6-5-4-3-2-1-0.8-0.6-0.4-0.20示值1-6.999-5.999-4.999-3.999-2.999-2.000-1.000-0.800-0.600-0.399-0.1980.0022-6.999-5.999-4.999-3.999-2.999-2.000-1.000-0.800-0.600-0.399-0.1980.002平 均-6.999-5.999-4.999-3.999-2.999-2.000-1.000-0.800-0.600-0.399-0.1980.002px0.0010.0010.0010.0010.0010.0000.0000.0000.0000.0010.0020.002输入值0.20.40.60.81234567-示值10.2010.4000.6000.8001.0002.0003.0004.0004.9995.9996.999-20.2010.4000.6000.8001.0002.0003.0003.9994.9995.9996.999-平 均0.2010.4000.6000.8001.0002.0003.0003.9994.9995.9996.999-px0.0010.0000.0000.0000.0000.0000.000-0.001-0.001-0.001-0.001-PX2输入值-7-6-5-4-3-2-1-0.8-0.6-0.4-0.20示值1-7.001-6.001-5.002-4.001-3.001-2.001-1.0010.8000.6000.4000.2010.0022-6.999-5.999-4.999-3.999-2.999-2.000-1.000-0.800-0.600-0.399-0.1980.002平 均-6.999-5.999-4.999-3.999-2.999-2.000-1.000-0.800-0.600-0.399-0.1980.002px0.0010.0010.0010.0010.0010.0000.0000.0000.0000.0010.0020.002输入值0.20.40.60.81234567-示值10.1990.3990.5980.7980.9971.9972.9963.9964.9965.9966.995-20.1990.3990.5980.7980.9971.9972.9963.9964.9965.9966.995-平 均0.1990.3990.5980.7980.9971.9972.9963.9964.9965.9966.995-px-0.001-0.001-0.002-0.002-0.003-0.003-0.004-0.004-0.004-0.004-0.005- mV + 输入024681020406080100示值10.02.04.06.08.010.120.140.160.180.1100.120.02.04.06.08.010.120.140.160.180.1100.1平均0.000000.10.10.10.10.10.1误差/%FS000000.0050.0050.0050.0050.0050.005 + 输入200300400500600700800900100011001200示值1200.1300.1400.1500.2600.2700.2800.2900.21000.21100.21200.32200.1300.1400.1500.2600.2700.2800.2900.21000.21100.21200.3平均0.10.10.10.20.20.20.20.20.20.20.05误差/%FS0.0050.0050.0050.010.010.010.010.010.010.010.015 + 输入13001400150016001700180019001920194019601980.4示值1300.31400.31500.31600.41700.41800.51900.51920.51940.51960.41980.41300.31400.31500.31600.41700.41800.51900.51920.51940.51960.41980.4平均1300.31400.31500.31600.41700.41800.51900.51920.51940.51960.41980.4误差/%FS0.0150.0150.0150.020.020.0250.0250.0250.0250.020.02 - 输入024681020406080100示值10.02.04.06.08.010.120.140.160.180.1100.120.02.04.06.08.010.120.140.160.180.1100.1平均0.02.04.06.08.010.120.140.160.180.1100.1误差/%FS000000.0050.0050.0050.0050.0050.005 - 输入200300400500600700800900100011001200示值1200.1300.1400.1500.1600.1700.2800.2900.21000.21100.21200.22200.1300.1400.1500.1600.1700.2800.2900.21000.21100.21200.2平均200.1300.1400.1500.1600.1700.2800.2900.21000.21100.21200.2误差/%FS0.0050.0050.0050.0050.0050.010.010.010.010.010.01 - 输入13001400150016001700180019001920194019601980示值11300.21400.21500.31600.31700.31800.41900.41920.41940.31960.31980.321300.21400.21500.31600.31700.31800.41900.41920.41940.41960.31980.3平均1300.21400.21500.31600.31700.31800.41900.41920.41940.41960.31980.3误差/%FS0.010.010.0150.0150.0150.0200.0200.0200.0200.0150.015C 浓度 输入电位标准值 示值12平 均Cw输入电位标准值示值12平 均Cw注 (三) 输入电流 温度补偿器示值 25 串联电阻电 计 示 值 /pX输入电流123平均变化量 0 0.0020.0020.0020.00200.0020 0.12 pA 996 M0.0040.0040.0040.0040(四) 输 入 阻 抗串联电阻输入量 电计示值平均范围变化量阻 抗0 +6 pX5.9995.9995.9995.99911.9980.00403.0 T -6 pX-5.999-5.999-5.999-5.999996 M+6 pX5.9945.9955.9955.994711.9940-6 pX-5.999-6.000-5.999-5.9993(五) 离子计重复性输入电位/mV电 计 示 值s123456300.000300.0300.1300.0300.0300.1300.00.05 mV354.9605.9965.9975.9965.9975.9975.9970.0005 pX (六) 温度补偿误差温度补偿示值 /输入电位/mV电 计 示 值 /pX标称值/pX误差/pX12平 均5331.1465.9955.9955.9956.000-0.00315343.0566.0006.0006.000-0.00025354.9605.9995.9995.999-0.00045378.7685.9995.9995.999-0.00160396.6305.9985.9985.998-0.001(七) 温度测量误差输入量标准温度 /5.025.045.0示 值 /5.125.145.0T /+0.1+0.10.0 (八) 输出误差输入值012345678910示 值无输出值12平 均误差 (九) 稳定性时间 / min0102030405060pXmaxpX00.0030.0030.0020.0020.0030.0030.0030.001pXh5.9995.9995.9996.0005.9995.9995.9990.001 (十) 电源电压适应性电源电压标准电压仪器示值+10 % 仪器示值-10 % 仪器示值pXmaxpX00.003 pX0.002 Px0.003 Px0.001 pXpXh5.999 pX5.999 pX6.000 pX0.001 pX(十一) 斜率补偿范围 斜率补偿器位置输入电位 / mV 范围备 注12平 均数字计算100上限下限(十二) 等电位调节范围 调节器位置上限中下限调节范围备 注示 值无(十三) 定位调节范围调节器位置上限中下限调节范围示 值数字调节 (十四) 绝缘电阻 100 M离子计检定/校准原始记录检定校准日期 2005 年 10 月 11 日 共 4 页 第 1 页记录编号1382证书编号化学 字第 20051382 号结 论合格送检单位眉山市东坡区疾病预防控制中心检定员陈 宇核验员倪德志样品名称数字pH/离子计型号规格SA 720等 级0.01级制造厂ORION出厂编号RQ 173 A生产日期/环境条件温度：22 湿度：63 RH备 注主要基标准器名 称直流电位差计型号规格UJ-21编 号079有效期2006.6.13证书号电位字第20050091号等 级0.01级依据的技术文件： JJG 757-200X(一) 外观和初步检查(二) 离子计示值误差 PXl 等电位值： 温度补偿器值： 输入值00.20.40.60.81234567示值10.010.210.410.610.811.012.003.004.005.006.007.0020.010.210.410.610.811.012.013.004.005.006.007.00平 均0.010.210.410.610.811.012.003.004.005.006.007.00px-0.01-0.01-0.01-0.01-0.01-0.010.000.000.000.000.000.00输入值891011121313.213.413.613.814-示值18.008.999.9910.9911.9912.9913.1913.3913.5913.7913.99-28.009.009.9910.9911.9912.9913.1913.3913.5913.7913.99-平 均8.009.009.9910.9911.9912.9913.1913.3913.5913.7913.99-px0.000.000.010.010.010.010.010.010.010.010.01-PX2输入值00.20.40.60.81234567示值1无2平 均px输入值891011121313.213.413.613.814-示值1-2-平 均-px- mV + 输入024681020406080100示值10.01.93.95.97.99.919.939.959.879.899.820.01.93.95.97.99.919.939.959.879.899.8平均0.01.93.95.97.99.919.939.959.879.899.8误差/%FS0.00-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.1-0.1-0.1 + 输入200300400500600700800900100011001200示值1199.7299.7399.6499.6599.5699.5799.5899.4999.4109911992199.7299.7399.6499.6599.5699.5799.5899.4999.410991199平均199.7299.7399.6499.6599.5699.5799.5899.4999.410991199误差/%FS-0.15-0.15-0.2-0.2-0.25-0.25-0.25-0.3-0.3-0.5-0.5 + 输入13001400150016001700180019001920194019601980示值112991399149915991699179918991919193919591978212991399149915991699179918991919193919591979平均12991399149915991699179918991919193919591978.5误差/%FS-0.5-0.5-0.5-0.5-0.5-0.5-0.5-0.5-0.5-0.5-0.8 - 输入024681020406080100示值10.01.93.95.97.99.919.939.959.879.899.820.01.93.95.97.99.919.939.959.879.899.8平均0.01.93.95.97.99.919.939.959.979.999.9误差/%FS0.00-0.05-0.05-0.05-0.05-0.05-0.05-0.05-0.1-0.1-0.1 + 输入200300400500600700800900100011001200示值1199.7299.7399.6499.6599.5699.5799.5899.4999.4109911992199.7299.7399.6499.6599.5699.5799.5899.4999.410991199平均199.7299.7399.6499.6599.5699.5799.5899.4999.410991199误差/%FS-0.2-0.2-0.2-0.2-0.25-0.25-0.25-0.3-0.3-0.5-0.5 + 输入13001400150016001700180019001920194019601980示值112991399149915991699179918991919193919591978212991399149915991699179918991919193919591978平均12991399149915991699179918991919193919591978误差/%FS-0.5-0.5-0.5-0.5-0.5-0.5-0.5-0.5-0.5-0.5-1.0C 浓度 或 离子pX值输入电位17.80935.61846.03553.42759.16076.96887.38694.777100.510105.195112.587标准值 20406080100200300400500600800示值120.0540.0560.0580.06100.08200.08300.12400.12500.37599.92799.92220.0540.0560.0580.06100.0820