简介Waters UPLC故障排除 教育学习

,WatersUPLCTroubleshootingTraining,Agenda,ACQUITYUPLCFamily：UPLC&H-ClassWatersUPLCSystemUPLCSolventManagement(BSM)UPLCSampleManagement(SM)WatersACQUITYH-ClassSystemQuaternarySolventManager(QSM)SampleManager-FlowThroughNeedle(SM-FTN)WatersUPLCDetectorTroubleshootingTrainingWatersUPLCPDAandPDAeTUVFLRELSDOpenDiscussion,ACQUITYUPLCFamily,ACQUITYUPLCSystem,ACQUITYUPLCSystem,Detectors:Opticaland/orMassSpecTunableUVorPhotodiodeArrayOptimizedflowcellforUPLCHighspeeddatasampling,ColumnManager:InnovativepivotdesignPositionscolumntodetectorE-Cordconnection,SampleManager:LowdispersionXYZZFormatFastcycletimesLowcarryoverPlatesand/orvialsOptionalSampleOrganizer,BinarySolventManager:HighpressureblendingBinarygradientsFoursolventchoicesOn-linedegassingLowdispersiondesignUPLCpressurecapabilities,SampleOrganizer:(option)Expandscapacity(22/15/8)ShuttlesplatefeedHeated/chilled,SystemConsiderations:SmallFootprintRedesignedtubingandfittingsConsolidatedwastemanagementIntegratedsystemdiagnosticsConnectionsInsightremotediagnostics,FluidicsandConnections,TubingmanagementChromatographicsolvents:A1/A2,B1/B2TwoSampleManagerwashsolventsSealWashCommonfittingsandtoolsforusersColumninlets/outletsandfittingsFingertight,turn(use1/4”wrench)Dedicatedtubing3piececompressionscrewandferruleSmallfootprint13”wide24.25”withSampleOrganizer,UPLCSolventManager,ACQUITYUPLCSystemSolventDelivery,15KpsiperformanceAccurateandpreciseflowratesAccurateandprecisecompositionLowdelayvolumeforgradientapplications5%EthylAcetateTolueneChlorinatedsolvents:(Trichlorobenzene),UPLCSampleManager,SampleManagerFluidicsTray,PressureTransducerValveManifold,DriveGears,WashSyringesWeakWashStrongWash,MeteringSyringeDriveAssembly,MeteringSyringeValve3WayRotaryValve,MeteringSyringeAssembly,SampleSyringe50uLvolumePN410001348100LvolumePN700002570250LvolumePN410001347forusewith50Lloop,ColumnHeatingCompartment,ACQUITYIn-LineFilter,19,ColumnIn-LineFilterAssembly,ColumnIn-LineFilterAssembly,ColumnHeating,SampleManagerFlowPath,AvailableLoops,DescriptionP/NStatus1LLoop430001516Optional2LLoop430001264Optional5LLoop430001233Optional10LLoop430001326Standard20LLoop430001320Optional50LLoop430001325Optional100LLoop170001792(Kit)Optional250LLoop176001780(Kit)Optional,VolumeConfigurationMenu,BeforerunningtheCharacterizeNeedleandLoopVolumefunction,makesurethepropervolumesareconfiguredintheVolumesConfigurationmenu.TheabovevaluesarestandardforcurrentlyshippingACQUITYsystem.,RecommendedInjectionVolumes,LoopSizesandInjectionModes,RecommendedPLNOinjectionvolume20%to75%ofloopvolumeRecommendedPartialLoopInjection20%to50%ofloopvolume,ACQUITYH-ClassSystem,QSMQuaternarySolventManager,SM-FTNSampleManager-FlowThroughNeedle,CH-AHighTemperatureColumnHeaterActivePre-Heating,DetectorsTUV,PDAePDA,FLR,ELSD,TheACQUITYH-ClassSystemconsistsofthefollowing:QuaternarySolventManager(QSM)FoursolventlowpressuregradientmixingSupportsUPLCPressuresLowgradientdelayvolumeSM-FTN(SampleManager-FlowThroughNeedle)Oneinjectionmode-directinjecttypeMuchsimpler-JustspecifyinjectionvolumeExcellentrecoveryandprecisionCH-AHightemperaturecolumnheaterwithactivepre-heating,ACQUITYH-ClassSystem,QSMFluidics-FrontView,PrimaryHead,AccumulatorHead,VentValve,100ulMixer,GradientProportioningValvePairs,LowPressureManifold,DegasserChambers,SealWashPump,QSMConsoleTopLevelMenu,ACQUITYH-ClassSystem,SMDIFrontPanelFluidics,MeteringSyringeValve,CheckValveandUnion,InjectValve,WashSolventInletLine(notdegassed),LeakSensorConnections,SampleMeteringSyringe,SDMIInjectValveConnections,ToCheckValve,ToCH-AandColumn,StationarySideTube,FromPump,ToPressureTransducer,ToSampleNeedle,SampleCompartment,PowerandStatusLEDs,PlateSelectorSwitch,RotaryTray(PlateHolder),MagneticDoorSensor,PowerSwitch,SM-FTNInteractiveDisplayMenu,CH-A,ImprovedDoorGasket,AddedTubingGasket(topandbottom)For3rdpartyMassSpecatleftsideofACQUITYStack.,AllowsuseofexistingPassivePre-heater,NowirestoconnectActivePre-heater,InstallingtheActivePre-Heater,GoldPlatedCompressionScrew,PEEKFerrule,StainlessSteelCapNut,StainlessSteelTubing(withbrazedoncollet),InstallingtheActivePre-Heater,UPLCDetectors,Detectors,SupportsallcurrentACQUITYdetectorsPDAandPDAeTUVFLRELSD,ACQUITYUPLCPDA,ACQUITYUPLCPDAPMkits,